A: Tetrapyrrole-binding protein B: Tetrapyrrole-binding protein C: Tetrapyrrole-binding protein D: Tetrapyrrole-binding protein E: Tetrapyrrole-binding protein F: Tetrapyrrole-binding protein
マシュー密度: 2.64 Å3/Da / 溶媒含有率: 53 % / 解説: very small hexagonal rods
結晶化
温度: 293 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 8 詳細: 1:1 ratio of protein (35 mg/mL in 20 mM Tricine (pH 8.0), 2 mM beta-mercaptoethanol) to well solution (1.0 M ammonium citrate (pH 7.0), 0.1 M Bis Tris Propane (pH 7.0). Crystals only appeared ...詳細: 1:1 ratio of protein (35 mg/mL in 20 mM Tricine (pH 8.0), 2 mM beta-mercaptoethanol) to well solution (1.0 M ammonium citrate (pH 7.0), 0.1 M Bis Tris Propane (pH 7.0). Crystals only appeared after 44 weeks, likely the time taken for proteolysis, resulting in the N- and C-terminal truncations PH範囲: 7.0-8.0
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データ収集
回折
平均測定温度: 100 K
放射光源
由来: シンクロトロン / サイト: Australian Synchrotron / ビームライン: MX2 / 波長: 0.9537 Å
解像度: 3.5→44.5 Å / Cor.coef. Fo:Fc: 0.879 / Cor.coef. Fo:Fc free: 0.813 / SU B: 43.036 / SU ML: 0.663 / 交差検証法: THROUGHOUT / ESU R Free: 0.77 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.31315
753
5.4 %
RANDOM
Rwork
0.25602
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obs
0.25907
13187
99.05 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK