Resolution: 3.4→24.96 Å / Cor.coef. Fo:Fc: 0.891 / Cor.coef. Fo:Fc free: 0.891 / SU B: 76.972 / SU ML: 0.489 / Cross valid method: THROUGHOUT / ESU R Free: 0.549 Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. Final anisotropy correction with the Diffraction Anisotropy Server (https://services.mbi.ucla.edu/anisoscale/ ref. M. Strong, M.R. Sawaya, ...Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. Final anisotropy correction with the Diffraction Anisotropy Server (https://services.mbi.ucla.edu/anisoscale/ ref. M. Strong, M.R. Sawaya, S. Wang, M. Phillips, D. Cascio, D. Eisenberg, Proc Natl Acad Sci USA. 103, 8060-8-65, 2006).
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.26789
708
4.9 %
RANDOM
Rwork
0.23042
-
-
-
obs
0.23218
13730
82.97 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å