ソフトウェア | 名称 | バージョン | 分類 |
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HKL-3000 | | データ収集 | MOLREP | | 位相決定 | REFMAC | 5.5.0110精密化 | HKL-3000 | | データ削減 | HKL-3000 | | データスケーリング | |
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精密化 | 構造決定の手法: 分子置換 開始モデル: PDB entry 1vic 解像度: 1.75→25.06 Å / Cor.coef. Fo:Fc: 0.964 / Cor.coef. Fo:Fc free: 0.95 / SU B: 7.131 / SU ML: 0.1 / Isotropic thermal model: Isotropic / 交差検証法: THROUGHOUT / ESU R: 0.133 / ESU R Free: 0.125 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
| Rfactor | 反射数 | %反射 | Selection details |
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Rfree | 0.23209 | 4919 | 5 % | RANDOM |
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Rwork | 0.19806 | - | - | - |
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obs | 0.19979 | 93730 | 100 % | - |
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all | - | 93730 | - | - |
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溶媒の処理 | イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK |
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原子変位パラメータ | Biso mean: 37.235 Å2
| Baniso -1 | Baniso -2 | Baniso -3 |
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1- | -0.42 Å2 | -1.05 Å2 | 0.56 Å2 |
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2- | - | 0.36 Å2 | -1.6 Å2 |
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3- | - | - | 0.63 Å2 |
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精密化ステップ | サイクル: LAST / 解像度: 1.75→25.06 Å
| タンパク質 | 核酸 | リガンド | 溶媒 | 全体 |
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原子数 | 7768 | 0 | 1 | 690 | 8459 |
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拘束条件 | Refine-ID | タイプ | Dev ideal | Dev ideal target | 数 |
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X-RAY DIFFRACTION | r_bond_refined_d0.009 | 0.022 | 7979 | X-RAY DIFFRACTION | r_bond_other_d | | | X-RAY DIFFRACTION | r_angle_refined_deg1.228 | 1.957 | 10898 | X-RAY DIFFRACTION | r_angle_other_deg | | | X-RAY DIFFRACTION | r_dihedral_angle_1_deg9.818 | 5 | 1014 | X-RAY DIFFRACTION | r_dihedral_angle_2_deg34.874 | 24.429 | 359 | X-RAY DIFFRACTION | r_dihedral_angle_3_deg13.86 | 15 | 1295 | X-RAY DIFFRACTION | r_dihedral_angle_4_deg15.395 | 15 | 56 | X-RAY DIFFRACTION | r_chiral_restr0.086 | 0.2 | 1247 | X-RAY DIFFRACTION | r_gen_planes_refined0.01 | 0.021 | 6124 | X-RAY DIFFRACTION | r_gen_planes_other | | | X-RAY DIFFRACTION | r_nbd_refined | | | X-RAY DIFFRACTION | r_nbd_other | | | X-RAY DIFFRACTION | r_nbtor_refined | | | X-RAY DIFFRACTION | r_nbtor_other | | | X-RAY DIFFRACTION | r_xyhbond_nbd_refined | | | X-RAY DIFFRACTION | r_xyhbond_nbd_other | | | X-RAY DIFFRACTION | r_metal_ion_refined | | | X-RAY DIFFRACTION | r_metal_ion_other | | | X-RAY DIFFRACTION | r_symmetry_vdw_refined | | | X-RAY DIFFRACTION | r_symmetry_vdw_other | | | X-RAY DIFFRACTION | r_symmetry_hbond_refined | | | X-RAY DIFFRACTION | r_symmetry_hbond_other | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_refined | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_other | | | X-RAY DIFFRACTION | r_mcbond_it0.475 | 1.5 | 5062 | X-RAY DIFFRACTION | r_mcbond_other | | | X-RAY DIFFRACTION | r_mcangle_it0.882 | 2 | 8214 | X-RAY DIFFRACTION | r_scbond_it1.557 | 3 | 2917 | X-RAY DIFFRACTION | r_scangle_it2.654 | 4.5 | 2680 | X-RAY DIFFRACTION | r_rigid_bond_restr | | | X-RAY DIFFRACTION | r_sphericity_free | | | X-RAY DIFFRACTION | r_sphericity_bonded | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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LS精密化 シェル | 解像度: 1.753→1.798 Å / Total num. of bins used: 20
| Rfactor | 反射数 | %反射 |
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Rfree | 0.322 | 351 | - |
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Rwork | 0.287 | 6714 | - |
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obs | - | - | 100 % |
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精密化 TLS | 手法: refined / Refine-ID: X-RAY DIFFRACTION ID | L11 (°2) | L12 (°2) | L13 (°2) | L22 (°2) | L23 (°2) | L33 (°2) | S11 (Å °) | S12 (Å °) | S13 (Å °) | S21 (Å °) | S22 (Å °) | S23 (Å °) | S31 (Å °) | S32 (Å °) | S33 (Å °) | T11 (Å2) | T12 (Å2) | T13 (Å2) | T22 (Å2) | T23 (Å2) | T33 (Å2) | Origin x (Å) | Origin y (Å) | Origin z (Å) |
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1 | 5.1089 | 1.9337 | -0.043 | 9.5482 | 1.2706 | 4.4677 | -0.1261 | 0.2946 | -0.2186 | -0.0825 | -0.0079 | 0.134 | 0.2031 | 0.0491 | 0.1341 | 0.1719 | 0.0031 | 0.0216 | 0.151 | -0.03 | 0.1316 | 46.9608 | 28.2512 | -14.379 | 2 | 3.0333 | 2.0117 | 0.9965 | 5.79 | 2.578 | 7.092 | -0.1683 | 0.0456 | 0.3872 | -0.2178 | -0.2261 | 0.4908 | -0.2473 | -0.7298 | 0.3944 | 0.1788 | 0.0017 | -0.0193 | 0.0941 | -0.0152 | 0.2337 | 56.0423 | 46.4821 | -5.2978 | 3 | 3.205 | 1.1063 | 0.1559 | 2.3473 | 0.2857 | 1.7796 | -0.1351 | 0.4312 | 0.0491 | -0.2632 | 0.0487 | -0.0896 | -0.0974 | 0.1349 | 0.0865 | 0.1802 | -0.0096 | 0.0398 | 0.1711 | 0.0117 | 0.0739 | 56.8775 | 34.9803 | -15.7941 | 4 | 7.6757 | 3.1434 | -0.4464 | 3.8924 | -1.1178 | 3.437 | 0.9764 | -0.358 | 1.1306 | 0.4331 | -1.0043 | 0.9192 | -0.6458 | -0.0468 | 0.0279 | 0.2596 | -0.028 | 0.0811 | 0.411 | -0.2024 | 0.2834 | 41.7308 | 42.3289 | -14.3861 | 5 | 2.3453 | -0.4285 | 0.1059 | 1.7537 | -0.1254 | 1.6513 | -0.0325 | 0.2586 | -0.1178 | -0.2375 | -0.0013 | 0.126 | -0.1237 | -0.1075 | 0.0338 | 0.1732 | 0.0077 | 0.0013 | 0.1359 | -0.0161 | 0.1484 | 46.9389 | 28.3346 | -11.6186 | 6 | 2.081 | 0.7062 | 0.7023 | 2.2036 | 1.1753 | 4.2591 | -0.0372 | -0.2158 | -0.2003 | 0.0544 | 0.1267 | -0.0917 | 0.0289 | 0.1656 | -0.0895 | 0.1137 | 0.0346 | 0.0066 | 0.1554 | 0.0163 | 0.1933 | 42.685 | 23.4798 | 1.8328 | 7 | 1.9196 | 0.1293 | -0.698 | 1.3302 | -0.0587 | 1.855 | 0.0507 | -0.2853 | -0.0356 | 0.1336 | -0.0683 | -0.0357 | -0.0024 | 0.1471 | 0.0176 | 0.1301 | 0.0068 | -0.0036 | 0.1711 | 0.0203 | 0.1569 | 37.7502 | 27.8114 | 12.0824 | 8 | 1.8492 | 0.1286 | -0.4314 | 0.7748 | -0.0792 | 0.9628 | 0.0585 | -0.0615 | 0.0179 | 0.0231 | -0.0039 | -0.0169 | -0.2206 | 0.0696 | -0.0546 | 0.1859 | 0.0262 | -0.0033 | 0.1267 | -0.0075 | 0.1744 | 37.5027 | 30.8218 | 3.3396 | 9 | 2.1259 | -0.5218 | -0.6157 | 1.3241 | 0.6043 | 0.8032 | 0.0374 | 0.0502 | 0.0179 | -0.0358 | -0.02 | 0.0527 | -0.1166 | -0.0704 | -0.0174 | 0.158 | 0.0235 | -0.0008 | 0.1263 | 0.0303 | 0.1661 | 34.7605 | 31.4115 | 0.6211 | 10 | 2.4528 | 0.4228 | 0.3015 | 2.5282 | -0.178 | 0.2776 | 0.1029 | -0.1203 | -0.0038 | 0.012 | -0.0712 | -0.0796 | 0.0118 | 0.102 | -0.0317 | 0.1992 | -0.0047 | -0.0102 | 0.1262 | -0.0035 | 0.1252 | 64.3963 | 33.2682 | -0.4712 | 11 | 5.5458 | 0.21 | -0.1303 | 4.6496 | 1.855 | 3.3159 | 0.1805 | 0.0146 | -0.1912 | 0.5142 | -0.0138 | -0.0945 | 0.5057 | 0.2053 | -0.1667 | 0.1615 | -0.0463 | -0.0206 | 0.2283 | -0.0335 | 0.1179 | 9.3671 | 18.7454 | 25.9644 | 12 | 1.897 | -0.1137 | 0.6624 | 4.436 | 0.6526 | 7.3463 | 0.1269 | -0.1115 | -0.0291 | 0.5521 | -0.021 | 0.1976 | 0.1999 | -0.239 | -0.1059 | 0.1024 | -0.0624 | 0.0538 | 0.2255 | -0.0129 | 0.0852 | 5.6767 | 22.8204 | 31.3534 | 13 | 3.0996 | -3.8486 | -3.0767 | 7.4089 | 0.102 | 8.9786 | -0.2641 | -0.2095 | -0.3656 | 0.5056 | -0.2316 | 0.1548 | 0.5126 | 0.7147 | 0.4958 | 0.3895 | -0.1732 | -0.1944 | 0.2685 | 0.1193 | 0.2315 | 9.4051 | 12.4752 | 31.3523 | 14 | 2.1558 | 0.6001 | -0.7878 | 3.1804 | 1.228 | 1.3421 | -0.0078 | 0.122 | -0.2117 | 0.1425 | 0.0637 | -0.0062 | 0.0717 | -0.1616 | -0.0559 | 0.086 | -0.0201 | 0.0022 | 0.2506 | -0.0311 | 0.1213 | 8.0754 | 19.4671 | 19.8193 | 15 | 2.4271 | 1.0351 | 0.4912 | 2.2907 | 0.4284 | 1.6558 | 0.0808 | -0.3035 | 0.0421 | -0.0542 | -0.102 | 0.0094 | -0.1036 | -0.16 | 0.0212 | 0.113 | 0.0319 | 0.0282 | 0.219 | -0.0168 | 0.1395 | 16.1064 | 31.4003 | 13.6894 | 16 | 1.9437 | 0.6382 | -0.1523 | 1.379 | 0.1222 | 1.6817 | 0.1158 | -0.2264 | 0.1825 | 0.1364 | -0.0771 | -0.0028 | -0.1401 | -0.0252 | -0.0387 | 0.1438 | 0.0205 | 0.0146 | 0.1592 | -0.0141 | 0.1456 | 28.3294 | 36.407 | 15.4221 | 17 | 16.8594 | -11.9312 | -3.2754 | 9.824 | 4.7597 | 5.0191 | 0.1821 | 0.2963 | -0.1837 | -0.0478 | -0.5045 | 0.2206 | 0.1036 | -0.4573 | 0.3224 | 0.0806 | -0.0803 | 0.0273 | 0.2571 | 0.1675 | 0.3461 | 16.9989 | 13.9271 | 12.9187 | 18 | 2.2852 | -0.1112 | -0.2252 | 1.4839 | 0.4006 | 1.4346 | 0.0135 | -0.142 | -0.3285 | 0.039 | -0.0508 | 0.0358 | 0.1035 | -0.0284 | 0.0373 | 0.1487 | -0.0052 | 0.0294 | 0.1551 | 0.0488 | 0.1579 | 24.8798 | 21.4483 | 13.4369 | 19 | 1.9168 | 0.5301 | -4.2491 | 7.2191 | -3.0259 | 11.7853 | 0.2195 | 0.1057 | 0.1336 | 0.6562 | -0.1312 | -0.6784 | -0.3829 | 0.5717 | -0.0884 | 0.2924 | -0.0342 | -0.0218 | 0.385 | 0.0107 | 0.0849 | 13.6995 | 33.6947 | 34.3916 | 20 | 5.9939 | 0.2273 | -4.1468 | 44.0302 | -36.7981 | 39.7639 | 0.4035 | 0.1496 | 1.5882 | 0.41 | -0.197 | -0.7701 | -1.2612 | -1.1285 | -0.2064 | 0.5902 | 0.0654 | 0.1921 | 0.2954 | -0.0339 | 0.4785 | 3.7567 | 38.8932 | 36.5894 | 21 | 7.8088 | 4.4391 | 1.4129 | 8.6825 | 3.4852 | 3.8809 | -0.0671 | 0.0478 | 0.1942 | -0.1819 | 0.1278 | 0.3659 | -0.1513 | 0.0207 | -0.0607 | 0.1903 | -0.033 | 0.002 | 0.1813 | -0.0076 | 0.1156 | -21.5537 | -3.8115 | 19.2785 | 22 | 4.2634 | 0.8204 | -0.5626 | 4.7481 | 0.276 | 1.03 | -0.0608 | -0.2504 | -0.1607 | 0.3751 | 0.0807 | 0.4016 | 0.0668 | 0.0222 | -0.0198 | 0.1603 | -0.044 | 0.0594 | 0.1645 | 0.0225 | 0.0842 | -23.7233 | -11.1537 | 22.4743 | 23 | 6.3302 | 0.276 | -1.7011 | 9.3449 | -2.6937 | 2.5794 | -0.0674 | -0.0967 | 0.1995 | 0.2251 | 0.2967 | 1.0631 | -0.0982 | -0.3415 | -0.2293 | 0.0961 | -0.0297 | 0.101 | 0.1763 | -0.0348 | 0.2504 | -31.7697 | -2.9356 | 21.6535 | 24 | 9.7917 | -2.1709 | 0.5126 | 9.0887 | 0.8227 | 5.699 | -0.285 | -0.137 | 0.2341 | 0.2178 | 0.4338 | 0.1176 | -0.2561 | 0.0679 | -0.1487 | 0.1117 | -0.001 | 0.0132 | 0.0499 | -0.0584 | 0.222 | -20.8272 | 6.6723 | 18.3222 | 25 | 3.8792 | 2.0457 | -0.678 | 3.4968 | -0.0345 | 0.8565 | 0.0456 | -0.3059 | 0.0244 | 0.1341 | -0.0347 | -0.051 | 0.0254 | 0.0648 | -0.0109 | 0.1543 | -0.039 | -0.0296 | 0.1776 | -0.0218 | 0.1052 | -9.9638 | -4.5653 | 19.8077 | 26 | 0.9097 | 0.4449 | -0.5205 | 1.4109 | 0.4485 | 1.7857 | -0.004 | -0.0593 | -0.1043 | 0.0039 | -0.0337 | -0.0491 | 0.1918 | 0.1242 | 0.0377 | 0.1433 | 0.0253 | -0.0258 | 0.0976 | 0.0214 | 0.1816 | -3.2282 | -8.9727 | 2.9439 | 27 | 3.6416 | -1.0962 | -3.3169 | 2.3466 | 2.4625 | 6.7029 | 0.0588 | 0.1178 | -0.3817 | -0.0958 | -0.1097 | -0.1554 | 0.2913 | 0.1344 | 0.0509 | 0.1568 | 0.0715 | -0.0287 | 0.0561 | 0.0102 | 0.193 | 0.491 | -15.3345 | -0.7772 | 28 | 0.6796 | 0.3335 | 0.7672 | 7.1182 | -6.6785 | 8.0526 | 0.0245 | -0.1816 | 0.1199 | 0.0956 | -0.2856 | -0.0501 | -0.0437 | -0.0937 | 0.2611 | 0.0515 | 0.024 | -0.0063 | 0.2346 | -0.1584 | 0.2803 | -13.3007 | 8.4661 | 11.9374 | 29 | 1.213 | 0.5531 | 0.294 | 1.6996 | -0.1061 | 2.0083 | 0.0096 | -0.0956 | 0.1041 | 0.007 | -0.0753 | 0.1269 | -0.0647 | -0.1415 | 0.0657 | 0.1134 | 0.0277 | -0.0071 | 0.1093 | -0.0096 | 0.2004 | -8.6434 | 0.6995 | 5.4372 | 30 | 6.6808 | -0.3249 | 2.5682 | 4.6494 | -1.5908 | 9.0852 | -0.0329 | -0.017 | -0.708 | 0.1574 | 0.0036 | -0.2276 | 0.3004 | 0.2093 | 0.0293 | 0.1336 | -0.04 | 0.0312 | 0.0823 | -0.0295 | 0.2571 | -21.7385 | -23.5395 | 17.0239 | 31 | 5.2292 | 0.5782 | -0.1144 | 0.5566 | -0.2079 | 7.4247 | -0.0045 | 0.2459 | 0.2441 | -0.0004 | 0.1552 | 0.178 | -0.2237 | -0.1359 | -0.1508 | 0.1981 | -0.1147 | 0.0673 | 0.1396 | -0.0104 | 0.1394 | 20.7054 | 14.4134 | -13.3423 | 32 | 15.7025 | -5.7346 | -0.1102 | 22.4697 | -6.9787 | 15.4898 | 0.1535 | 1.1104 | -2.2234 | 1.0024 | 0.3757 | -1.8594 | 0.98 | 0.8722 | -0.5292 | 0.3533 | 0.0615 | -0.2564 | 0.2864 | -0.4276 | 0.8474 | 23.834 | -3.0234 | -25.3375 | 33 | 6.0166 | -1.7936 | -0.9666 | 4.3401 | 1.6315 | 4.4871 | -0.078 | 0.7758 | 0.1489 | -0.13 | 0.091 | -0.3562 | -0.1616 | 0.5014 | -0.013 | 0.1642 | -0.1295 | 0.0694 | 0.2553 | -0.019 | 0.0713 | 23.5188 | 11.0441 | -21.8904 | 34 | 15.7151 | -3.0692 | 0.3004 | 0.8662 | 2.0181 | 17.6669 | -0.667 | 0.1864 | -1.1708 | 0.3364 | 0.1398 | 0.1982 | 1.6848 | 1.0879 | 0.5272 | 0.3015 | 0.0091 | 0.1722 | 0.2042 | -0.2011 | 0.5589 | 30.3808 | 3.5062 | -16.3526 | 35 | 4.1709 | 0.9932 | 2.7376 | 1.0991 | 1.3356 | 3.5757 | 0.0641 | 0.1369 | -0.0982 | -0.0145 | 0.0764 | -0.2234 | 0.2585 | 0.0463 | -0.1405 | 0.2066 | -0.073 | 0.0541 | 0.1329 | 0.0028 | 0.089 | 20.1367 | 11.2279 | -12.8234 | 36 | 2.0223 | 0.6702 | -0.1039 | 1.4787 | -0.5771 | 0.5863 | -0.1085 | 0.2192 | -0.0531 | -0.2353 | 0.1652 | 0.0492 | -0.0581 | 0.0438 | -0.0567 | 0.2283 | -0.0139 | -0.011 | 0.1381 | -0.0078 | 0.1408 | 1.5911 | 4.0042 | -9.317 | 37 | 4.4076 | 2.334 | 0.8807 | 2.2561 | 0.5795 | 1.4406 | -0.0659 | 0.1554 | -0.1812 | -0.2524 | 0.1103 | -0.0143 | -0.0107 | 0.0043 | -0.0444 | 0.2065 | -0.0015 | -0.0329 | 0.1087 | 0.0037 | 0.138 | 0.2692 | 1.566 | -10.3849 | 38 | 9.4668 | 10.9889 | 3.1459 | 13.6197 | 5.8323 | 6.5648 | 0.2459 | -0.6933 | -0.6637 | 0.4433 | -0.1106 | -0.7042 | 0.4319 | 1.5831 | -0.1353 | 0.0314 | 0.0943 | -0.0371 | 0.6472 | 0.0724 | 0.2956 | 14.332 | -3.5557 | 1.1017 | 39 | 1.7477 | 0.0983 | -0.0519 | 3.1168 | -2.1382 | 4.7527 | 0.015 | -0.0803 | -0.125 | -0.018 | 0.0516 | -0.1578 | -0.3693 | 0.3525 | -0.0666 | 0.1179 | -0.0503 | 0.0156 | 0.1521 | -0.0353 | 0.1355 | 8.1963 | 5.1489 | -3.6454 | 40 | 7.15 | -2.9074 | -0.4006 | 2.5972 | 1.8053 | 11.0922 | 0.2848 | 0.9816 | -0.6232 | 0.0297 | -0.2583 | 0.3114 | 0.1777 | -0.0723 | -0.0266 | 0.2279 | -0.1012 | 0.0564 | 0.298 | -0.1545 | 0.1003 | 12.397 | 1.8856 | -31.2007 |
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精密化 TLSグループ | ID | Refine-ID | Refine TLS-ID | Auth asym-ID | Auth seq-ID |
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1 | X-RAY DIFFRACTION | 1 | A1 - 9 | 2 | X-RAY DIFFRACTION | 2 | A10 - 19 | 3 | X-RAY DIFFRACTION | 3 | A20 - 65 | 4 | X-RAY DIFFRACTION | 4 | A66 - 83 | 5 | X-RAY DIFFRACTION | 5 | A84 - 111 | 6 | X-RAY DIFFRACTION | 6 | A112 - 134 | 7 | X-RAY DIFFRACTION | 7 | A135 - 166 | 8 | X-RAY DIFFRACTION | 8 | A167 - 203 | 9 | X-RAY DIFFRACTION | 9 | A204 - 228 | 10 | X-RAY DIFFRACTION | 10 | A229 - 252 | 11 | X-RAY DIFFRACTION | 11 | B1 - 13 | 12 | X-RAY DIFFRACTION | 12 | B14 - 51 | 13 | X-RAY DIFFRACTION | 13 | B52 - 78 | 14 | X-RAY DIFFRACTION | 14 | B79 - 110 | 15 | X-RAY DIFFRACTION | 15 | B111 - 134 | 16 | X-RAY DIFFRACTION | 16 | B135 - 184 | 17 | X-RAY DIFFRACTION | 17 | B185 - 198 | 18 | X-RAY DIFFRACTION | 18 | B199 - 228 | 19 | X-RAY DIFFRACTION | 19 | B229 - 243 | 20 | X-RAY DIFFRACTION | 20 | B244 - 251 | 21 | X-RAY DIFFRACTION | 21 | C1 - 13 | 22 | X-RAY DIFFRACTION | 22 | C14 - 49 | 23 | X-RAY DIFFRACTION | 23 | C50 - 72 | 24 | X-RAY DIFFRACTION | 24 | C73 - 92 | 25 | X-RAY DIFFRACTION | 25 | C93 - 123 | 26 | X-RAY DIFFRACTION | 26 | C124 - 163 | 27 | X-RAY DIFFRACTION | 27 | C164 - 184 | 28 | X-RAY DIFFRACTION | 28 | C185 - 199 | 29 | X-RAY DIFFRACTION | 29 | C200 - 231 | 30 | X-RAY DIFFRACTION | 30 | C232 - 251 | 31 | X-RAY DIFFRACTION | 31 | D1 - 8 | 32 | X-RAY DIFFRACTION | 32 | D9 - 26 | 33 | X-RAY DIFFRACTION | 33 | D27 - 51 | 34 | X-RAY DIFFRACTION | 34 | D52 - 79 | 35 | X-RAY DIFFRACTION | 35 | D80 - 110 | 36 | X-RAY DIFFRACTION | 36 | D111 - 163 | 37 | X-RAY DIFFRACTION | 37 | D164 - 193 | 38 | X-RAY DIFFRACTION | 38 | D194 - 208 | 39 | X-RAY DIFFRACTION | 39 | D209 - 228 | 40 | X-RAY DIFFRACTION | 40 | D229 - 250 | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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