温度: 281 K / 手法: 蒸気拡散法, シッティングドロップ法 詳細: the reservoir condition consisted of 2.9 M ammonium sulfate with 0.1 M Tris buffer at pH 8.3; concentrated CA II at ~10 mg mL-1 was set up with seeding; dry compound was added to crystals ...詳細: the reservoir condition consisted of 2.9 M ammonium sulfate with 0.1 M Tris buffer at pH 8.3; concentrated CA II at ~10 mg mL-1 was set up with seeding; dry compound was added to crystals several days before harvesting and data collection
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データ収集
回折
平均測定温度: 100 K
放射光源
由来: シンクロトロン / サイト: Australian Synchrotron / ビームライン: MX1 / 波長: 0.9537 Å
解像度: 1.21→41.5 Å / Cor.coef. Fo:Fc: 0.96 / Cor.coef. Fo:Fc free: 0.955 / SU B: 1.36 / SU ML: 0.027 / 交差検証法: THROUGHOUT / ESU R: 0.049 / ESU R Free: 0.045 / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS