Software | Name | Version | Classification |
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PHENIX | 1.11rc1_2513refinementXSCALE | | data scalingPHASER | | phasingPDB_EXTRACT | 3.2 | data extractionXDS | | data reductionCoot | | model building | | | | | | |
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Refinement | Method to determine structure: MOLECULAR REPLACEMENT Starting model: 4eit Resolution: 1.95→40.863 Å / SU ML: 0.19 / Cross valid method: FREE R-VALUE / σ(F): 1.35 / Phase error: 19.4
| Rfactor | Num. reflection | % reflection |
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Rfree | 0.1869 | 2005 | 1.82 % |
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Rwork | 0.1509 | - | - |
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obs | 0.1516 | 110338 | 99.7 % |
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Solvent computation | Shrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å |
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Displacement parameters | Biso max: 106.24 Å2 / Biso mean: 34.5054 Å2 / Biso min: 10.82 Å2 |
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Refinement step | Cycle: final / Resolution: 1.95→40.863 Å
| Protein | Nucleic acid | Ligand | Solvent | Total |
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Num. atoms | 11675 | 0 | 294 | 821 | 12790 |
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Biso mean | - | - | 34.93 | 38.7 | - |
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Num. residues | - | - | - | - | 1573 |
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Refine LS restraints | Refine-ID | Type | Dev ideal | Number |
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X-RAY DIFFRACTION | f_bond_d0.007 | 12383 | X-RAY DIFFRACTION | f_angle_d0.835 | 16885 | X-RAY DIFFRACTION | f_chiral_restr0.052 | 1961 | X-RAY DIFFRACTION | f_plane_restr0.005 | 2240 | X-RAY DIFFRACTION | f_dihedral_angle_d15.78 | 7422 | | | | | |
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LS refinement shell | Refine-ID: X-RAY DIFFRACTION / Total num. of bins used: 14 Resolution (Å) | Rfactor Rfree | Num. reflection Rfree | Rfactor Rwork | Num. reflection Rwork | Num. reflection all | % reflection obs (%) |
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1.95-1.9988 | 0.2864 | 121 | 0.2293 | 7709 | 7830 | 100 | 1.9988-2.0528 | 0.2374 | 150 | 0.2032 | 7666 | 7816 | 100 | 2.0528-2.1132 | 0.2403 | 140 | 0.1931 | 7720 | 7860 | 100 | 2.1132-2.1814 | 0.2428 | 154 | 0.1794 | 7694 | 7848 | 100 | 2.1814-2.2594 | 0.206 | 133 | 0.1656 | 7773 | 7906 | 100 | 2.2594-2.3499 | 0.2142 | 153 | 0.1568 | 7638 | 7791 | 100 | 2.3499-2.4568 | 0.2024 | 169 | 0.1519 | 7685 | 7854 | 100 | 2.4568-2.5863 | 0.2036 | 138 | 0.1553 | 7795 | 7933 | 100 | 2.5863-2.7483 | 0.203 | 123 | 0.1551 | 7712 | 7835 | 100 | 2.7483-2.9604 | 0.2238 | 133 | 0.1558 | 7782 | 7915 | 100 | 2.9604-3.2583 | 0.1699 | 143 | 0.1565 | 7749 | 7892 | 100 | 3.2583-3.7295 | 0.2085 | 148 | 0.1392 | 7767 | 7915 | 100 | 3.7295-4.6976 | 0.1388 | 151 | 0.1188 | 7786 | 7937 | 100 | 4.6976-40.8722 | 0.1421 | 149 | 0.1418 | 7857 | 8006 | 99 |
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Refinement TLS params. | Method: refined / Refine-ID: X-RAY DIFFRACTION ID | L11 (°2) | L12 (°2) | L13 (°2) | L22 (°2) | L23 (°2) | L33 (°2) | S11 (Å °) | S12 (Å °) | S13 (Å °) | S21 (Å °) | S22 (Å °) | S23 (Å °) | S31 (Å °) | S32 (Å °) | S33 (Å °) | T11 (Å2) | T12 (Å2) | T13 (Å2) | T22 (Å2) | T23 (Å2) | T33 (Å2) | Origin x (Å) | Origin y (Å) | Origin z (Å) |
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1 | 3.1481 | 0.3613 | -0.1684 | 3.4746 | -1.2291 | 3.4313 | 0.0185 | -0.042 | 0.0178 | -0.0244 | -0.0683 | 0.3244 | 0.0872 | -0.3967 | 0.0223 | 0.1317 | -0.0638 | -0.003 | 0.3428 | -0.0614 | 0.2572 | -23.6145 | 10.2456 | 43.88 | 2 | 3.5123 | -1.514 | 0.0213 | 8.0629 | -1.1888 | 2.2554 | 0.18 | -0.438 | -0.4143 | 0.3306 | -0.2764 | 1.0548 | 0.2655 | -1.0618 | 0.0854 | 0.3071 | -0.1484 | 0.089 | 0.6138 | -0.1384 | 0.5348 | -32.4802 | 4.5783 | 49.8725 | 3 | 2.2802 | -0.3187 | 1.0514 | 0.9847 | -0.6769 | 1.2999 | 0.1267 | -0.0793 | -0.3103 | -0.1114 | -0.0148 | 0.2404 | 0.3804 | -0.3625 | -0.0691 | 0.2573 | -0.1212 | 0.0247 | 0.2715 | -0.0343 | 0.2547 | -14.9345 | -2.2089 | 49.4096 | 4 | 1.6916 | -0.1446 | 1.136 | 1.7962 | -0.4801 | 0.9331 | 0.0046 | -0.1564 | -0.0309 | 0.098 | -0.0047 | 0.0593 | 0.1107 | -0.2988 | 0.0229 | 0.1772 | -0.0856 | 0.022 | 0.1895 | -0.0297 | 0.1983 | -8.0315 | 3.6369 | 50.305 | 5 | 5.1221 | 0.2684 | 2.0925 | 3.6183 | -0.6578 | 5.2294 | -0.0008 | -0.8739 | 0.2321 | 0.2878 | -0.0281 | 0.2396 | -0.3576 | -0.887 | 0.0097 | 0.2245 | 0.065 | -0.0006 | 0.3884 | -0.0957 | 0.2221 | -10.5207 | 18.5724 | 65.2037 | 6 | 2.6983 | -0.1468 | 0.74 | 1.3541 | -0.3297 | 0.5097 | -0.2008 | -0.1283 | 0.2797 | 0.0751 | 0.0192 | 0.0601 | -0.088 | -0.2127 | 0.1733 | 0.188 | -0.0277 | -0.0159 | 0.1617 | -0.031 | 0.2201 | -7.392 | 16.5144 | 52.2346 | 7 | 2.1961 | 0.576 | 0.3045 | 3.722 | 0.2553 | 3.2124 | -0.1363 | 0.1141 | -0.0319 | -0.0397 | -0.0205 | -0.2878 | -0.0158 | 0.3985 | 0.1359 | 0.1173 | -0.0426 | -0.0068 | 0.2296 | 0.0345 | 0.1709 | 33.9233 | 9.6518 | 70.064 | 8 | 6.0507 | -3.513 | 1.668 | 2.088 | -0.9139 | 5.5025 | -0.2869 | 0.0744 | 0.6854 | -0.3892 | 0.1239 | -0.19 | -0.3811 | 0.3031 | 0.1882 | 0.232 | -0.082 | -0.0641 | 0.2876 | 0.0376 | 0.2318 | 37.7779 | 20.1857 | 75.6117 | 9 | 0.2077 | 0.3529 | -0.6574 | 2.4784 | -0.3695 | 3.4418 | -0.2566 | 0.6053 | 0.5101 | 0.0238 | -0.099 | -0.5172 | 0.0979 | 1.3345 | 0.3058 | 0.1483 | -0.2821 | -0.0194 | 0.713 | 0.2249 | 0.4075 | 41.2397 | 19.2115 | 61.3083 | 10 | 3.3805 | -2.024 | 0.8845 | 2.9948 | -0.418 | 1.2005 | -0.2496 | 0.0003 | 0.4994 | -0.0142 | 0.0045 | -0.04 | -0.4587 | 0.2366 | 0.2077 | 0.3304 | -0.1234 | -0.0779 | 0.213 | 0.0252 | 0.2865 | 20.6483 | 26.106 | 60.9532 | 11 | 5.4936 | -2.334 | 0.7515 | 1.7648 | 0.4074 | 2.8181 | 0.0747 | 0.6534 | -0.0398 | -0.3955 | -0.0546 | -0.0848 | -0.1689 | 1.316 | 0.0667 | 0.2449 | -0.1188 | 0.0236 | 0.5853 | 0.0788 | 0.2116 | 33.2583 | 16.3735 | 52.5321 | 12 | 3.403 | -0.6752 | 1.3404 | 3.3557 | -0.1319 | 1.7773 | -0.1313 | 0.102 | 0.3911 | 0.0493 | 0.0111 | -0.1103 | -0.2244 | 0.136 | 0.0408 | 0.1961 | -0.0625 | -0.0049 | 0.113 | 0.0118 | 0.1216 | 17.6013 | 14.5173 | 61.1192 | 13 | 2.4897 | -2.1823 | -0.385 | 5.07 | 2.8137 | 3.4093 | -0.2486 | 0.3662 | 0.1821 | -0.0582 | 0.0808 | -0.0904 | -0.0656 | 0.238 | 0.169 | 0.2064 | -0.1044 | -0.0063 | 0.2154 | 0.045 | 0.1789 | 20.5809 | 15.3112 | 53.1373 | 14 | 3.3234 | -0.0003 | -0.3938 | 1.2985 | -0.1607 | 2.378 | -0.1245 | -0.247 | 0.3757 | 0.1303 | 0.0311 | 0.0761 | -0.2061 | -0.0234 | 0.0712 | 0.1723 | -0.005 | -0.0089 | 0.1177 | -0.0179 | 0.1813 | 13.9507 | 13.7739 | 71.5571 | 15 | 1.6535 | 0.3683 | 1.1822 | 2.2465 | 1.2853 | 5.0837 | -0.0993 | 0.1642 | -0.1004 | 0.1145 | 0.0451 | -0.1362 | 0.2522 | 0.3309 | 0.063 | 0.1279 | -0.0154 | 0.0308 | 0.1419 | 0.0164 | 0.1799 | 24.8001 | 2.3655 | 63.8132 | 16 | 4.5022 | -1.2354 | 1.432 | 4.0171 | 0.5573 | 3.5074 | -0.1321 | -0.3097 | -0.2032 | 0.186 | 0.023 | 0.3578 | -0.1168 | -0.2917 | 0.1325 | 0.1715 | -0.0253 | 0.0281 | 0.1167 | -0.0013 | 0.1508 | 6.7565 | 8.3155 | 67.6896 | 17 | 3.8533 | 1.5359 | 1.1178 | 3.7037 | 1.0757 | 3.0912 | 0.2621 | 0.0736 | -0.7901 | -0.1686 | -0.0773 | -0.2612 | 0.5927 | 0.1953 | -0.1554 | 0.3352 | 0.0629 | 0.0287 | 0.1431 | 0.0146 | 0.4106 | 19.3212 | -17.6855 | 65.4733 | 18 | 4.0987 | -0.113 | 0.5702 | 0.7416 | 0.0763 | 0.9506 | 0.4705 | 0.139 | -1.1307 | -0.4658 | -0.1601 | 0.0916 | 0.8187 | 0.0816 | -0.2298 | 0.6521 | 0.0376 | -0.0388 | 0.2297 | -0.0151 | 0.7335 | 12.3929 | -26.8295 | 63.3391 | 19 | 1.6371 | 0.1172 | 0.2107 | 1.7508 | -0.558 | 1.0185 | 0.0219 | -0.1227 | -0.5369 | 0.0084 | 0.0242 | 0.1043 | 0.4469 | -0.0203 | -0.0832 | 0.3894 | -0.0764 | 0.0459 | 0.2068 | 0.0505 | 0.4247 | 6.9862 | -19.1883 | 69.371 | 20 | 1.9091 | -0.1125 | 1.7471 | 1.8997 | -0.7415 | 1.9372 | 0.0566 | 0.2864 | -0.4997 | -0.4575 | 0.1175 | 0.1873 | 0.7008 | 0.0699 | -0.142 | 0.4452 | -0.1067 | 0.0149 | 0.2427 | -0.0767 | 0.3522 | -3.4465 | -12.87 | 46.9084 | 21 | 1.9887 | 0.2102 | 0.8854 | 2.087 | -1.3322 | 2.5905 | -0.0117 | -0.0434 | -0.2941 | -0.0174 | 0.0496 | 0.0426 | 0.2913 | -0.1383 | 0.0031 | 0.2053 | -0.0405 | 0.0484 | 0.1206 | -0.0162 | 0.2553 | 5.9503 | -8.3611 | 61.4773 | 22 | 2.279 | 0.5169 | 2.5179 | 1.3888 | 2.1446 | 7.3299 | 0.1219 | -0.0585 | -0.1738 | 0.0729 | 0.1176 | -0.0263 | 0.4101 | 0.1252 | -0.2049 | 0.1713 | -0.0477 | 0.048 | 0.1161 | 0.005 | 0.2045 | 2.5535 | -3.7444 | 61.1716 | 23 | 2.9531 | -0.0059 | 0.4795 | 2.4024 | -0.9462 | 0.4394 | 0.0885 | 0.477 | -0.4933 | -0.3353 | 0.0224 | -0.0131 | 1.0353 | -0.0485 | -0.0054 | 0.3675 | -0.0498 | 0.018 | 0.1808 | -0.0805 | 0.2918 | 12.4263 | -9.4031 | 55.1635 | 24 | 2.2644 | -0.6718 | 1.519 | 3.933 | -0.2988 | 4.5226 | 0.0872 | 0.702 | -0.3562 | -0.4733 | -0.0553 | 0.0241 | 0.3488 | 0.5068 | -0.0532 | 0.2727 | 0.0376 | 0.038 | 0.4462 | -0.1318 | 0.2738 | 20.9352 | -5.1255 | 42.3413 | 25 | 2.1974 | -0.4337 | 0.7379 | 2.9089 | 0.1559 | 2.3651 | 0.0959 | -0.0684 | -0.2451 | 0.0604 | -0.0171 | -0.1367 | 0.1227 | 0.1548 | -0.0135 | 0.1657 | -0.0169 | 0.0323 | 0.1034 | 0.0133 | 0.205 | 19.285 | -4.5502 | 65.2589 | 26 | 2.8797 | -0.5044 | 0.9917 | 4.7111 | -0.8044 | 1.9838 | -0.0636 | 0.5764 | -0.0001 | -0.5118 | -0.0859 | -0.2304 | 0.1712 | 0.5318 | 0.1549 | 0.2025 | -0.0589 | 0.0354 | 0.3111 | -0.0258 | 0.1691 | 17.6064 | 2.7809 | 46.3033 | 27 | 2.9103 | -0.1599 | -1.8228 | 1.9163 | 0.8263 | 4.0408 | -0.169 | 0.7901 | 0.5427 | -0.4814 | -0.2357 | 0.4239 | -0.8786 | -0.4265 | 0.3774 | 0.4738 | -0.0229 | -0.242 | 0.3451 | 0.0801 | 0.5053 | -4.6652 | 32.8651 | 36.8479 | 28 | 1.8437 | 0.164 | -0.5142 | 2.0438 | 0.3515 | 0.4627 | -0.2703 | 0.5608 | 0.6241 | -0.506 | 0.0464 | 0.3278 | -0.6235 | 0.0911 | 0.0808 | 0.5337 | -0.111 | -0.2122 | 0.3139 | 0.1943 | 0.4759 | -1.7638 | 33.6732 | 34.6793 | 29 | 5.7831 | 0.2512 | -1.0075 | 2.2092 | 0.1354 | 1.4852 | 0.0756 | 0.0132 | 0.3987 | -0.6035 | -0.029 | -0.0931 | -0.931 | 0.6615 | -0.0164 | 0.8546 | -0.3961 | -0.2063 | 0.7074 | 0.3809 | 0.5604 | 5.2554 | 39.9614 | 28.8161 | 30 | 1.2095 | -1.414 | 0.2731 | 1.8794 | -0.9962 | 2.1159 | -0.2 | 0.0361 | 0.6168 | 0.0041 | 0.222 | 0.1453 | -0.8075 | 0.5432 | 0.1098 | 0.7503 | -0.1666 | -0.2545 | 0.2047 | 0.1823 | 0.7717 | 5.3246 | 43.7561 | 43.0635 | 31 | 1.662 | -0.3719 | 0.6163 | 1.4759 | -0.3863 | 1.6727 | -0.1978 | 0.26 | 0.3933 | -0.166 | -0.0604 | 0.0045 | -0.54 | 0.3095 | 0.2627 | 0.4027 | -0.1532 | -0.1205 | 0.2659 | 0.0937 | 0.3511 | 13.0683 | 30.1678 | 46.1449 | 32 | 2.1003 | -0.0809 | 0.2427 | 1.2806 | -0.1705 | 2.0361 | -0.2215 | 0.1616 | 0.2984 | -0.104 | 0.0242 | 0.0814 | -0.3549 | 0.1482 | 0.1541 | 0.2478 | -0.0925 | -0.0741 | 0.171 | 0.03 | 0.2442 | 7.6213 | 22.0311 | 48.9381 | 33 | 2.4951 | -1.0804 | 0.8811 | 3.4921 | 0.895 | 1.947 | -0.1662 | 0.2206 | 0.5478 | -0.3125 | 0.2019 | -0.3223 | -0.2315 | 0.5445 | -0.1039 | 0.276 | -0.127 | -0.0716 | 0.2573 | 0.0414 | 0.2947 | 6.377 | 22.3424 | 40.051 | 34 | 2.4054 | -0.8517 | -0.2778 | 2.3253 | 0.773 | 2.4607 | -0.0625 | 0.4826 | 0.1136 | -0.2298 | 0.009 | -0.1643 | -0.0344 | 0.2496 | 0.0202 | 0.1898 | -0.0946 | -0.0292 | 0.2812 | 0.0249 | 0.1829 | 3.8951 | 12.2627 | 36.2214 | 35 | 2.5904 | -0.0889 | 0.9286 | 3.6965 | -1.2764 | 5.2307 | 0.1187 | -0.195 | 0.0116 | 0.1776 | -0.1049 | 0.1725 | -0.2505 | -0.536 | -0.0568 | 0.1682 | 0.0742 | 0.0352 | 0.444 | -0.0533 | 0.2399 | -23.3444 | 14.5413 | 14.9938 | 36 | 3.8848 | 0.4187 | 0.1375 | 2.8619 | 1.2305 | 1.595 | 0.0228 | -0.12 | 0.5417 | -0.2469 | -0.2479 | 0.494 | -0.6068 | -0.7269 | 0.1733 | 0.3348 | 0.1739 | -0.0371 | 0.5288 | -0.0655 | 0.3302 | -24.5074 | 22.3641 | 11.2078 | 37 | 2.1632 | -0.2326 | -1.2155 | 1.5206 | 0.1224 | 3.2211 | 0.0939 | -0.1408 | 0.2841 | -0.0019 | -0.1214 | 0.0756 | -0.4819 | -0.1338 | 0.0209 | 0.2109 | 0.0288 | -0.0284 | 0.2397 | -0.0271 | 0.2281 | -9.5501 | 20.3088 | 5.7584 | 38 | 0.8431 | -0.2207 | 1.2709 | 1.5013 | -3.2908 | 9.8716 | 0.011 | -0.018 | -0.0174 | 0.0052 | -0.0176 | -0.0245 | -0.1725 | -0.0516 | 0.0073 | 0.1122 | 0.0017 | 0.0018 | 0.1865 | -0.0148 | 0.1732 | -3.0576 | 13.1665 | 7.4455 | 39 | 3.4085 | 0.834 | 3.852 | 1.577 | 1.4101 | 5.5015 | -0.1288 | -0.1108 | 0.0946 | -0.1714 | 0.0697 | 0.2617 | -0.9115 | -1.0856 | 0.0028 | 0.234 | 0.0849 | 0.0096 | 0.4007 | -0.005 | 0.2089 | -15.2545 | 10.5756 | 3.989 | 40 | 2.2892 | -0.4795 | 0.029 | 1.7491 | -0.0973 | 2.2571 | 0.1136 | 0.1656 | 0.0334 | -0.2103 | -0.0692 | 0.1375 | 0.0955 | -0.5714 | -0.0447 | 0.146 | -0.0202 | -0.0034 | 0.3081 | 0.0125 | 0.1978 | -17.2155 | 2.1539 | -2.4151 | 41 | 3.6748 | 1.0135 | 0.6578 | 4.2959 | -0.0259 | 3.7447 | 0.3138 | 0.2291 | -0.2269 | -0.046 | -0.0876 | -0.257 | 0.3104 | 0.769 | -0.2386 | 0.3223 | 0.2319 | 0.0385 | 0.5341 | -0.1041 | 0.2363 | 20.5653 | -15.286 | -17.7643 | 42 | 1.3151 | -0.8485 | -1.0879 | 1.3252 | -0.256 | 2.2585 | 0.1711 | 0.5462 | -0.4663 | -0.4492 | -0.1145 | -0.1901 | 0.6192 | 0.4037 | -0.0244 | 0.4747 | 0.2435 | -0.0149 | 0.5619 | -0.1606 | 0.3333 | 18.3151 | -19.879 | -22.1332 | 43 | 3.6507 | -0.1001 | -0.8519 | 1.2454 | 0.206 | 2.0988 | 0.0644 | 0.1379 | -0.6463 | -0.0062 | -0.0523 | -0.1027 | 0.6125 | 0.2187 | 0.0193 | 0.3976 | 0.0885 | -0.0673 | 0.2654 | -0.0384 | 0.296 | 10.178 | -23.9786 | -8.2085 | 44 | 4.8492 | -0.3438 | -1.0581 | 1.9466 | 0.2949 | 2.1873 | 0.2861 | 0.018 | -0.3137 | -0.1131 | -0.1409 | 0.0151 | 0.2244 | 0.1576 | -0.1489 | 0.2519 | 0.0126 | -0.0161 | 0.2609 | -0.0188 | 0.1561 | 5.8839 | -10.8963 | -8.3766 | 45 | 6.4412 | 2.1229 | 1.9293 | 1.9014 | 1.2065 | 4.2781 | 0.1506 | 0.0764 | -0.0356 | -0.0365 | -0.0824 | -0.0932 | 0.3026 | 0.2332 | -0.0752 | 0.2308 | 0.0577 | 0.0138 | 0.1875 | -0.0109 | 0.1613 | 7.9428 | -13.2128 | -0.7431 | 46 | 4.3778 | -2.5567 | 2.2276 | 3.1486 | -1.6284 | 3.7814 | 0.1467 | 0.2986 | -0.4032 | -0.2538 | -0.0464 | 0.3247 | 0.2823 | -0.0729 | -0.0957 | 0.1754 | -0.0089 | 0.0256 | 0.2853 | -0.0446 | 0.1729 | 1.3346 | -7.1353 | -18.6376 | 47 | 1.973 | 0.4435 | 0.0504 | 1.1094 | 0.3826 | 3.2146 | 0.0204 | 0.2725 | 0.0113 | -0.1592 | -0.0295 | -0.0105 | 0.0079 | 0.1004 | -0.0147 | 0.1894 | 0.0276 | 0.0192 | 0.2417 | 0.0087 | 0.1245 | 7.8655 | -0.825 | -13.429 |
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Refinement TLS group | ID | Refine-ID | Refine TLS-ID | Selection details | Auth asym-ID | Auth seq-ID |
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1 | X-RAY DIFFRACTION | 1 | chain 'A' and (resid 4 through 44 )A4 - 44 | 2 | X-RAY DIFFRACTION | 2 | chain 'A' and (resid 45 through 59 )A45 - 59 | 3 | X-RAY DIFFRACTION | 3 | chain 'A' and (resid 60 through 159 )A60 - 159 | 4 | X-RAY DIFFRACTION | 4 | chain 'A' and (resid 160 through 205 )A160 - 205 | 5 | X-RAY DIFFRACTION | 5 | chain 'A' and (resid 206 through 224 )A206 - 224 | 6 | X-RAY DIFFRACTION | 6 | chain 'A' and (resid 225 through 267 )A225 - 267 | 7 | X-RAY DIFFRACTION | 7 | chain 'B' and (resid 4 through 44 )B4 - 44 | 8 | X-RAY DIFFRACTION | 8 | chain 'B' and (resid 45 through 59 )B45 - 59 | 9 | X-RAY DIFFRACTION | 9 | chain 'B' and (resid 60 through 86 )B60 - 86 | 10 | X-RAY DIFFRACTION | 10 | chain 'B' and (resid 87 through 124 )B87 - 124 | 11 | X-RAY DIFFRACTION | 11 | chain 'B' and (resid 125 through 138 )B125 - 138 | 12 | X-RAY DIFFRACTION | 12 | chain 'B' and (resid 139 through 159 )B139 - 159 | 13 | X-RAY DIFFRACTION | 13 | chain 'B' and (resid 160 through 183 )B | | | | | | | | | | | | | | | | | | | | | | | | | |
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