regulation of chromatin organization / localization / intermediate filament / negative regulation of proteasomal ubiquitin-dependent protein catabolic process / negative regulation of autophagy / chromosome segregation / cellular response to gamma radiation / chromatin organization / peptidyl-serine phosphorylation / non-specific serine/threonine protein kinase ...regulation of chromatin organization / localization / intermediate filament / negative regulation of proteasomal ubiquitin-dependent protein catabolic process / negative regulation of autophagy / chromosome segregation / cellular response to gamma radiation / chromatin organization / peptidyl-serine phosphorylation / non-specific serine/threonine protein kinase / intracellular signal transduction / protein phosphorylation / protein serine kinase activity / protein serine/threonine kinase activity / DNA damage response / perinuclear region of cytoplasm / nucleoplasm / ATP binding / identical protein binding / nucleus 類似検索 - 分子機能
Serine/threonine-protein kinase, active site / Serine/Threonine protein kinases active-site signature. / Protein kinase domain / Serine/Threonine protein kinases, catalytic domain / Protein kinase, ATP binding site / Protein kinases ATP-binding region signature. / Protein kinase domain profile. / Protein kinase domain / Protein kinase-like domain superfamily 類似検索 - ドメイン・相同性
プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 0.99987 Å / 相対比: 1
反射
解像度: 2.85→72.76 Å / Num. obs: 15761 / % possible obs: 100 % / 冗長度: 2 % / Net I/σ(I): 13.07
反射 シェル
解像度: 2.857→2.959 Å / Num. unique obs: 15761 / % possible all: 100
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解析
ソフトウェア
名称
バージョン
分類
REFMAC
5.8.0158
精密化
XDS
データ削減
SCALA
データスケーリング
PHASER
位相決定
精密化
構造決定の手法: 分子置換 / 解像度: 2.86→89.11 Å / Cor.coef. Fo:Fc: 0.967 / Cor.coef. Fo:Fc free: 0.949 / SU B: 35.731 / SU ML: 0.254 / 交差検証法: THROUGHOUT / ESU R: 0.353 / ESU R Free: 0.244 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.20979
794
5 %
RANDOM
Rwork
0.18251
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-
-
obs
0.18392
14971
99.94 %
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溶媒の処理
イオンプローブ半径: 0.9 Å / 減衰半径: 0.9 Å / VDWプローブ半径: 1 Å / 溶媒モデル: MASK