Mass: 18.015 Da / Num. of mol.: 8 / Source method: isolated from a natural source / Formula: H2O
Sequence details
RESIDUES 1-76 WERE TRUNCATED IN THE CONSTRUCT CLONED
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 3.6 Å3/Da / Density % sol: 65.7 % Description: AN INITIAL MODEL HAS BUILT FROM 3 WAVELENGTH SE-MET MAD. THIS WAS USED FOR MOLECULAR REPLACEMENT IN THE HIGHEST RESOLUTION NATIVE IN SPACEGROUP P212121. THE MODEL FROM THE REFINED ...Description: AN INITIAL MODEL HAS BUILT FROM 3 WAVELENGTH SE-MET MAD. THIS WAS USED FOR MOLECULAR REPLACEMENT IN THE HIGHEST RESOLUTION NATIVE IN SPACEGROUP P212121. THE MODEL FROM THE REFINED P212121 STRUCTURE WAS USED FOR MOLECULAR REPLACEMENT FOR THIS I222 DATA SET.
Crystal grow
Details: 0.12M ETHYLENE GLYCOL, 12.5% PEG 3350, 12.5% PEG 1K, 12.5% MPD, 0.1 M BICINE/TRIZMA BASE
Resolution: 3.1→39.92 Å / Cor.coef. Fo:Fc: 0.926 / Cor.coef. Fo:Fc free: 0.891 / SU B: 17.956 / SU ML: 0.329 / Cross valid method: THROUGHOUT / ESU R Free: 0.469 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.27846
741
5.1 %
RANDOM
Rwork
0.21646
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obs
0.21953
13833
98.38 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK