ENGINEERED RESIDUE IN CHAIN A, SER 72 TO ASN ENGINEERED RESIDUE IN CHAIN B, SER 72 TO ASN ...ENGINEERED RESIDUE IN CHAIN A, SER 72 TO ASN ENGINEERED RESIDUE IN CHAIN B, SER 72 TO ASN ENGINEERED RESIDUE IN CHAIN C, SER 72 TO ASN ENGINEERED RESIDUE IN CHAIN D, SER 72 TO ASN ENGINEERED RESIDUE IN CHAIN E, SER 72 TO ASN ENGINEERED RESIDUE IN CHAIN F, SER 72 TO ASN
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実験情報
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実験
実験
手法: X線回折
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試料調製
結晶
マシュー密度: 2.9 Å3/Da / 溶媒含有率: 57 % / 解説: NONE
結晶化
詳細: 100 MM BIS-TRIS PROPANE (PH 8.5), 200 MM KSCN AND 13% PEG 3350 (V/V)
解像度: 2.72→25 Å / Cor.coef. Fo:Fc: 0.957 / Cor.coef. Fo:Fc free: 0.936 / SU B: 38.109 / SU ML: 0.334 / 交差検証法: THROUGHOUT / ESU R: 0.984 / ESU R Free: 0.336 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. HYDROGENS HAVE BEEN USED IF PRESENT IN THE INPUT
Rfactor
反射数
%反射
Selection details
Rfree
0.24508
825
5.8 %
RANDOM
Rwork
0.20703
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obs
0.20931
13396
90.71 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK