PDB-6dqy: Crystal Structure analysis of Superoxide Dismutase from Trichoder...

Basic information

• Entry: Database: PDB / ID: 6dqy
• Title: Crystal Structure analysis of Superoxide Dismutase from Trichoderma reesei
• Components: Superoxide dismutase
• Keywords: OXIDOREDUCTASE / enzymatic activity

Function / homology

Function:

superoxide dismutase / superoxide dismutase activity / manganese ion binding / mitochondrial matrix

Domain/homology:

: / Iron/manganese superoxide dismutase, C-terminal domain / Fe,Mn superoxide dismutase (SOD) domain / minor pseudopilin epsh fold / 3-Layer(bab) Sandwich / Manganese/iron superoxide dismutase, binding site / Manganese and iron superoxide dismutases signature. / Manganese/iron superoxide dismutase / Manganese/iron superoxide dismutase, N-terminal / Iron/manganese superoxide dismutases, alpha-hairpin domain / Manganese/iron superoxide dismutase, C-terminal / Manganese/iron superoxide dismutase, C-terminal domain superfamily / Manganese/iron superoxide dismutase, N-terminal domain superfamily / Iron/manganese superoxide dismutases, C-terminal domain / Helix Hairpins / Orthogonal Bundle / Mainly Alpha / Alpha Beta

Component:

: / Superoxide dismutase

• Biological species: Hypocrea jecorina (fungus)
• Method: X-RAY DIFFRACTION / SYNCHROTRON / MOLECULAR REPLACEMENT / Resolution: 2.3 Å
• Authors: Mendoza, E.R. / Stelmastchuk, L.B.F. / Ferreira Junior, J.R.S. / Garratt, R.C.

Funding support

Brazil, 1items

Organization	Grant number	Country
Sao Paulo Research Foundation (FAPESP)	2014/01855-2	Brazil

• Citation: Journal: To Be Published; Title: Crystal Structure of Superoxide Dismutase from Trichoderma reesei; Authors: Mendoza, E.R. / Stelmastchuk, L.B.F. / Ferreira Junior, J.R.S. / Garratt, R.C.

History

Deposition	Jun 11, 2018	Deposition site: RCSB / Processing site: RCSB
Revision 1.0	Dec 12, 2018	Provider: repository / Type: Initial release
Revision 1.1	Jan 1, 2020	Group: Author supporting evidence / Category: pdbx_audit_support / Item: _pdbx_audit_support.funding_organization
Revision 1.2	Mar 13, 2024	Group: Data collection / Database references / Derived calculations / Refinement description Category: chem_comp_atom / chem_comp_bond / database_2 / struct_conn / struct_ncs_dom_lim Item: _database_2.pdbx_DOI / _database_2.pdbx_database_accession / _struct_conn.pdbx_dist_value / _struct_conn.ptnr1_auth_asym_id / _struct_conn.ptnr1_auth_comp_id / _struct_conn.ptnr1_auth_seq_id / _struct_conn.ptnr1_label_asym_id / _struct_conn.ptnr1_label_atom_id / _struct_conn.ptnr1_label_comp_id / _struct_conn.ptnr1_label_seq_id / _struct_conn.ptnr2_auth_asym_id / _struct_conn.ptnr2_auth_comp_id / _struct_conn.ptnr2_auth_seq_id / _struct_conn.ptnr2_label_asym_id / _struct_conn.ptnr2_label_atom_id / _struct_conn.ptnr2_label_comp_id / _struct_ncs_dom_lim.beg_auth_comp_id / _struct_ncs_dom_lim.beg_label_asym_id / _struct_ncs_dom_lim.beg_label_comp_id / _struct_ncs_dom_lim.beg_label_seq_id / _struct_ncs_dom_lim.end_auth_comp_id / _struct_ncs_dom_lim.end_label_asym_id / _struct_ncs_dom_lim.end_label_comp_id / _struct_ncs_dom_lim.end_label_seq_id

Assembly

Deposited unit

A: Superoxide dismutase

B: Superoxide dismutase

C: Superoxide dismutase

D: Superoxide dismutase

E: Superoxide dismutase

F: Superoxide dismutase

G: Superoxide dismutase

H: Superoxide dismutase

I: Superoxide dismutase

J: Superoxide dismutase

K: Superoxide dismutase

L: Superoxide dismutase

M: Superoxide dismutase

N: Superoxide dismutase

O: Superoxide dismutase

P: Superoxide dismutase

Q: Superoxide dismutase

R: Superoxide dismutase

S: Superoxide dismutase

T: Superoxide dismutase

U: Superoxide dismutase

V: Superoxide dismutase

W: Superoxide dismutase

X: Superoxide dismutase

hetero molecules

Summary:

• 560 kDa, 24 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	559,565	48
Polymers	558,247	24
Non-polymers	1,319	24
Water	49,667	2757

1

A: Superoxide dismutase

C: Superoxide dismutase

D: Superoxide dismutase

O: Superoxide dismutase

hetero molecules

Summary:

• defined by author&software
• 93.3 kDa, 4 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	93,261	8
Polymers	93,041	4
Non-polymers	220	4
Water	72	4

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Buried area	8070 Å2
ΔGint	-53 kcal/mol
Surface area	32320 Å2
Method	PISA

2

B: Superoxide dismutase

G: Superoxide dismutase

I: Superoxide dismutase

T: Superoxide dismutase

hetero molecules

Summary:

• defined by author&software
• 93.3 kDa, 4 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	93,261	8
Polymers	93,041	4
Non-polymers	220	4
Water	72	4

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Buried area	7990 Å2
ΔGint	-54 kcal/mol
Surface area	32390 Å2
Method	PISA

3

E: Superoxide dismutase

J: Superoxide dismutase

P: Superoxide dismutase

S: Superoxide dismutase

hetero molecules

Summary:

• defined by author&software
• 93.3 kDa, 4 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	93,261	8
Polymers	93,041	4
Non-polymers	220	4
Water	72	4

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Buried area	8250 Å2
ΔGint	-49 kcal/mol
Surface area	32480 Å2
Method	PISA

4

F: Superoxide dismutase

K: Superoxide dismutase

M: Superoxide dismutase

Q: Superoxide dismutase

hetero molecules

Summary:

• defined by author&software
• 93.3 kDa, 4 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	93,261	8
Polymers	93,041	4
Non-polymers	220	4
Water	72	4

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Buried area	8000 Å2
ΔGint	-56 kcal/mol
Surface area	32450 Å2
Method	PISA

5

H: Superoxide dismutase

U: Superoxide dismutase

V: Superoxide dismutase

W: Superoxide dismutase

hetero molecules

Summary:

• defined by author&software
• 93.3 kDa, 4 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	93,261	8
Polymers	93,041	4
Non-polymers	220	4
Water	72	4

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Buried area	7920 Å2
ΔGint	-57 kcal/mol
Surface area	32550 Å2
Method	PISA

6

L: Superoxide dismutase

N: Superoxide dismutase

R: Superoxide dismutase

X: Superoxide dismutase

hetero molecules

Summary:

• defined by author&software
• 93.3 kDa, 4 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	93,261	8
Polymers	93,041	4
Non-polymers	220	4
Water	72	4

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Buried area	7820 Å2
ΔGint	-53 kcal/mol
Surface area	32430 Å2
Method	PISA

Unit cell

Length a, b, c (Å)	73.770, 113.060, 162.710
Angle α, β, γ (deg.)	91.590, 93.790, 89.980
Int Tables number	1
Space group name H-M	P1

Noncrystallographic symmetry (NCS)

NCS domain:

ID	Ens-ID	Details
1	1	(chain A and resid 3 through 200)
2	1	(chain B and resid 3 through 200)
3	1	(chain C and resid 3 through 200)
4	1	(chain D and resid 3 through 200)
5	1	(chain E and resid 3 through 200)
6	1	(chain F and resid 3 through 200)
7	1	(chain G and resid 3 through 200)
8	1	(chain H and resid 3 through 200)
9	1	(chain I and resid 3 through 200)
10	1	(chain J and resid 3 through 200)
11	1	(chain K and resid 3 through 200)
12	1	(chain L and resid 3 through 200)
13	1	(chain M and resid 3 through 200)
14	1	(chain N and resid 3 through 200)
15	1	(chain O and resid 3 through 200)
16	1	(chain P and resid 3 through 200)
17	1	(chain Q and resid 3 through 200)
18	1	(chain R and resid 3 through 200)
19	1	(chain S and resid 3 through 200)
20	1	(chain T and resid 3 through 200)
21	1	(chain U and resid 3 through 200)
22	1	(chain V and resid 3 through 200)
23	1	(chain W and resid 3 through 200)
24	1	(chain X and resid 3 through 200)

NCS domain segments:

Component-ID: 1 / Ens-ID: 1 / Beg auth comp-ID: VAL / Beg label comp-ID: VAL / End auth comp-ID: ASP / End label comp-ID: ASP / Auth seq-ID: 3 - 200 / Label seq-ID: 3 - 200

Dom-ID	Selection details	Auth asym-ID	Label asym-ID
1	(chain A and resid 3 through 200)	A	A
2	(chain B and resid 3 through 200)	B	B
3	(chain C and resid 3 through 200)	C	C
4	(chain D and resid 3 through 200)	D	D
5	(chain E and resid 3 through 200)	E	E
6	(chain F and resid 3 through 200)	F	F
7	(chain G and resid 3 through 200)	G	G
8	(chain H and resid 3 through 200)	H	H
9	(chain I and resid 3 through 200)	I	I
10	(chain J and resid 3 through 200)	J	J
11	(chain K and resid 3 through 200)	K	K
12	(chain L and resid 3 through 200)	L	L
13	(chain M and resid 3 through 200)	M	M
14	(chain N and resid 3 through 200)	N	N
15	(chain O and resid 3 through 200)	O	O
16	(chain P and resid 3 through 200)	P	P
17	(chain Q and resid 3 through 200)	Q	Q
18	(chain R and resid 3 through 200)	R	R
19	(chain S and resid 3 through 200)	S	S
20	(chain T and resid 3 through 200)	T	T
21	(chain U and resid 3 through 200)	U	U
22	(chain V and resid 3 through 200)	V	V
23	(chain W and resid 3 through 200)	W	W
24	(chain X and resid 3 through 200)	X	X

Components

#1: Protein

A B C D E F G H I J K L M N O P Q R S ...
Superoxide dismutase

Details:

Mass: 23260.285 Da / Num. of mol.: 24
Source method: isolated from a genetically manipulated source
Source: (gene. exp.) Hypocrea jecorina (fungus) / Strain: QM6a / Gene: TRIREDRAFT_66345 / Production host: Escherichia coli BL21(DE3) (bacteria) / References: UniProt: G0RQS7, superoxide dismutase

#2: Chemical

A-301 B-301 C-301 D-301 E-301 F-301 G-301 H-301 I-301 J-301 K-301 L-301 M-301 N-301 O-301 P-301 Q-301 R-301 S-301 T-301 ...
ChemComp-MN / MANGANESE (II) ION

Details:

Mass: 54.938 Da / Num. of mol.: 24 / Source method: obtained synthetically / Formula: Mn

#3: Water

ChemComp-HOH / water

Details:

Mass: 18.015 Da / Num. of mol.: 2757 / Source method: isolated from a natural source / Formula: H₂O

Experimental details

Experiment

• Experiment: Method: X-RAY DIFFRACTION / Number of used crystals: 1

Sample preparation

• Crystal: Density Matthews: 2.44 ų/Da / Density % sol: 49.56 %
• Crystal grow: Temperature: 291 K / Method: vapor diffusion, hanging drop / pH: 7 / Details: 100mM Bis-Tris pH 7.0, 25% PEG3350 / PH range: 6.5-7.0

Data collection

• Diffraction: Mean temperature: 100 K
• Diffraction source: Source: SYNCHROTRON / Site: APS / Beamline: 21-ID-G / Wavelength: 0.9786 Å
• Detector: Type: RAYONIX MX-300 / Detector: CCD / Date: Feb 11, 2016
• Radiation: Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
• Radiation wavelength: Wavelength: 0.9786 Å / Relative weight: 1
• Reflection: Resolution: 2.3→93.98 Å / Num. all: 226540 / Num. obs: 226540 / % possible obs: 97.2 % / Redundancy: 3.9 % / B_iso Wilson estimate: 22.86 Ų / CC_1/2: 0.995 / R_merge(I) obs: 0.084 / R_pim(I) all: 0.049 / R_rim(I) all: 0.098 / R_sym value: 0.084 / Net I/σ(I): 11.8 / Num. measured all: 875231

Reflection shell

Diffraction-ID: 1 / Redundancy: 3.8 %

Resolution (Å)	Rmerge(I) obs	Num. measured all	Num. unique obs	CC1/2	Rpim(I) all	Rrim(I) all	Rsym value	Net I/σ(I) obs	% possible all
2.3-2.42	0.301	123159	32634	0.904	0.022	0.042	0.036	4.4	96.2
7.27-93.98	0.036	27269	7219	0.997	0.036	0.072	0.062	22	97.8

Processing

Software

Name	Version	Classification
PHENIX	1.11.1_2575	refinement
SCALA	3.3.22	data scaling
PDB_EXTRACT	3.24	data extraction
iMOSFLM		data reduction
PHENIX		phasing

Refinement

Method to determine structure: MOLECULAR REPLACEMENT / Resolution: 2.3→81.146 Å / SU ML: 0.24 / Cross valid method: THROUGHOUT / σ(F): 1.98 / Phase error: 20.47

	Rfactor	Num. reflection	% reflection
Rfree	0.2066	11460	5.06 %
Rwork	0.1621	-	-
obs	0.1643	226479	97.22 %

• Solvent computation: Shrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å
• Displacement parameters: B_iso max: 113.4 Ų / B_iso mean: 31.2597 Ų / B_iso min: 6.14 Ų

Refinement step

Cycle: final / Resolution: 2.3→81.146 Å

	Protein	Nucleic acid	Ligand	Solvent	Total
Num. atoms	38662	0	24	2757	41443
Biso mean	-	-	23.11	30.71	-
Num. residues	-	-	-	-	4983

Refine LS restraints

Refine-ID	Type	Dev ideal	Number
X-RAY DIFFRACTION	f_bond_d	0.007	39741
X-RAY DIFFRACTION	f_angle_d	0.777	54094
X-RAY DIFFRACTION	f_chiral_restr	0.05	5823
X-RAY DIFFRACTION	f_plane_restr	0.006	6923
X-RAY DIFFRACTION	f_dihedral_angle_d	10.907	23111

Refine LS restraints NCS

Ens-ID	Dom-ID	Auth asym-ID	Number	Refine-ID	Rms	Type
1	1	A	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	2	B	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	3	C	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	4	D	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	5	E	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	6	F	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	7	G	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	8	H	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	9	I	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	10	J	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	11	K	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	12	L	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	13	M	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	14	N	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	15	O	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	16	P	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	17	Q	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	18	R	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	19	S	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	20	T	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	21	U	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	22	V	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	23	W	22422	X-RAY DIFFRACTION	4.87	TORSIONAL
1	24	X	22422	X-RAY DIFFRACTION	4.87	TORSIONAL

LS refinement shell

Refine-ID: X-RAY DIFFRACTION / R_factor R_free error: 0 / Total num. of bins used: 30

Resolution (Å)	Rfactor Rfree	Num. reflection Rfree	Rfactor Rwork	Num. reflection Rwork	Num. reflection all	% reflection obs (%)
2.3-2.3261	0.2595	388	0.1911	7050	7438	96
2.3261-2.3535	0.2436	362	0.1898	7102	7464	96
2.3535-2.3822	0.2212	334	0.1854	7134	7468	96
2.3822-2.4124	0.2439	358	0.1818	7163	7521	96
2.4124-2.4441	0.2508	368	0.1836	7100	7468	96
2.4441-2.4776	0.2596	348	0.1841	7110	7458	96
2.4776-2.513	0.2345	331	0.1707	7166	7497	97
2.513-2.5505	0.2334	361	0.1758	7201	7562	97
2.5505-2.5904	0.2376	365	0.1795	7128	7493	97
2.5904-2.6328	0.2346	377	0.1773	7191	7568	97
2.6328-2.6782	0.2318	375	0.185	7108	7483	97
2.6782-2.7269	0.2649	430	0.1876	7151	7581	97
2.7269-2.7794	0.2413	412	0.1907	7042	7454	97
2.7794-2.8361	0.2324	435	0.1805	7230	7665	97
2.8361-2.8978	0.2373	391	0.1816	7104	7495	97
2.8978-2.9652	0.246	404	0.1838	7194	7598	97
2.9652-3.0394	0.2482	397	0.1821	7129	7526	97
3.0394-3.1215	0.2142	382	0.181	7170	7552	97
3.1215-3.2134	0.2103	392	0.1787	7277	7669	98
3.2134-3.3171	0.2249	384	0.1877	7161	7545	98
3.3171-3.4357	0.2245	392	0.1794	7169	7561	98
3.4357-3.5732	0.2112	363	0.1669	7208	7571	98
3.5732-3.7359	0.2056	381	0.1656	7238	7619	98
3.7359-3.9328	0.1728	380	0.1441	7223	7603	98
3.9328-4.1792	0.1528	449	0.1311	7148	7597	98
4.1792-4.5019	0.1622	368	0.1257	7247	7615	98
4.5019-4.9549	0.1562	355	0.1211	7278	7633	98
4.9549-5.6717	0.1791	394	0.1344	7239	7633	98
5.6717-7.1451	0.1908	445	0.1423	7143	7588	98
7.1451-81.1962	0.1572	339	0.1344	7215	7554	97

Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°2)	L12 (°2)	L13 (°2)	L22 (°2)	L23 (°2)	L33 (°2)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å2)	T12 (Å2)	T13 (Å2)	T22 (Å2)	T23 (Å2)	T33 (Å2)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	1.3414	-1.8181	0.3694	3.2272	-0.5791	0.3932	0.0619	0.1392	0.2724	-0.1672	-0.0568	-0.4283	0.0037	0.0999	-0.0114	0.1341	-0.033	0.0378	0.1602	-0.0136	0.196	181.5366	-51.0646	203.6217
2	1.9337	-1.9457	1.5372	3.1898	-1.8049	1.88	0.0863	0.1919	0.0008	-0.0784	-0.1117	-0.0005	0.0426	0.1144	-0.0045	0.1313	-0.0088	0.0262	0.143	-0.0294	0.1846	175.119	-57.3993	201.776
3	1.5384	0.6967	-0.4516	1.3481	-0.056	2.3457	0.136	0.4407	-0.3167	-0.1189	-0.0102	0.2333	0.3761	-0.5555	0.1078	0.317	-0.0795	-0.2107	0.4782	-0.0194	0.373	152.7483	-58.011	191.9119
4	3.4315	0.8186	2.3326	0.9674	0.8967	3.1626	0.1609	0.1584	0.0246	-0.0352	0.2817	0.5678	0.0764	-1.1571	-0.286	0.1601	-0.0406	0.015	0.3454	0.0386	0.4083	154.1014	-53.1386	204.0696
5	4.2253	-0.3823	-0.0356	1.304	-0.3226	7.0985	0.1931	0.0771	0.1022	0.0394	-0.2568	0.2701	0.4878	-0.1868	0.067	0.1523	-0.0247	-0.0043	0.0773	-0.0051	0.1949	164.3557	-59.0838	205.2108
6	5.6556	0.7168	0.9141	1.5849	0.0875	5.9689	0.2221	0.306	-0.4913	-0.3214	-0.1882	0.3293	1.233	-0.5124	-0.0656	0.2863	-0.0329	-0.0658	0.173	-0.0534	0.3196	161.1005	-63.2715	202.0126
7	1.531	0.1818	1.7748	0.0272	0.2571	2.5094	0.1808	0.2405	-0.3575	0.0171	0.073	0.4799	0.6314	-0.0173	-0.185	0.265	-0.0433	-0.0467	0.1986	-0.0484	0.2314	168.1219	-60.301	202.4403
8	1.562	-0.5688	0.3123	1.3772	-0.2117	2.316	-0.0413	-0.1974	0.0695	-0.0412	-0.0704	0.29	-0.0222	-0.1094	0.0623	0.1313	-0.0208	0.0287	0.122	-0.0046	0.172	167.1739	-44.7242	212.9575
9	2.2269	0.0087	-0.5985	1.6603	-0.3238	6.2409	0.0341	0.0604	-0.0424	-0.0412	0.0736	0.5169	0.0384	-0.5321	0.0265	0.1543	-0.019	-0.0043	0.1458	-0.0205	0.2413	160.2003	-44.7306	204.4728
10	3.9028	1.9033	2.1176	6.1242	0.9217	3.3795	0.1011	0.6924	-0.1939	-0.8701	-0.1053	0.361	0.1005	-0.0951	0.0612	0.2198	-0.0163	-0.0598	0.2585	-0.03	0.1858	164.2597	-54.0702	189.9258
11	4.8096	3.692	4.3425	3.1634	2.4427	6.997	-0.1902	0.9065	-1.051	-1.0977	0.1001	-0.4772	0.7156	0.6002	0.0787	0.5459	0.0537	0.0138	0.3844	-0.0073	0.3976	174.7328	-62.139	191.5487
12	3.6164	-1.5546	0.3861	3.5995	-0.0888	2.2394	0.0392	0.0549	0.1587	-0.181	0.0579	-0.0618	-0.2729	-0.1655	-0.0926	0.1946	-0.0173	0.0427	0.1187	0.0233	0.1298	158.1017	-18.8393	201.2117
13	1.0957	-0.9401	-1.0043	1.0182	0.6254	1.0789	0.1751	0.2494	0.0334	-0.2134	-0.2123	-0.0013	-0.1214	-0.1391	0.035	0.1507	-0.0148	-0.0019	0.1216	0.0179	0.1685	150.281	-14.1778	208.3466
14	4.6287	2.1346	-0.5045	2.726	-0.8694	2.918	0.2671	-0.307	0.146	0.3898	-0.3632	-0.3345	-0.366	0.4539	0.1032	0.1112	-0.0791	-0.0191	0.231	0.012	0.2674	173.513	-16.1529	225.1504
15	3.2947	1.077	0.7179	1.9011	-0.5898	2.2444	0.101	-0.0999	0.2716	0.1584	-0.159	-0.0216	-0.0045	0.0373	0.0267	0.1148	0.0005	0.0236	0.0983	-0.0322	0.1722	159.3758	-19.0306	221.8227
16	2.4568	0.8913	0.5472	2.247	0.731	1.7766	-0.0277	0.0568	0.1539	0.0261	0.0485	-0.0548	-0.1407	0.0983	-0.02	0.1037	0.0048	0.0436	0.1139	0.0233	0.1344	161.6326	-20.6314	212.845
17	1.1306	-0.0756	0.901	1.7457	0.9464	1.7794	0.2229	-0.1997	0.4154	0.4849	-0.2752	0.3572	-0.2038	-0.0808	0.0414	0.2226	-0.0211	0.0215	0.1247	-0.0558	0.2343	164.6129	-42.7547	233.8659
18	2.7088	2.8447	0.2544	4.7188	0.6053	0.8084	0.1458	-0.1451	0.3936	0.0296	-0.1476	0.5772	-0.1367	-0.0964	0.0055	0.1278	0.0237	0.0091	0.1024	0.0005	0.1928	156.5529	-50.8757	227.0985
19	2.1135	1.4253	0.855	2.1957	0.5667	1.1257	0.1514	-0.1446	0.1215	0.1989	-0.1411	0.0896	-0.0161	-0.009	-0.0007	0.1702	0.001	0.0321	0.1233	-0.0034	0.1418	164.745	-54.8542	232.2903
20	7.5192	-0.7246	-2.2834	3.445	4.218	7.2253	-0.2675	-0.6392	-0.365	0.6999	0.1492	-0.5398	0.3105	0.8763	-0.0382	0.3351	-0.0192	-0.1521	0.2554	0.0467	0.2975	186.7639	-58.7021	242.4523
21	6.3561	0.1781	6.0388	1.3193	-0.1136	6.675	0.0979	0.2239	0.1146	0.1512	-0.0805	-0.4289	-0.3577	0.8616	-0.0314	0.1862	-0.0632	-0.0059	0.2445	0.0072	0.3242	186.2729	-55.0423	229.878
22	2.6937	0.1229	1.2226	0.4119	-1.0699	8.0213	0.3123	-0.2423	-0.1983	-0.1065	0.1104	0.0472	0.531	0.0721	-0.3623	0.1338	-0.0277	-0.0206	0.1285	0.0145	0.1883	175.0188	-58.9111	229.2155
23	3.2662	-0.5958	3.145	4.6074	0.6439	7.6745	0.3835	-0.4443	-0.985	0.2732	-0.0545	-0.2464	1.174	-0.1532	-0.3128	0.2688	-0.0025	0.0015	0.1887	0.0519	0.3265	177.3703	-63.2843	232.9312
24	2.0574	-0.4512	2.1177	0.108	-0.5237	2.4754	0.1008	0.0148	-0.4379	0.2714	-0.0575	-0.134	0.6241	-0.0478	-0.0215	0.3051	0.0011	-0.008	0.1374	0.02	0.2626	170.8399	-59.0154	232.1376
25	0.5446	-0.6583	-0.1831	1.5881	-1.3874	4.4858	-0.0726	0.0411	-0.0858	0.0343	-0.0508	-0.2576	-0.2894	0.5051	0.1494	0.1516	-0.0481	0.0066	0.1316	0.0001	0.1763	177.8496	-45.3699	223.5898
26	4.1373	0.9144	1.7569	5.9955	-0.9637	1.0644	0.203	-0.652	0.0263	0.5502	-0.1083	0.078	-0.1549	-0.0018	-0.0971	0.332	-0.0915	-0.0084	0.2087	-0.035	0.1725	176.2183	-52.3635	243.8837
27	4.0468	-1.0925	5.1112	5.1541	-0.725	6.7102	0.1187	-0.9669	-0.5863	1.0257	-0.1934	0.6056	0.2286	-0.8804	0.0682	0.5234	-0.1134	0.101	0.3273	-0.0307	0.3557	164.5265	-58.419	243.0425
28	2.9883	-0.611	-0.1356	2.3214	-0.2207	2.843	-0.205	-0.1187	-0.0628	-0.2787	0.0122	-0.2406	0.4236	0.3388	0.1954	0.1335	0.0349	0.0237	0.115	-0.0415	0.1916	184.4634	-96.0324	217.8344
29	0.4442	-0.0198	-0.3038	1.6191	-1.1853	1.3238	-0.0695	-0.0044	-0.0834	-0.1216	0.0472	-0.0167	0.1694	0.0739	0.0269	0.1696	0.0087	0.0021	0.1337	-0.0332	0.1449	182.2967	-85.4171	213.772
30	2.9054	-0.8817	1.9408	1.7826	-0.0624	5.1851	-0.1979	-0.2128	0.2439	0.1368	0.0019	-0.1747	-0.2759	0.2784	0.1608	0.1444	-0.0109	-0.0109	0.152	-0.0441	0.1748	179.9645	-80.4677	232.0502
31	3.9838	0.6674	1.0816	2.6701	0.3657	2.2265	-0.0901	-0.1849	-0.1318	-0.0972	0.0057	-0.1137	-0.0154	0.2431	0.0682	0.143	0.0441	0.0227	0.1013	-0.0078	0.1269	180.5816	-89.0541	227.3413
32	0.4115	0.2996	0.1088	1.9481	0.823	0.9317	0.0064	-0.105	-0.0177	0.3796	-0.1005	0.2265	0.3234	-0.0086	0.0368	0.28	-0.0523	0.0712	0.1688	-0.0071	0.1629	179.4726	6.4027	190.2558
33	1.521	-0.3371	0.6723	2.2426	-0.5529	3.0976	0.0118	-0.1667	-0.1732	0.3925	0.0277	-0.1053	0.5138	0.0783	0.0027	0.2991	0.0175	-0.0078	0.1472	-0.0086	0.1591	190.7403	6.0037	189.598
34	1.1181	-0.0883	-0.1206	1.5353	-0.4822	1.3292	-0.0072	0.1037	-0.1366	-0.0458	0.1233	-0.0117	0.2659	0.1109	-0.1226	0.1442	-0.0041	0.0004	0.1608	-0.0583	0.1657	215.9873	-92.1161	168.0756
35	4.7516	-0.2777	1.0125	2.8039	-0.2279	0.2399	-0.0327	0.2254	0.4552	0.008	0.0711	-0.3397	0.0442	0.413	-0.0371	0.1279	0.0116	-0.0052	0.2743	-0.0396	0.2214	224.5342	-81.6374	172.7412
36	4.0784	-0.4261	-0.8225	1.2286	0.0877	2.185	-0.0881	-0.0695	-0.2504	0.0047	0.1167	-0.1736	0.2674	0.3133	-0.0497	0.1833	0.0104	-0.0317	0.155	-0.0269	0.1677	221.7217	-90.0894	175.6593
37	2.1646	-0.8502	-1.4731	0.8349	0.3733	1.496	0.0887	0.0282	0.3293	-0.0276	0.1285	-0.1097	-0.12	-0.0642	-0.2336	0.1179	0.0069	-0.0211	0.1108	-0.002	0.1913	130.0947	2.4599	228.8493
38	6.8535	0.3077	2.0524	2.5848	-0.1833	2.7179	0.0215	0.0747	-0.3626	-0.0118	0.0835	0.117	0.2896	-0.0718	-0.0771	0.1262	-0.0043	-0.0004	0.0983	0.0071	0.1783	119.7337	-15.9037	231.6798
39	3.4551	0.3694	1.2435	1.8723	0.4272	3.6794	-0.0756	0.1214	0.074	-0.075	0.134	-0.0292	0.0532	-0.0256	-0.0416	0.0909	0.0085	0.0044	0.0875	-0.0037	0.1733	122.7674	-5.9745	232.6514
40	0.9509	-0.6504	-0.6935	1.8546	0.0803	0.6117	0.107	-0.0496	0.03	0.1617	0.0669	0.0053	0.4613	-0.2637	-0.2182	0.3135	-0.0912	-0.0625	0.2459	0.0478	0.1523	158.3181	-81.1134	138.8887
41	3.2975	-0.1036	3.2013	1.4163	0.0756	5.3963	0.0012	-0.0944	0.0221	0.0848	0.03	0.0882	0.0096	-0.6954	-0.0531	0.1829	-0.0396	0.011	0.2974	0.0185	0.1575	150.4924	-74.43	130.4428
42	3.2614	-0.6356	1.969	1.5437	-0.1123	3.5305	0.0919	0.1068	-0.018	-0.0256	0.0337	0.0722	0.094	-0.3686	-0.1589	0.1946	-0.0553	-0.0012	0.2999	0.0423	0.1599	151.5014	-76.5508	121.667
43	1.6738	0.0953	-0.7267	1.8542	-0.0728	0.3214	0.0619	0.0846	-0.0108	-0.1075	0.0737	0.047	0.6726	0.443	-0.1666	0.4098	0.0996	-0.114	0.3439	-0.0327	0.2313	171.3707	-91.212	138.1264
44	1.5935	-0.2396	-0.4628	1.3321	-0.4129	0.8936	-0.0367	0.5787	-0.277	-0.5824	0.061	-0.1287	0.7906	0.3041	-0.0612	0.6542	0.1534	-0.1011	0.4809	-0.0985	0.2754	178.0223	-94.5061	122.9512
45	3.9593	-3.7009	0.9667	7.3649	-2.5162	3.2944	-0.1118	0.1624	0.117	-0.0661	0.1784	-0.6637	0.4004	0.4893	-0.0821	0.2577	0.0456	-0.0703	0.4093	-0.073	0.248	179.5295	-81.9744	125.136
46	2.6309	-0.202	0.0032	3.3861	-1.7464	0.9621	0.2201	-0.0537	-0.1045	-0.6421	0.1568	0.237	0.2958	0.2815	-0.3138	0.3345	-0.0881	-0.1046	0.3006	0.0075	0.2011	168.2241	-79.6913	121.7045
47	4.8273	-3.2131	-0.8289	4.6143	-1.6841	2.802	0.5567	0.8346	-0.4595	-1.5019	-0.3413	0.8349	0.6001	-0.2922	-0.1449	0.404	-0.0086	-0.1488	0.4755	0.0162	0.2717	169.4628	-84.5182	117.7764
48	1.4934	-1.0212	-0.5211	2.911	1.1336	1.6385	0.0834	0.323	0.0292	-0.1719	0.1131	-0.0629	0.3057	0.1083	-0.1517	0.268	-0.0594	-0.0837	0.2368	0.0535	0.1498	166.86	-75.5903	128.1252
49	1.2851	-0.3314	-0.7914	3.4788	0.784	1.1649	-0.0915	-0.1195	-0.0584	0.3066	0.2272	-0.4217	0.3808	0.4757	-0.3008	0.2626	0.0243	-0.1152	0.3344	-0.093	0.2351	175.7743	-78.374	134.3523
50	2.1634	-1.2279	-0.2386	3.1031	4.1563	6.7479	0.187	0.1774	-0.5107	-0.0298	-0.0809	0.1367	0.8141	-0.1708	-0.0773	0.553	0.0165	-0.1173	0.2455	-0.0482	0.2573	167.8643	-93.7276	130.1379
51	9.256	-4.588	0.7986	9.9207	2.087	9.0142	0.0624	0.301	-0.6201	0.1021	0.1972	0.8293	0.9218	-0.6007	-0.2262	0.6671	-0.112	-0.0075	0.4686	0.026	0.4014	155.8844	-91.9534	124.6623
52	0.9657	0.0764	-0.0859	1.9105	0.3154	1.1791	0.0017	-0.0693	-0.2372	0.0064	0.1097	-0.0786	0.4469	-0.2005	-0.0827	0.1567	-0.052	0.0047	0.1799	0.0517	0.249	141.7889	-41.1164	224.2705
53	4.2246	1.3086	0.3709	0.8135	0.2701	0.1149	0.0428	-0.1118	0.1835	-0.066	0.2186	0.2938	-0.0075	-0.761	-0.0992	0.1283	-0.0402	-0.0267	0.4192	0.1241	0.3349	127.3327	-30.3745	217.7219
54	3.2933	0.8999	-1.5203	1.1116	-0.3258	1.0653	-0.0952	0.0654	-0.2743	-0.1187	0.1192	0.1637	0.3952	-0.5076	0.0034	0.2076	-0.0947	-0.0187	0.3048	0.0347	0.2701	133.4077	-38.5628	216.2476
55	0.5499	-0.6029	-0.0428	2.0681	-0.2197	0.9123	0.0194	0.1228	0.052	-0.1517	-0.1263	-0.0924	0.0029	0.0309	0.1119	0.1824	-0.0256	-0.0031	0.1454	-0.0149	0.1101	189.8886	9.0258	159.4772
56	3.0678	0.7614	1.5933	1.6419	0.1353	3.8371	0.1441	0.0751	-0.3282	-0.0656	-0.0416	0.3428	0.3532	-0.0888	-0.0113	0.2313	-0.0099	-0.0012	0.1231	-0.054	0.2313	177.4254	2.0219	160.8261
57	1.4535	0.048	0.6714	2.0523	0.9895	3.6013	0.0224	0.1633	-0.131	-0.4165	-0.18	0.222	-0.0672	0.0704	0.1471	0.2419	0.011	-0.0325	0.108	0.0007	0.1476	181.1949	10.638	158.364
58	1.908	0.5803	-1.2678	1.0337	-0.228	1.1446	0.3095	0.0347	0.555	0.0717	0.0852	0.2779	-0.3167	-0.0377	-0.3486	0.2211	0.0127	0.0864	0.1444	0.0406	0.3538	224.6459	-49.6318	163.0125
59	6.9434	-0.4043	2.2338	2.8673	0.5577	2.8518	0.0749	-0.2733	-0.3209	0.1214	0.1793	-0.0567	0.2782	0.015	-0.2073	0.1282	-0.0033	0.0071	0.1268	0.0274	0.17	234.8157	-68.0761	160.282
60	2.8374	-0.5417	1.4562	0.9625	0.4415	3.5013	0.0463	0.0589	0.0845	0.0103	0.0805	0.0563	-0.0563	-0.0198	-0.1117	0.106	-0.0291	0.0205	0.0897	0.0342	0.2338	231.72	-58.9781	156.2557
61	8.3509	-7.1576	4.7566	7.2971	-4.8847	6.3112	-0.2586	-0.9316	1.0688	1.0734	0.1751	0.0105	-0.7481	-0.2358	0.1029	0.338	-0.0344	0.1275	0.2849	-0.0935	0.4867	232.8595	-53.8596	173.9125
62	0.7536	0.8858	-0.2073	1.3724	0.3751	1.2113	-0.2119	-0.0131	-0.1275	-0.1903	0.14	-0.0832	0.3066	0.2598	0.0586	0.3516	0.0794	0.0121	0.227	0.0144	0.126	133.2075	-137.6113	90.6689
63	1.86	0.3245	2.4879	1.2599	-0.4825	4.18	-0.1671	-0.0179	-0.1591	-0.0989	0.1305	-0.1496	0.2966	0.6603	0.004	0.3083	0.1385	0.0241	0.359	0.0123	0.181	141.2152	-131.1193	99.1407
64	3.4528	0.2804	1.8293	1.3211	-0.5805	1.9046	-0.0649	-0.1983	-0.2274	0.0917	0.0425	-0.1649	0.2625	0.5344	-0.0739	0.3244	0.1703	0.0197	0.451	0.0191	0.1793	140.2375	-133.2561	107.9005
65	0.9215	1.16	-0.3983	1.7682	-0.5686	0.1884	0.0091	-0.1635	-0.1193	0.0345	0.0701	0.1637	0.9387	-0.2655	0.003	0.534	-0.0687	-0.0222	0.2411	0.0457	0.2379	120.026	-147.5374	91.4207
66	1.9942	0.557	-0.5364	1.2473	-0.5451	1.451	0.1014	-0.4307	-0.2712	0.3566	0.0245	0.406	0.7435	-0.1986	-0.0557	0.8272	-0.1665	0.1327	0.389	0.0889	0.3432	113.4298	-150.911	106.4359
67	6.0595	5.6031	0.6875	8.1183	1.4993	2.5748	0.0438	-0.1293	0.0441	0.3814	-0.0136	0.5974	0.6715	-0.473	-0.0478	0.3859	-0.0585	0.0158	0.3765	0.0581	0.277	112.2599	-137.8791	104.6816
68	4.5742	1.2755	-0.598	1.8229	0.2597	1.7502	0.0866	-0.3574	-0.3125	0.7392	0.0416	0.0701	0.4522	-0.1472	-0.0798	0.4178	0.0559	-0.0063	0.2892	0.0275	0.1446	123.7219	-136.5944	107.9702
69	4.3081	2.8104	-0.66	3.0918	0.1003	0.4071	0.2799	-0.6301	-0.3204	0.6349	-0.244	-0.1944	0.6041	0.0155	0.0561	0.563	0.0867	-0.0376	0.3284	0.0506	0.2087	125.6897	-139.7416	109.1363
70	1.5623	0.1638	-0.3691	1.9091	-0.7881	1.7502	0.032	-0.0495	-0.1631	-0.0192	0.0347	0.213	0.4774	-0.2662	-0.0771	0.37	0.0217	-0.0753	0.2209	0.0388	0.1517	120.5999	-136.0809	96.7969
71	8.0231	4.8962	-1.6072	4.0384	-2.975	5.0715	-0.626	-0.548	-0.6698	0.2544	0.3516	-0.5815	0.8365	0.3812	0.2906	1.1421	0.2852	0.0391	0.5365	0.008	0.4428	136.1522	-148.2436	103.938
72	1.839	0.6595	-0.7794	1.0144	-0.3465	1.2359	0.1186	-0.2604	0.254	0.0811	-0.0516	-0.0486	-0.0933	0.1707	-0.0404	0.1382	-0.0125	0.008	0.1159	-0.0408	0.1562	202.7036	-67.3957	184.9539
73	4.0942	-1.4818	0.4562	1.451	0.388	1.7477	0.1282	0.3364	0.3161	-0.1915	-0.1935	0.0058	-0.0572	-0.0939	0.0685	0.1435	-0.011	-0.0038	0.1266	0.0348	0.1581	192.3625	-70.6298	169.2595
74	2.6939	-2.0564	0.1295	4.0061	-0.6437	2.307	-0.0169	0.1843	-0.1379	-0.0653	0.0837	0.1689	0.1826	0.1634	-0.0557	0.1239	-0.0244	-0.0022	0.1174	-0.0158	0.0881	196.3055	-83.5108	178.8251
75	5.5344	-0.8212	0.4913	6.1548	-1.2256	4.257	0.0947	-0.2608	0.7813	0.1931	-0.2225	-0.0796	-0.5286	0.1025	0.0787	0.1866	0.0168	-0.0024	0.1789	-0.02	0.1817	189.5584	-61.0366	178.9038
76	0.14	-0.0857	0.0536	1.4504	-0.87	2.3705	0.0013	-0.0083	0.0821	0.1282	0.1073	0.1009	-0.1757	-0.3385	-0.1379	0.198	0.0982	-0.0028	0.244	-0.0213	0.1827	120.195	-108.7865	107.7909
77	1.8192	0.8556	0.5358	2.8402	-0.0666	2.1665	0.0457	-0.2448	0.1583	0.3606	-0.0092	-0.0848	-0.122	0.1718	-0.0352	0.2314	0.0881	-0.0244	0.2903	-0.0209	0.1805	131.6156	-108.2359	107.3741
78	1.327	0.5622	0.2651	2.1218	0.8684	1.4953	0.0674	0.0612	-0.1763	0.0862	-0.1245	0.1154	0.116	-0.1905	0.0518	0.1117	-0.0051	0.0035	0.1415	-0.0105	0.1637	150.9411	-84.1228	222.1162
79	3.0746	0.333	1.4677	1.3922	-0.4763	3.5917	-0.0878	0.4877	0.1046	-0.2742	0.019	0.1096	-0.3189	-0.0897	0.0499	0.2397	0.0159	-0.0515	0.2301	-0.0225	0.1651	155.0775	-78.8468	204.2755
80	2.9249	-0.3547	1.0917	1.3897	-0.714	1.9253	0.0837	0.2612	-0.172	-0.1528	-0.1208	0.2744	-0.1098	-0.1757	0.0383	0.212	-0.0125	-0.0388	0.1906	-0.0775	0.1956	152.3842	-86.6053	209.8328
81	0.3988	0.4609	0.1366	1.1999	0.1376	0.4438	-0.1403	-0.089	-0.1599	0.2062	-0.0846	0.2716	0.3323	-0.1452	0.1543	0.4636	-0.1034	0.1816	0.1663	0.0133	0.346	172.2654	-26.958	177.4593
82	4.3563	0.2462	1.8894	0.493	-0.5359	5.2788	-0.2838	0.5144	0.0373	-0.1992	0.1538	0.1648	0.1284	-0.1241	0.1636	0.3133	-0.0794	0.0428	0.1583	0.0176	0.2602	175.6115	-21.0141	156.5412
83	4.0962	1.5959	2.4819	1.1377	-0.0524	6.5196	-0.3858	-0.0746	0.3498	0.0697	-0.0127	0.2636	-0.5046	-0.2282	0.3405	0.3173	-0.0318	0.0276	0.1122	-0.0214	0.3628	174.0262	-17.5097	165.6557
84	4.0085	-0.7176	1.8216	2.5894	-0.6287	1.6529	-0.2012	-0.0444	-0.4043	0.0235	0.0584	0.1577	0.1966	-0.1703	0.1382	0.3751	-0.0821	0.1467	0.1814	-0.018	0.2775	174.0961	-28.1526	165.0796
85	0.6293	-0.3148	0.4213	3.2306	-1.5406	2.7653	-0.1298	0.4845	0.1253	-0.5283	-0.0143	0.1223	0.1158	-0.1936	0.1144	0.1969	-0.0442	-0.0464	0.5154	0.0977	0.2439	212.9999	-70.9645	141.1895
86	0.435	-0.3676	0.2772	0.7065	0.1257	0.5983	0.0631	0.1616	0.4192	-0.2199	-0.0103	0.9908	-0.0168	-0.5606	-0.0034	0.238	0.0531	-0.0965	0.6119	0.1985	0.7963	199.7946	-58.5823	146.6011
87	0.0982	0.0616	-0.0652	0.5649	-0.3852	0.2739	0.0694	-0.186	-0.1428	0.1919	-0.127	-0.2238	0.0429	0.7205	-0.0051	0.3268	0.0818	-0.0279	1.2379	0.1768	0.3591	152.5733	-127.967	140.6489
88	0.1074	0.0103	0.079	0.0707	-0.0576	0.1587	0.2471	-0.0643	-0.2094	-0.1564	-0.2273	-0.1153	0.4551	0.5131	-0.0637	0.4295	0.769	-0.124	0.9116	0.3365	0.1628	147.747	-136.1623	131.218
89	1.2457	-0.5301	-0.2468	1.6409	0.7427	2.2552	-0.072	-0.4829	-0.2154	-0.0819	0.091	0.0673	0.252	0.669	0.1526	0.3328	0.4417	0.054	0.7552	0.2401	0.3091	145.2435	-132.2195	123.4441
90	2.5128	-0.5568	0.3539	0.6902	0.2508	0.2411	0.1746	0.0159	0.8613	0.2318	-0.5247	-0.6034	-0.703	1.2627	0.3868	0.5936	-0.3491	-0.1002	1.0388	0.1694	0.6449	153.4731	-111.5751	143.4213
91	0.6699	1.2098	-0.3402	2.4401	-0.2866	0.5934	0.1194	0.3521	1.0691	-0.1614	-0.0838	-0.0374	-0.6317	0.8386	-0.0569	0.7628	-0.4511	-0.0945	0.9215	0.3679	0.9111	146.7235	-101.322	132.0393
92	1.4697	1.268	2.6146	3.6808	0.9127	5.3576	-0.2179	0.1827	1.0603	0.2114	-0.1769	-0.2866	-1.2163	0.9152	0.3672	0.5411	-0.152	0.0104	0.5709	0.0925	0.5115	136.8498	-108.8138	136.9782
93	0.7015	-0.6176	-0.9212	1.8937	1.0762	1.5666	-0.2521	0.4995	0.4932	-0.5823	0.0558	-0.4184	-0.2411	0.7328	0.1819	0.4141	0.0185	0.0479	0.6944	0.2329	0.3744	139.9662	-117.5559	129.6115
94	2.1504	0.3467	-0.647	2.3027	1.5243	1.3973	-0.0891	0.5646	0.3177	-0.5744	0.129	-0.3484	-0.3201	0.6205	-0.1376	0.357	-0.0002	0.0997	0.9762	0.2497	0.3962	142.8404	-116.8532	127.0564
95	4.5556	0.5638	0.0095	2.5118	-0.2464	4.4716	0.2703	-0.0559	0.4971	0.3043	-0.3524	-0.0001	-0.1942	0.862	0.0588	0.3049	-0.0282	0.0577	0.4978	0.0743	0.2407	137.4804	-121.0985	143.8883
96	3.8276	1.8097	-0.476	3.5931	-1.6405	0.9627	-0.1977	0.5046	0.0038	-0.4774	0.0306	-0.5161	0.123	-0.0235	0.1074	0.4935	-0.2372	0.0695	1.2828	0.2951	0.6249	154.2394	-111.2803	133.1442
97	0.4754	-0.8368	0.6503	3.0813	-1.3212	0.9074	-0.1548	-0.3544	-0.6915	0.0292	-0.3237	-0.5792	0.3162	0.3283	0.4061	0.3804	0.1125	0.0955	0.3175	0.1739	0.6455	207.5764	-30.7946	173.1974
98	1.3336	0.3196	-0.051	5.3392	-2.4701	2.0226	-0.1177	0.0297	-0.4974	-0.2926	-0.1511	-0.2348	0.3664	0.2143	0.2361	0.308	0.034	0.0996	0.2034	0.0369	0.3243	202.1815	-22.8058	164.0251
99	1.8857	-0.1049	0.0093	4.7896	-2.3733	2.5084	-0.1196	-0.1763	-0.1643	0.3119	-0.0607	-0.2403	0.0713	0.1379	0.1932	0.2325	-0.0081	0.0355	0.1692	0.0212	0.164	200.5965	-14.2462	166.8236
100	2.7258	0.3706	0.0394	2.1216	1.1787	2.6998	-0.261	-0.6291	-0.0477	0.6732	-0.2773	-0.5935	-0.8336	0.3465	0.4082	0.8041	-0.0568	-0.182	0.605	0.2347	0.4059	208.3048	-23.6478	193.7375
101	2.0754	0.9398	2.2651	0.4278	0.9339	4.9591	-0.0578	-1.1692	-0.348	1.1128	-0.098	-0.2533	-0.1165	-0.0138	0.1202	0.822	0.0873	-0.0431	0.6918	0.1586	0.33	194.9729	-22.6345	193.2257
102	6.4846	0.5619	1.4572	1.7125	0.6916	4.5876	-0.4724	-0.8504	0.3117	0.6202	-0.0691	-0.1008	-0.6501	0.3403	0.4552	0.5745	0.0055	-0.0454	0.413	0.1053	0.2528	197.0163	-17.3766	182.82
103	5.5914	0.3608	1.4101	2.329	1.0327	5.7283	-0.3835	-0.653	0.2126	0.5405	-0.0065	-0.128	-0.8365	0.2729	0.3671	0.5807	-0.011	-0.074	0.3267	0.0631	0.2844	199.9888	-14.964	182.5341
104	1.1716	-0.2083	0.5829	0.9679	-0.0519	1.7153	-0.1077	-0.5316	-0.4257	0.5538	-0.1558	-0.2639	-0.0007	0.1147	0.2233	0.4551	0.0393	0.053	0.3416	0.1752	0.4015	193.487	-31.8437	182.5084
105	1.3087	-0.1676	1.4539	2.0909	0.4219	2.2669	-0.2392	-0.3752	-0.0577	0.4916	-0.1796	-0.5486	-0.5491	0.8443	0.4103	0.6715	-0.0712	-0.2093	0.7004	0.2925	0.5692	211.6	-21.4273	188.0444
106	5.3407	0.9519	1.4515	3.8325	3.7407	5.3307	0.0062	-0.1321	0.4766	-0.0384	-0.3149	-0.7074	-0.7969	0.2668	0.2638	0.7467	0.0381	-0.2246	0.4972	0.1448	0.5321	212.6933	-13.5958	177.9817
107	1.3833	0.0673	0.2801	0.7489	0.2654	1.5473	-0.3743	-0.5176	-0.0607	0.5561	0.2612	-0.6907	0.1828	-0.0006	-0.1099	0.1682	0.2163	-0.2576	0.3822	-0.075	0.301	147.0414	-15.5303	250.0697
108	1.4056	0.38	0.1048	0.1549	0.1588	0.6588	-0.1082	-0.1341	0.2581	0.3128	0.2502	-0.8552	0.1118	0.2991	-0.0646	0.2195	0.0861	-0.1693	0.3654	-0.1494	0.5464	152.8104	-7.6442	243.8849
109	1.3241	-0.2297	0.6647	0.4593	0.4245	2.3109	0.1342	-0.0165	0.1298	-0.0741	-0.043	0.1569	-0.1193	-0.8102	-0.0998	0.2011	0.0552	0.0128	0.4956	-0.0007	0.2402	143.387	-69.5671	97.0474
110	3.0643	-3.5685	-0.1902	7.9924	0.9725	0.9641	0.0344	-0.1375	0.9863	-0.3549	-0.1637	-0.22	-0.8796	-0.3057	0.0489	0.561	0.1417	0.0324	0.3527	-0.0467	0.385	155.0286	-51.452	92.722
111	2.8809	-0.474	-1.3847	3.4744	0.6873	0.7432	-0.0147	-0.6968	0.3884	0.6223	0.0777	0.3029	-0.4208	-0.5439	-0.0402	0.374	0.1384	0.0567	0.5685	-0.0611	0.2511	150.3699	-60.2832	101.6718
112	2.7445	-1.4282	-1.1922	3.0203	1.0721	0.6281	0.0923	-0.123	0.3657	-0.2521	-0.0438	0.1693	-0.627	-0.6385	-0.0784	0.3725	0.213	0.0254	0.4591	0.0081	0.2679	149.3683	-61.0004	88.8786
113	2.4292	-0.2549	0.4021	2.7629	-0.0372	0.4064	0.2621	0.0521	0.0347	-0.164	-0.0047	0.5919	-0.0608	-0.5246	-0.181	0.7904	0.2284	-0.0891	1.4008	0.0065	0.8471	136.0554	-62.7328	105.1616
114	0.3871	0.5053	0.1626	0.6641	0.278	2.2681	0.273	0.0368	0.2032	-0.1342	0.2159	-0.2321	-0.6751	0.5387	-0.382	0.3241	-0.1471	0.1192	0.3794	0.0097	0.3317	174.9221	-53.9584	122.6714
115	1.1479	-1.2039	0.9881	4.0138	-1.0628	0.8493	0.0651	0.2729	0.385	-0.2929	0.2698	0.5281	-0.5787	-0.7736	-0.2862	0.5433	0.2906	0.1292	0.7093	0.2839	0.4378	150.212	-46.2902	121.2954
116	2.2256	0.4036	0.7516	3.7659	-0.9049	2.1749	0.2843	0.5401	0.2646	-0.6711	0.0527	0.2423	-0.4233	-0.4367	-0.2516	0.4484	0.0436	0.0724	0.4681	0.1434	0.2669	160.8528	-53.8534	116.7113
117	1.5295	-0.1913	0.8333	0.7797	-0.1755	2.1544	0.1705	0.1785	0.3829	-0.1294	0.1608	0.0585	-0.6162	-0.4539	-0.3349	0.3706	0.0301	0.1014	0.2974	0.1155	0.3105	160.9316	-51.5781	129.4194
118	8.2446	2.0781	-0.4193	8.6561	1.1859	0.2337	0.2751	0.4092	0.8458	-0.1204	0.2966	0.0999	-0.8883	0.1304	-0.5544	1.1742	-0.0157	0.1168	0.4521	0.0365	0.4298	170.9954	-43.6894	112.8307
119	0.7252	0.1834	-0.1425	1.6509	1.1543	2.1236	0.0785	-0.0101	0.0995	-0.1731	0.1934	-0.1477	-0.4812	0.4891	-0.2537	0.268	-0.0752	0.0816	0.2721	-0.0085	0.2145	174.919	-68.4143	91.8847
120	2.969	-1.8041	0.7277	2.9029	-0.4326	2.8741	0.2436	-0.3046	-0.313	0.0941	0.0316	-0.1398	0.4385	0.1297	-0.2277	0.2858	-0.0138	-0.0341	0.2103	0.0254	0.2172	171.0897	-86.3047	96.2787
121	1.1044	0.0071	0.0584	1.0688	-1.4372	4.0381	0.0173	-0.1441	0.0041	0.348	0.0902	0.166	-0.2386	-0.3305	-0.074	0.3293	0.011	0.0586	0.247	-0.0329	0.1671	117.1272	-126.2523	142.0917
122	1.713	-0.1387	0.3046	3.7752	-2.804	5.7727	0.0747	0.0484	0.1509	0.1152	-0.0883	0.1734	0.0709	-0.3327	-0.0177	0.2514	0.032	0.031	0.259	0.0027	0.1613	117.2102	-122.5755	130.3524
123	0.1587	0.0984	0.1512	0.0579	0.0862	0.1445	0.1155	0.1374	-0.4044	-0.0864	0.051	0.0086	0.6992	-0.1409	0.1317	1.3233	-0.2233	-0.0402	0.1667	-0.0699	0.399	116.1005	-151.8886	135.0784
124	3.8233	2.0073	1.1467	4.0624	1.845	0.8716	0.1683	0.3484	-0.8371	-0.2827	-0.0262	-0.3648	1.234	0.3876	-0.0773	0.99	0.3003	-0.0264	0.5177	-0.0275	0.3575	128.4535	-148.5101	130.7279
125	4.1283	1.0365	-1.0523	3.7195	-0.4315	0.3935	-0.0112	0.797	-0.1912	-0.438	0.0788	0.1115	0.749	0.2061	-0.0434	0.7095	0.1576	0.0169	0.3831	0.0044	0.2013	123.3647	-137.9475	128.5403
126	3.4347	0.4944	-0.8297	5.6895	1.0139	3.4103	-0.0675	1.0628	-0.4229	-0.9782	0.1392	0.4316	1.0862	-0.2298	-0.0342	0.8459	0.0432	-0.0716	0.5262	-0.0642	0.329	120.945	-141.0367	123.9255
127	2.4325	0.7821	-0.3771	2.4857	0.7921	0.4334	-0.0477	0.8639	-0.02	-0.7077	0.107	0.4175	0.9303	0.044	-0.0213	0.6849	-0.0444	-0.0889	0.4105	0.0212	0.2378	119.1612	-135.8355	129.0148
128	1.756	-0.113	-0.0019	0.8585	0.2478	1.5326	0.2279	0.0607	-0.2366	-0.293	-0.2451	-0.185	1.1005	0.5076	-0.019	0.6344	0.1676	-0.0036	0.3519	0.0435	0.1832	130.8899	-139.7238	141.4454
129	1.543	0.1874	0.185	2.3551	1.1215	3.9769	0.0215	0.4526	-0.4577	-0.2286	0.0215	0.4734	0.6184	-0.4851	0.1605	0.925	-0.2558	-0.0595	0.3803	-0.1163	0.3333	111.5999	-146.6295	135.0027
130	8.642	2.0288	2.978	7.0066	-1.3862	3.3661	0.3234	0.4579	0.3004	-0.2726	0.2334	0.8138	0.6446	-0.7174	-0.4868	0.7477	-0.1563	0.1158	0.7034	0.0692	0.5727	106.4926	-134.9114	131.0643

Refinement TLS group

ID	Refine-ID	Refine TLS-ID	Selection details	Auth asym-ID	Auth seq-ID
1	X-RAY DIFFRACTION	1	chain 'A' and (resid 2 through 54 )	A	2 - 54
2	X-RAY DIFFRACTION	2	chain 'A' and (resid 55 through 98 )	A	55 - 98
3	X-RAY DIFFRACTION	3	chain 'A' and (resid 99 through 111 )	A	99 - 111
4	X-RAY DIFFRACTION	4	chain 'A' and (resid 112 through 125 )	A	112 - 125
5	X-RAY DIFFRACTION	5	chain 'A' and (resid 126 through 137 )	A	126 - 137
6	X-RAY DIFFRACTION	6	chain 'A' and (resid 138 through 147 )	A	138 - 147
7	X-RAY DIFFRACTION	7	chain 'A' and (resid 148 through 163 )	A	148 - 163
8	X-RAY DIFFRACTION	8	chain 'A' and (resid 164 through 176 )	A	164 - 176
9	X-RAY DIFFRACTION	9	chain 'A' and (resid 177 through 187 )	A	177 - 187
10	X-RAY DIFFRACTION	10	chain 'A' and (resid 188 through 198 )	A	188 - 198
11	X-RAY DIFFRACTION	11	chain 'A' and (resid 199 through 209 )	A	199 - 209
12	X-RAY DIFFRACTION	12	chain 'B' and (resid 2 through 23 )	B	2 - 23
13	X-RAY DIFFRACTION	13	chain 'B' and (resid 24 through 98 )	B	24 - 98
14	X-RAY DIFFRACTION	14	chain 'B' and (resid 99 through 111 )	B	99 - 111
15	X-RAY DIFFRACTION	15	chain 'B' and (resid 112 through 163 )	B	112 - 163
16	X-RAY DIFFRACTION	16	chain 'B' and (resid 164 through 209 )	B	164 - 209
17	X-RAY DIFFRACTION	17	chain 'C' and (resid 2 through 23 )	C	2 - 23
18	X-RAY DIFFRACTION	18	chain 'C' and (resid 24 through 54 )	C	24 - 54
19	X-RAY DIFFRACTION	19	chain 'C' and (resid 55 through 98 )	C	55 - 98
20	X-RAY DIFFRACTION	20	chain 'C' and (resid 99 through 111 )	C	99 - 111
21	X-RAY DIFFRACTION	21	chain 'C' and (resid 112 through 125 )	C	112 - 125
22	X-RAY DIFFRACTION	22	chain 'C' and (resid 126 through 137 )	C	126 - 137
23	X-RAY DIFFRACTION	23	chain 'C' and (resid 138 through 147 )	C	138 - 147
24	X-RAY DIFFRACTION	24	chain 'C' and (resid 148 through 163 )	C	148 - 163
25	X-RAY DIFFRACTION	25	chain 'C' and (resid 164 through 187 )	C	164 - 187
26	X-RAY DIFFRACTION	26	chain 'C' and (resid 188 through 198 )	C	188 - 198
27	X-RAY DIFFRACTION	27	chain 'C' and (resid 199 through 209 )	C	199 - 209
28	X-RAY DIFFRACTION	28	chain 'D' and (resid 2 through 23 )	D	2 - 23
29	X-RAY DIFFRACTION	29	chain 'D' and (resid 24 through 98 )	D	24 - 98
30	X-RAY DIFFRACTION	30	chain 'D' and (resid 99 through 163 )	D	99 - 163
31	X-RAY DIFFRACTION	31	chain 'D' and (resid 164 through 208 )	D	164 - 208
32	X-RAY DIFFRACTION	32	chain 'E' and (resid 2 through 111 )	E	2 - 111
33	X-RAY DIFFRACTION	33	chain 'E' and (resid 112 through 209 )	E	112 - 209
34	X-RAY DIFFRACTION	34	chain 'F' and (resid 2 through 111 )	F	2 - 111
35	X-RAY DIFFRACTION	35	chain 'F' and (resid 112 through 163 )	F	112 - 163
36	X-RAY DIFFRACTION	36	chain 'F' and (resid 164 through 209 )	F	164 - 209
37	X-RAY DIFFRACTION	37	chain 'G' and (resid 2 through 98 )	G	2 - 98
38	X-RAY DIFFRACTION	38	chain 'G' and (resid 99 through 147 )	G	99 - 147
39	X-RAY DIFFRACTION	39	chain 'G' and (resid 148 through 209 )	G	148 - 209
40	X-RAY DIFFRACTION	40	chain 'H' and (resid 2 through 23 )	H	2 - 23
41	X-RAY DIFFRACTION	41	chain 'H' and (resid 24 through 54 )	H	24 - 54
42	X-RAY DIFFRACTION	42	chain 'H' and (resid 55 through 83 )	H	55 - 83
43	X-RAY DIFFRACTION	43	chain 'H' and (resid 84 through 98 )	H	84 - 98
44	X-RAY DIFFRACTION	44	chain 'H' and (resid 99 through 111 )	H	99 - 111
45	X-RAY DIFFRACTION	45	chain 'H' and (resid 112 through 124 )	H	112 - 124
46	X-RAY DIFFRACTION	46	chain 'H' and (resid 125 through 137 )	H	125 - 137
47	X-RAY DIFFRACTION	47	chain 'H' and (resid 138 through 147 )	H	138 - 147
48	X-RAY DIFFRACTION	48	chain 'H' and (resid 148 through 176 )	H	148 - 176
49	X-RAY DIFFRACTION	49	chain 'H' and (resid 177 through 187 )	H	177 - 187
50	X-RAY DIFFRACTION	50	chain 'H' and (resid 188 through 198 )	H	188 - 198
51	X-RAY DIFFRACTION	51	chain 'H' and (resid 199 through 209 )	H	199 - 209
52	X-RAY DIFFRACTION	52	chain 'I' and (resid 2 through 98 )	I	2 - 98
53	X-RAY DIFFRACTION	53	chain 'I' and (resid 99 through 163 )	I	99 - 163
54	X-RAY DIFFRACTION	54	chain 'I' and (resid 164 through 212 )	I	164 - 212
55	X-RAY DIFFRACTION	55	chain 'J' and (resid 2 through 111 )	J	2 - 111
56	X-RAY DIFFRACTION	56	chain 'J' and (resid 112 through 163 )	J	112 - 163
57	X-RAY DIFFRACTION	57	chain 'J' and (resid 164 through 212 )	J	164 - 212
58	X-RAY DIFFRACTION	58	chain 'K' and (resid 2 through 98 )	K	2 - 98
59	X-RAY DIFFRACTION	59	chain 'K' and (resid 99 through 147 )	K	99 - 147
60	X-RAY DIFFRACTION	60	chain 'K' and (resid 148 through 198 )	K	148 - 198
61	X-RAY DIFFRACTION	61	chain 'K' and (resid 199 through 209 )	K	199 - 209
62	X-RAY DIFFRACTION	62	chain 'L' and (resid 2 through 23 )	L	2 - 23
63	X-RAY DIFFRACTION	63	chain 'L' and (resid 24 through 54 )	L	24 - 54
64	X-RAY DIFFRACTION	64	chain 'L' and (resid 55 through 83 )	L	55 - 83
65	X-RAY DIFFRACTION	65	chain 'L' and (resid 84 through 98 )	L	84 - 98
66	X-RAY DIFFRACTION	66	chain 'L' and (resid 99 through 111 )	L	99 - 111
67	X-RAY DIFFRACTION	67	chain 'L' and (resid 112 through 125 )	L	112 - 125
68	X-RAY DIFFRACTION	68	chain 'L' and (resid 126 through 137 )	L	126 - 137
69	X-RAY DIFFRACTION	69	chain 'L' and (resid 138 through 163 )	L	138 - 163
70	X-RAY DIFFRACTION	70	chain 'L' and (resid 164 through 198 )	L	164 - 198
71	X-RAY DIFFRACTION	71	chain 'L' and (resid 199 through 211 )	L	199 - 211
72	X-RAY DIFFRACTION	72	chain 'M' and (resid 2 through 98 )	M	2 - 98
73	X-RAY DIFFRACTION	73	chain 'M' and (resid 99 through 163 )	M	99 - 163
74	X-RAY DIFFRACTION	74	chain 'M' and (resid 164 through 187 )	M	164 - 187
75	X-RAY DIFFRACTION	75	chain 'M' and (resid 188 through 209 )	M	188 - 209
76	X-RAY DIFFRACTION	76	chain 'N' and (resid 2 through 111 )	N	2 - 111
77	X-RAY DIFFRACTION	77	chain 'N' and (resid 112 through 208 )	N	112 - 208
78	X-RAY DIFFRACTION	78	chain 'O' and (resid 2 through 98 )	O	2 - 98
79	X-RAY DIFFRACTION	79	chain 'O' and (resid 99 through 163 )	O	99 - 163
80	X-RAY DIFFRACTION	80	chain 'O' and (resid 164 through 209 )	O	164 - 209
81	X-RAY DIFFRACTION	81	chain 'P' and (resid 2 through 98 )	P	2 - 98
82	X-RAY DIFFRACTION	82	chain 'P' and (resid 99 through 137 )	P	99 - 137
83	X-RAY DIFFRACTION	83	chain 'P' and (resid 138 through 163 )	P	138 - 163
84	X-RAY DIFFRACTION	84	chain 'P' and (resid 164 through 209 )	P	164 - 209
85	X-RAY DIFFRACTION	85	chain 'Q' and (resid 3 through 83 )	Q	3 - 83
86	X-RAY DIFFRACTION	86	chain 'Q' and (resid 84 through 208 )	Q	84 - 208
87	X-RAY DIFFRACTION	87	chain 'R' and (resid 2 through 23 )	R	2 - 23
88	X-RAY DIFFRACTION	88	chain 'R' and (resid 24 through 54 )	R	24 - 54
89	X-RAY DIFFRACTION	89	chain 'R' and (resid 55 through 83 )	R	55 - 83
90	X-RAY DIFFRACTION	90	chain 'R' and (resid 84 through 98 )	R	84 - 98
91	X-RAY DIFFRACTION	91	chain 'R' and (resid 99 through 111 )	R	99 - 111
92	X-RAY DIFFRACTION	92	chain 'R' and (resid 112 through 125 )	R	112 - 125
93	X-RAY DIFFRACTION	93	chain 'R' and (resid 126 through 137 )	R	126 - 137
94	X-RAY DIFFRACTION	94	chain 'R' and (resid 138 through 163 )	R	138 - 163
95	X-RAY DIFFRACTION	95	chain 'R' and (resid 164 through 187 )	R	164 - 187
96	X-RAY DIFFRACTION	96	chain 'R' and (resid 188 through 200 )	R	188 - 200
97	X-RAY DIFFRACTION	97	chain 'S' and (resid 2 through 23 )	S	2 - 23
98	X-RAY DIFFRACTION	98	chain 'S' and (resid 24 through 54 )	S	24 - 54
99	X-RAY DIFFRACTION	99	chain 'S' and (resid 55 through 83 )	S	55 - 83
100	X-RAY DIFFRACTION	100	chain 'S' and (resid 84 through 111 )	S	84 - 111
101	X-RAY DIFFRACTION	101	chain 'S' and (resid 112 through 125 )	S	112 - 125
102	X-RAY DIFFRACTION	102	chain 'S' and (resid 126 through 137 )	S	126 - 137
103	X-RAY DIFFRACTION	103	chain 'S' and (resid 138 through 163 )	S	138 - 163
104	X-RAY DIFFRACTION	104	chain 'S' and (resid 164 through 187 )	S	164 - 187
105	X-RAY DIFFRACTION	105	chain 'S' and (resid 188 through 198 )	S	188 - 198
106	X-RAY DIFFRACTION	106	chain 'S' and (resid 199 through 208 )	S	199 - 208
107	X-RAY DIFFRACTION	107	chain 'T' and (resid 2 through 111 )	T	2 - 111
108	X-RAY DIFFRACTION	108	chain 'T' and (resid 112 through 208 )	T	112 - 208
109	X-RAY DIFFRACTION	109	chain 'U' and (resid 2 through 111 )	U	2 - 111
110	X-RAY DIFFRACTION	110	chain 'U' and (resid 112 through 124 )	U	112 - 124
111	X-RAY DIFFRACTION	111	chain 'U' and (resid 125 through 163 )	U	125 - 163
112	X-RAY DIFFRACTION	112	chain 'U' and (resid 164 through 198 )	U	164 - 198
113	X-RAY DIFFRACTION	113	chain 'U' and (resid 199 through 208 )	U	199 - 208
114	X-RAY DIFFRACTION	114	chain 'V' and (resid 2 through 98 )	V	2 - 98
115	X-RAY DIFFRACTION	115	chain 'V' and (resid 99 through 124 )	V	99 - 124
116	X-RAY DIFFRACTION	116	chain 'V' and (resid 125 through 163 )	V	125 - 163
117	X-RAY DIFFRACTION	117	chain 'V' and (resid 164 through 198 )	V	164 - 198
118	X-RAY DIFFRACTION	118	chain 'V' and (resid 199 through 208 )	V	199 - 208
119	X-RAY DIFFRACTION	119	chain 'W' and (resid 2 through 83 )	W	2 - 83
120	X-RAY DIFFRACTION	120	chain 'W' and (resid 84 through 209 )	W	84 - 209
121	X-RAY DIFFRACTION	121	chain 'X' and (resid 2 through 54 )	X	2 - 54
122	X-RAY DIFFRACTION	122	chain 'X' and (resid 55 through 83 )	X	55 - 83
123	X-RAY DIFFRACTION	123	chain 'X' and (resid 84 through 111 )	X	84 - 111
124	X-RAY DIFFRACTION	124	chain 'X' and (resid 112 through 125 )	X	112 - 125
125	X-RAY DIFFRACTION	125	chain 'X' and (resid 126 through 137 )	X	126 - 137
126	X-RAY DIFFRACTION	126	chain 'X' and (resid 138 through 147 )	X	138 - 147
127	X-RAY DIFFRACTION	127	chain 'X' and (resid 148 through 163 )	X	148 - 163
128	X-RAY DIFFRACTION	128	chain 'X' and (resid 164 through 187 )	X	164 - 187
129	X-RAY DIFFRACTION	129	chain 'X' and (resid 188 through 198 )	X	188 - 198
130	X-RAY DIFFRACTION	130	chain 'X' and (resid 199 through 209 )	X	199 - 209