THE AUTHORS STATE THAT THERE IS A PARTIAL HYDROLYSIS OF THE BOND BETWEEN RESIDUES 116 AND 117. FOR ...THE AUTHORS STATE THAT THERE IS A PARTIAL HYDROLYSIS OF THE BOND BETWEEN RESIDUES 116 AND 117. FOR RESIDUES 115-123, CONFORMER A REPRESENTS UNCLEAVED PROTEIN WITH A BOND BETWEEN RESIDUES 116-117. CONFORMER B REPRESENTS CLEAVED CHAIN AND THERE IS NO COVALENT BOND BETWEEN RESIDUES A116 AND B117 DUE TO AUTOCATALYTIC CLEAVAGE DURING CRYSTALLIZATION.
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 3.49 Å3/Da / 溶媒含有率: 64.71 %
結晶化
温度: 291 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 5.5 詳細: 1 M ammonium sulfate, 0.1 M Bis-Tris buffer, 1% PEG-3350, pH 5.5, VAPOR DIFFUSION, SITTING DROP, temperature 291K