- PDB-4mas: High Resolution Structure of Wild Type Human Transthyretin in Com... -
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基本情報
登録情報
データベース: PDB / ID: 4mas
タイトル
High Resolution Structure of Wild Type Human Transthyretin in Complex with 3,3',5,5'-tetrachloro-[1,1'-biphenyl]-4,4'diol
要素
Transthyretin
キーワード
TRANSPORT PROTEIN/INHIBITOR / hormone / binding protein / hormone transport / thyroxine / retinol binding protein / TRANSPORT PROTEIN-INHIBITOR complex
機能・相同性
機能・相同性情報
Retinoid cycle disease events / The canonical retinoid cycle in rods (twilight vision) / thyroid hormone binding / purine nucleobase metabolic process / Non-integrin membrane-ECM interactions / Retinoid metabolism and transport / hormone activity / azurophil granule lumen / Amyloid fiber formation / Neutrophil degranulation ...Retinoid cycle disease events / The canonical retinoid cycle in rods (twilight vision) / thyroid hormone binding / purine nucleobase metabolic process / Non-integrin membrane-ECM interactions / Retinoid metabolism and transport / hormone activity / azurophil granule lumen / Amyloid fiber formation / Neutrophil degranulation / extracellular space / extracellular exosome / extracellular region / identical protein binding 類似検索 - 分子機能
モノクロメーター: Side scattering bent cube-root I-beam single crystal, asymmetric cut 4.965 degrees プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 0.9797 Å / 相対比: 1
反射
解像度: 1.22→35.873 Å / Num. obs: 70897 / % possible obs: 99.5 % / 冗長度: 6.3 % / Biso Wilson estimate: 13.9 Å2 / Rsym value: 0.028 / Net I/σ(I): 27.6
反射 シェル
解像度: 1.22→1.29 Å / 冗長度: 6 % / Mean I/σ(I) obs: 3.5 / Num. unique all: 10085 / Rsym value: 0.515 / % possible all: 98.2
解像度: 1.22→35.873 Å / Cor.coef. Fo:Fc: 0.976 / Cor.coef. Fo:Fc free: 0.972 / SU B: 1.038 / SU ML: 0.021 / 交差検証法: THROUGHOUT / ESU R: 0.04 / ESU R Free: 0.039 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.17339
3580
5.1 %
RANDOM
Rwork
0.15053
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obs
0.15168
67215
99.25 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK