A: FANCONI ANEMIA GROUP M PROTEIN B: FANCONI ANEMIA-ASSOCIATED PROTEIN OF 24 KDA H: 5'-D(*TP*CP*AP*GP*CP*AP*TP*CP*AP*TP*CP)-3' I: 5'-D(*GP*AP*TP*GP*AP*TP*GP*CP*TP*GP*CP)-3' hetero molecules
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 1.5418 Å / Relative weight: 1
Reflection
Resolution: 2.15→30.34 Å / Num. obs: 32846 / % possible obs: 100 % / Observed criterion σ(I): 2 / Redundancy: 10 % / Biso Wilson estimate: 33.1 Å2 / Rmerge(I) obs: 0.06 / Net I/σ(I): 11.4
Reflection shell
Resolution: 2.15→2.27 Å / Redundancy: 9.9 % / Rmerge(I) obs: 0.37 / Mean I/σ(I) obs: 2.1 / % possible all: 100
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Processing
Software
Name
Version
Classification
REFMAC
5.5.0088
refinement
MOSFLM
datareduction
SCALA
datascaling
BNP
phasing
Refinement
Method to determine structure: SAD / Resolution: 2.15→25.43 Å / Cor.coef. Fo:Fc: 0.943 / Cor.coef. Fo:Fc free: 0.911 / SU B: 10.54 / SU ML: 0.129 / Cross valid method: THROUGHOUT / ESU R: 0.21 / ESU R Free: 0.192 Stereochemistry target values: MAXIMUM LIKELIHOOD WITH PHASES Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. RESIDUAL U VALUES ONLY. CHAIN A RESIDUES 1799-1817, 1963-1968, 2036-2048 HAVE NO VISIBLE ELECTRON DENSITY CHAIN B RESIDUES 1-11, 147-153 ...Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. RESIDUAL U VALUES ONLY. CHAIN A RESIDUES 1799-1817, 1963-1968, 2036-2048 HAVE NO VISIBLE ELECTRON DENSITY CHAIN B RESIDUES 1-11, 147-153 HAVE NO VISIBLE ELECTRON DENSITY.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.25523
1645
5.1 %
RANDOM
Rwork
0.2036
-
-
-
obs
0.20615
30696
100 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.4 Å / Solvent model: MASK