A SEQUENCE DATABASE REFERENCE FOR THIS PROTEIN DOES NOT CURRENTLY EXIST. THE WILD TYPE HAS BEEN ...A SEQUENCE DATABASE REFERENCE FOR THIS PROTEIN DOES NOT CURRENTLY EXIST. THE WILD TYPE HAS BEEN DEPOSITED TO PDB, 3NPU AND 3NPV. THIS SEQUENCE IS ALA 2 INSERTION AND Y48F, V176E, A204V MUTANT.
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2.45 Å3/Da / 溶媒含有率: 49.82 %
結晶化
温度: 277 K / 手法: マイクロバッチ法 / pH: 5.5 詳細: PCB pH5.0, PEG 1500, pH 5.5, Microbatch, temperature 277K
解像度: 2.02→50 Å / Cor.coef. Fo:Fc: 0.934 / Cor.coef. Fo:Fc free: 0.889 / SU B: 4.2 / SU ML: 0.122 / 交差検証法: THROUGHOUT / ESU R: 0.198 / ESU R Free: 0.184 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.26019
1757
5 %
RANDOM
Rwork
0.20521
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obs
0.20806
33171
97.85 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK