RESIDUES 1-76 WERE TRUNCATED IN THE CONSTRUCT CLONED
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 3.6 Å3/Da / 溶媒含有率: 65.7 % 解説: AN INITIAL MODEL HAS BUILT FROM 3 WAVELENGTH SE-MET MAD. THIS WAS USED FOR MOLECULAR REPLACEMENT IN THE HIGHEST RESOLUTION NATIVE IN SPACEGROUP P212121. THE MODEL FROM THE REFINED P212121 ...解説: AN INITIAL MODEL HAS BUILT FROM 3 WAVELENGTH SE-MET MAD. THIS WAS USED FOR MOLECULAR REPLACEMENT IN THE HIGHEST RESOLUTION NATIVE IN SPACEGROUP P212121. THE MODEL FROM THE REFINED P212121 STRUCTURE WAS USED FOR MOLECULAR REPLACEMENT FOR THIS I222 DATA SET.
結晶化
詳細: 0.12M ETHYLENE GLYCOL, 12.5% PEG 3350, 12.5% PEG 1K, 12.5% MPD, 0.1 M BICINE/TRIZMA BASE
解像度: 3.1→39.92 Å / Cor.coef. Fo:Fc: 0.926 / Cor.coef. Fo:Fc free: 0.891 / SU B: 17.956 / SU ML: 0.329 / 交差検証法: THROUGHOUT / ESU R Free: 0.469 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.27846
741
5.1 %
RANDOM
Rwork
0.21646
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obs
0.21953
13833
98.38 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK