詳細 | タイプ | Solution-ID | 内容 | Label | 溶媒系 |
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solution1 | 1.0 mM [U-99% 13C; U-99% 15N] HlyIIC, 20 mM sodium phosphate, 1 mM EDTA, 0.05 % w/v sodium azide, 1 mM AEBSF protease inhibitor, 90% H2O/10% D2O | 13C15N_sample90% H2O/10% D2Osolution2 | 1.0 mM [U-99% 15N] HlyIIC, 20 mM sodium phosphate, 1 mM EDTA, 1 mM AEBSF protease inhibitor, 0.05 % w/v sodium azide, 90% H2O/10% D2O | 15N_sample90% H2O/10% D2Osolution3 | 1.0 mM [U-99% 15N] HlyIIC, 20 mM sodium phosphate, 1.0 mM EDTA, 1.0 mM AEBSF protease inhibitor, 0.05 % w/v sodium azide, 100% D2O | D2O100% D2O | | | | | | | | |
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試料 | 濃度 (mg/ml) | 構成要素 | Isotopic labeling | Solution-ID |
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1.0 mMHlyIIC[U-99% 13C; U-99% 15N] | 1 | 20 mMsodium phosphatenone1 | 1 mMEDTAnone1 | 0.05 % w/vsodium azidenone1 | 1 mMAEBSF protease inhibitornone1 | 1.0 mMHlyIIC[U-99% 15N] | 2 | 20 mMsodium phosphatenone2 | 1 mMEDTAnone2 | 1 mMAEBSF protease inhibitornone2 | 0.05 % w/vsodium azidenone2 | 1.0 mMHlyIIC[U-99% 15N] | 3 | 20 mMsodium phosphatenone3 | 1.0 mMEDTAnone3 | 1.0 mMAEBSF protease inhibitornone3 | 0.05 % w/vsodium azidenone3 | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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試料状態 | イオン強度: 0 M / Label: 1 / pH: 6.0 / 圧: 1 atm / 温度: 310 K |
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