Method to determine structure: MOLECULAR REPLACEMENT / Resolution: 3.42→47.06 Å / Cor.coef. Fo:Fc: 0.931 / Cor.coef. Fo:Fc free: 0.897 / SU B: 16.412 / SU ML: 0.262 / Cross valid method: THROUGHOUT / ESU R Free: 0.386 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.20913
2003
9.4 %
RANDOM
Rwork
0.17338
-
-
-
all
0.17677
19299
-
-
obs
0.17677
19299
98.76 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK