Hydrolases; Acting on peptide bonds (peptidases); Metalloendopeptidases / proteasome binding / protein sumoylation / transition metal ion binding / metallopeptidase activity / single-stranded DNA binding / double-stranded DNA binding / DNA repair / proteolysis / zinc ion binding ...Hydrolases; Acting on peptide bonds (peptidases); Metalloendopeptidases / proteasome binding / protein sumoylation / transition metal ion binding / metallopeptidase activity / single-stranded DNA binding / double-stranded DNA binding / DNA repair / proteolysis / zinc ion binding / nucleus / cytosol Similarity search - Function
Resolution: 1→30 Å / Num. obs: 61720 / % possible obs: 98.7 % / Redundancy: 8.8 % / Rmerge(I) obs: 0.059 / Net I/σ(I): 21
Reflection shell
Resolution: 1→1.1 Å / Rmerge(I) obs: 0.399 / Mean I/σ(I) obs: 4.9 / % possible all: 99.7
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Processing
Software
Name
Version
Classification
REFMAC
5.7.0032
refinement
XDS
20151015
datareduction
XDS
20151015
datascaling
SHARP
2.8.5
phasing
Refinement
Method to determine structure: SAD / Resolution: 1→8 Å / Cor.coef. Fo:Fc: 0.969 / Cor.coef. Fo:Fc free: 0.959 / SU B: 0.63 / SU ML: 0.015 / Cross valid method: THROUGHOUT / ESU R: 0.023 / ESU R Free: 0.024 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.16724
3086
5 %
RANDOM
Rwork
0.14136
-
-
-
obs
0.14265
58634
98.71 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK