A: Uncharacterized protein B: Uncharacterized protein C: Uncharacterized protein D: Uncharacterized protein E: Uncharacterized protein F: Uncharacterized protein hetero molecules
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.9 Å / Relative weight: 1
Reflection
Resolution: 2.3→50 Å / Num. obs: 72889 / % possible obs: 99.6 % / Redundancy: 5.2 % / Net I/σ(I): 12.5
Reflection shell
Resolution: 2.3→2.34 Å / Redundancy: 4.4 % / Rmerge(I) obs: 0.403 / Mean I/σ(I) obs: 3.8 / % possible all: 99.2
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Processing
Software
Name
Version
Classification
REFMAC
5.5.0109
refinement
HKL-2000
datareduction
HKL-2000
datascaling
MOLREP
phasing
Refinement
Resolution: 2.3→46.57 Å / Cor.coef. Fo:Fc: 0.948 / Cor.coef. Fo:Fc free: 0.907 / SU B: 8.819 / SU ML: 0.218 / Cross valid method: THROUGHOUT / ESU R: 0.439 / ESU R Free: 0.283 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.27647
3668
5 %
RANDOM
Rwork
0.2089
-
-
-
obs
0.21232
69115
99.47 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.4 Å / Solvent model: BABINET MODEL WITH MASK