Type: RIGAKU RAXIS IV / Detector: IMAGE PLATE / Date: Feb 10, 2013
Radiation
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 1.52 Å / Relative weight: 1
Reflection
Redundancy: 4.5 % / Av σ(I) over netI: 10.5 / Number: 154132 / Rsym value: 0.051 / D res high: 1.65 Å / D res low: 19.561 Å / Num. obs: 34360 / % possible obs: 99.3
Diffraction reflection shell
Highest resolution (Å)
Lowest resolution (Å)
% possible obs (%)
ID
Rmerge(I) obs
Rsym value
Redundancy
5.22
19.56
98.1
1
0.028
0.028
4.3
3.69
5.22
99.9
1
0.03
0.03
4.6
3.01
3.69
100
1
0.036
0.036
4.7
2.61
3.01
99.9
1
0.044
0.044
4.7
2.33
2.61
99.9
1
0.054
0.054
4.7
2.13
2.33
100
1
0.063
0.063
4.7
1.97
2.13
99.9
1
0.085
0.085
4.6
1.84
1.97
99.9
1
0.124
0.124
4.6
1.74
1.84
99.8
1
0.191
0.191
4.5
1.65
1.74
96.5
1
0.271
0.271
3.7
Reflection
Resolution: 1.65→19.561 Å / Num. all: 34602 / Num. obs: 34360 / % possible obs: 99.3 % / Redundancy: 4.5 % / Biso Wilson estimate: 16.2 Å2 / Rmerge(I) obs: 0.051 / Rsym value: 0.051 / Net I/σ(I): 17.9
Reflection shell
Diffraction-ID: 1
Resolution (Å)
Redundancy (%)
Rmerge(I) obs
Mean I/σ(I) obs
Num. measured all
Num. unique all
Rsym value
% possible all
1.65-1.74
3.7
0.271
2.9
17555
4769
0.271
96.5
1.74-1.84
4.5
0.191
4.1
21059
4700
0.191
99.8
1.84-1.97
4.6
0.124
6.2
20447
4440
0.124
99.9
1.97-2.13
4.6
0.085
8.9
19102
4126
0.085
99.9
2.13-2.33
4.7
0.063
11.6
17980
3837
0.063
100
2.33-2.61
4.7
0.054
13.2
16365
3470
0.054
99.9
2.61-3.01
4.7
0.044
14.5
14549
3098
0.044
99.9
3.01-3.69
4.7
0.036
16.9
12282
2629
0.036
100
3.69-5.22
4.6
0.03
18.6
9599
2091
0.03
99.9
5.22-19.561
4.3
0.028
16.7
5194
1200
0.028
98.1
-
Phasing
Phasing
Method: molecular replacement
Phasing MR
Rfactor: 53.09 / Model details: Phaser MODE: MR_AUTO
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