ジャーナル: Metallomics / 年: 2017 タイトル: Flexible aspartates propel iron to the ferroxidation sites along pathways stabilized by a conserved arginine in Dps proteins from Mycobacterium smegmatis 著者: Williams, S.M. / Chatterji, D.
A: Putative starvation-induced DNA protecting protein/Ferritin and Dps B: Putative starvation-induced DNA protecting protein/Ferritin and Dps C: Putative starvation-induced DNA protecting protein/Ferritin and Dps D: Putative starvation-induced DNA protecting protein/Ferritin and Dps ヘテロ分子
A: Putative starvation-induced DNA protecting protein/Ferritin and Dps B: Putative starvation-induced DNA protecting protein/Ferritin and Dps C: Putative starvation-induced DNA protecting protein/Ferritin and Dps D: Putative starvation-induced DNA protecting protein/Ferritin and Dps ヘテロ分子
A: Putative starvation-induced DNA protecting protein/Ferritin and Dps B: Putative starvation-induced DNA protecting protein/Ferritin and Dps C: Putative starvation-induced DNA protecting protein/Ferritin and Dps D: Putative starvation-induced DNA protecting protein/Ferritin and Dps ヘテロ分子
A: Putative starvation-induced DNA protecting protein/Ferritin and Dps B: Putative starvation-induced DNA protecting protein/Ferritin and Dps C: Putative starvation-induced DNA protecting protein/Ferritin and Dps D: Putative starvation-induced DNA protecting protein/Ferritin and Dps ヘテロ分子
温度: 298 K / 手法: マイクロバッチ法 / pH: 6 / 詳細: 100 mM sodium cacodylate, 150 mM MgCl2, 20% PEG3350
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データ収集
回折
平均測定温度: 100 K
放射光源
由来: 回転陽極 / タイプ: BRUKER AXS MICROSTAR / 波長: 1.54179 Å
検出器
タイプ: MAR scanner 345 mm plate / 検出器: IMAGE PLATE / 日付: 2013年5月5日
放射
プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 1.54179 Å / 相対比: 1
反射
解像度: 2→30 Å / Num. obs: 41444 / % possible obs: 89.9 % / 冗長度: 17 % / Net I/σ(I): 38.5
反射 シェル
解像度: 2→2.11 Å / Mean I/σ(I) obs: 15.7 / % possible all: 82.2
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解析
ソフトウェア
名称
バージョン
分類
REFMAC
5.8.0103
精密化
MOSFLM
データ削減
SCALA
データスケーリング
REFMAC
位相決定
精密化
解像度: 2→30 Å / Cor.coef. Fo:Fc: 0.937 / Cor.coef. Fo:Fc free: 0.909 / SU B: 3.641 / SU ML: 0.103 / 交差検証法: THROUGHOUT / ESU R: 0.216 / ESU R Free: 0.177 / 詳細: HYDROGENS HAVE BEEN USED IF PRESENT IN THE INPUT