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- PDB-390d: STRUCTURAL VARIABILITY AND NEW INTERMOLECULAR INTERACTIONS OF Z-D... -
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Open data
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Basic information
Entry | Database: PDB / ID: 390d | ||||||||||||||||||
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Title | STRUCTURAL VARIABILITY AND NEW INTERMOLECULAR INTERACTIONS OF Z-DNA IN CRYSTALS OF D(PCPGPCPGPCPG) | ||||||||||||||||||
![]() | DNA (5'-D(P*![]() DNA / Z-DNA / DOUBLE HELIX | Function / homology | DNA | ![]() Method | ![]() ![]() Malinina, L. / Tereshko, V. / Ivanova, E. / Subirana, J.A. / Zarytova, V. / Nekrasov, Y. | ![]() ![]() Title: Structural variability and new intermolecular interactions of Z-DNA in crystals of d(pCpGpCpGpCpG). Authors: Malinina, L. / Tereshko, V. / Ivanova, E. / Subirana, J.A. / Zarytova, V. / Nekrasov, Y. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 17.8 KB | Display | ![]() |
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PDB format | ![]() | 11.5 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 357.4 KB | Display | ![]() |
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Full document | ![]() | 357.4 KB | Display | |
Data in XML | ![]() | 2.8 KB | Display | |
Data in CIF | ![]() | 3.5 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
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Links
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Assembly
Deposited unit | ![]()
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1 | ![]()
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2 | ![]()
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Unit cell |
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Components on special symmetry positions |
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Components
#1: DNA chain | Mass: 1810.205 Da / Num. of mol.: 3 / Source method: obtained synthetically #2: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 2.21 Å3/Da / Density % sol: 44.44 % | ||||||||||||||||||||||||||||
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Crystal grow | pH: 6 / Details: pH 6.00 | ||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS Method: other / Details: Malinina, L., (1991) J. Crystal Growth, 110, 252. | ||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 290 K |
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Diffraction source | Source: SEALED TUBE / Type: OTHER / Wavelength: 1.5418 |
Detector | Type: SYNTEX P21 / Detector: DIFFRACTOMETER / Date: Jan 1, 1988 |
Radiation | Monochromator: GRAPHITE / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength: 1.5418 Å / Relative weight: 1 |
Reflection | Resolution: 2→34.9 Å / Num. obs: 3248 / % possible obs: 93 % / Observed criterion σ(I): 1 / Redundancy: 3 % / Rmerge(I) obs: 0.06 |
Reflection | *PLUS Highest resolution: 2 Å / Lowest resolution: 34.9 Å / % possible obs: 93 % / Rmerge(I) obs: 0.026 |
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Processing
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Refinement | Resolution: 2→8 Å / Cross valid method: FREE R-VALUE / σ(F): 2
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Refinement step | Cycle: LAST / Resolution: 2→8 Å
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Refine LS restraints |
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Software | *PLUS Name: ![]() | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refinement | *PLUS Highest resolution: 2 Å / Lowest resolution: 8 Å / σ(F): 2 / Num. reflection Rfree: 309 / % reflection Rfree: 10 % | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Solvent computation | *PLUS | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | *PLUS | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refine LS restraints | *PLUS
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