ソフトウェア 名称 バージョン 分類 NB d*TREK9.2SSIデータスケーリング Show SOLVE2.09 位相決定 Show RESOLVE2.09 位相決定 Show REFMAC精密化 Show PDB_EXTRACT2 データ抽出 Show Blu-Iceデータ収集 CrystalClearデータ削減 CrystalClearデータスケーリング
精密化 構造決定の手法 : 多波長異常分散 / 解像度 : 1.7→34.08 Å / Cor.coef. Fo :Fc : 0.954 / Cor.coef. Fo :Fc free : 0.942 / SU B : 6.573 / SU ML : 0.109 / 交差検証法 : THROUGHOUT / σ(F) : 0 / ESU R : 0.127 / ESU R Free : 0.131 / 立体化学のターゲット値 : MAXIMUM LIKELIHOOD / 詳細 : HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONSRfactor 反射数 %反射 Selection details Rfree 0.271 677 4.9 % RANDOM Rwork 0.218 - - - all 0.221 13741 - - obs 0.221 13741 98.09 % -
溶媒の処理 イオンプローブ半径 : 0.8 Å / 減衰半径 : 0.8 Å / VDWプローブ半径 : 1.4 Å / 溶媒モデル : MASK原子変位パラメータ Biso mean : 24.302 Å2 Baniso -1 Baniso -2 Baniso -3 1- 0.76 Å2 0.38 Å2 0 Å2 2- - 0.76 Å2 0 Å2 3- - - -1.15 Å2
Refine analyze Luzzati coordinate error obs : 0.291 Å精密化ステップ サイクル : LAST / 解像度 : 1.7→34.08 Åタンパク質 核酸 リガンド 溶媒 全体 原子数 907 0 32 61 1000
拘束条件 大きな表を表示 (5 x 17) 大きな表を隠す Refine-ID タイプ Dev ideal Dev ideal target 数 X-RAY DIFFRACTION r_bond_refined_d0.021 0.022 949 X-RAY DIFFRACTION r_angle_refined_deg1.855 2.017 1280 X-RAY DIFFRACTION r_dihedral_angle_1_deg6.084 5 119 X-RAY DIFFRACTION r_dihedral_angle_2_deg36.48 24.211 38 X-RAY DIFFRACTION r_dihedral_angle_3_deg15.701 15 174 X-RAY DIFFRACTION r_dihedral_angle_4_deg23.688 15 8 X-RAY DIFFRACTION r_chiral_restr0.127 0.2 147 X-RAY DIFFRACTION r_gen_planes_refined0.008 0.02 680 X-RAY DIFFRACTION r_nbd_refined0.224 0.2 409 X-RAY DIFFRACTION r_nbtor_refined0.306 0.2 630 X-RAY DIFFRACTION r_xyhbond_nbd_refined0.157 0.2 57 X-RAY DIFFRACTION r_symmetry_vdw_refined0.193 0.2 61 X-RAY DIFFRACTION r_symmetry_hbond_refined0.185 0.2 18 X-RAY DIFFRACTION r_mcbond_it1.197 1.5 620 X-RAY DIFFRACTION r_mcangle_it1.586 2 954 X-RAY DIFFRACTION r_scbond_it2.517 3 366 X-RAY DIFFRACTION r_scangle_it3.522 4.5 325
LS精密化 シェル 解像度 : 1.695→1.739 Å / Total num. of bins used : 20 Rfactor 反射数 %反射 Rfree 0.304 50 - Rwork 0.275 819 - obs - 869 88.04 %
精密化 TLS 手法 : refined / Refine-ID : X-RAY DIFFRACTION
大きな表を表示 (25 x 20) 大きな表を隠す ID L11 (°2 )L12 (°2 )L13 (°2 )L22 (°2 )L23 (°2 )L33 (°2 )S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T11 (Å2 )T12 (Å2 )T13 (Å2 )T22 (Å2 )T23 (Å2 )T33 (Å2 )Origin x (Å)Origin y (Å)Origin z (Å)1 12.9066 -13.5821 14.163 17.8803 -19.2327 20.7643 -0.3746 0.0261 0.9489 -0.7892 0.2088 -1.3041 -0.1425 -0.2549 0.1658 0.2231 -0.0518 -0.0232 0.4078 -0.0307 0.154 7.3576 26.8831 37.1636 2 13.2737 0.0727 -8.1562 20.3227 17.675 28.1966 -0.1633 -0.2622 -0.0662 0.0498 0.2426 0.1505 -0.1612 0.7258 -0.0793 -0.1033 -0.0084 -0.0168 0.1904 -0.0069 -0.0482 6.7982 21.7914 45.302 3 9.3726 7.245 1.3449 6.855 0.4793 12.933 0.0856 0.2685 0.0384 0.1954 0.2467 -0.4374 -0.7362 0.6953 -0.3323 -0.0229 -0.0051 0.0071 0.2022 -0.0614 0.0855 3.9467 23.1762 48.3324 4 4.7532 0.6105 2.3904 6.1099 -1.8386 8.1761 -0.0408 0.7642 -0.2689 0.0549 0.1725 -0.1138 -0.0394 -0.1484 -0.1317 -0.1169 -0.0231 0.0061 0.2711 -0.0097 -0.0138 -3.9808 16.9471 42.2335 5 16.5673 0.5664 0.055 2.214 -4.039 7.4406 -0.1473 0.1849 -0.4405 0.4881 -0.1451 -0.1384 -0.0714 -0.4815 0.2925 0.0923 -0.0243 -0.0192 0.123 -0.0565 0.1906 -0.7236 10.5206 45.0899 6 28.8005 8.0577 -1.9649 13.9404 -0.0483 0.1556 -0.0632 -0.5675 -1.4692 0.844 -1.0266 -1.2429 0.279 -0.1177 1.0898 0.0863 -0.0612 -0.0162 0.1898 0.1652 0.2933 7.3915 9.3172 45.3338 7 14.5873 -8.8213 2.6744 11.8728 0.9489 11.6354 0.2676 -0.4584 -0.4413 -0.4999 -0.1294 0.0052 0.3751 -0.5615 -0.1382 -0.0968 -0.0381 0.0109 0.2048 -0.0397 0.0342 8.3899 16.4463 38.3768 8 24.095 -13.0466 4.923 20.7329 -2.5137 6.1603 -0.7412 1.1667 1.3343 0.6058 0.1374 0.3117 -1.1787 0.769 0.6038 0.1121 -0.1013 0.0126 0.2056 0.0875 0.0241 -0.7452 28.8822 35.7965 9 18.4751 -13.7457 -2.1925 19.8453 1.0725 1.332 0.1218 0.1934 0.1337 -0.3209 0.282 0.0917 -0.184 0.0532 -0.4039 -0.0156 -0.0332 0.0102 0.1743 0.0728 -0.0242 1.0874 20.8352 35.0573 10 35.3731 -28.1814 -28.2285 33.79 26.7686 45.3598 -0.5634 -1.3423 -0.7284 0.0719 0.93 -0.1551 2.5907 1.5565 -0.3667 0.1516 0.0797 -0.0642 0.0746 0.0294 0.0905 15.6629 10.4009 30.6515 11 12.6156 5.4589 12.0255 8.7995 8.831 17.3913 -0.0959 0.5752 1.0024 -0.0915 -0.4061 0.2079 -1.2719 0.3139 0.5019 0.1633 0.0058 0.0587 0.0542 0.0906 0.0216 16.6456 22.5856 22.4078 12 33.9314 -12.6316 -6.4568 10.9103 -13.715 43.08 0.0461 1.1932 0.7989 0.6031 -0.0056 -0.6018 -0.9875 -0.6959 -0.0405 0.1042 0.0966 0.0282 0.0856 0.0913 0 16.0705 17.9436 14.267 13 15.6488 -16.9718 0.3337 44.9234 -17.5266 20.4758 -0.3129 0.1363 1.0223 0.6892 0.7302 -0.7914 -0.8909 -0.2203 -0.4173 0.0034 0.015 0.0086 0.0612 -0.0496 0.0097 20.8172 16.1449 13.0645 14 2.011 -1.3111 2.2386 15.2766 6.0445 17.4652 -0.1294 0.0436 0.4076 0.4855 0.2567 -0.9176 0.9304 0.2932 -0.1273 0.0349 0.0614 -0.0165 0.0363 -0.0588 -0.0118 24.4629 10.5523 20.948 15 19.7788 -10.7712 3.0966 9.6567 0.2806 2.2689 -0.2773 0.3909 0.1609 0.1468 -0.1397 0.1669 -0.6728 -0.0783 0.417 0.395 -0.0359 -0.03 -0.0976 -0.0159 -0.0675 19.0379 4.7905 17.8246 16 21.0896 -11.3942 -13.2774 28.0267 1.9378 9.6125 -0.5469 -0.2219 -0.839 -1.6589 -0.1461 1.5216 0.6392 -1.1315 0.693 0.3303 0.1041 -0.1468 -0.0794 -0.0604 -0.0006 10.9449 6.4254 17.6225 17 12.4803 5.1281 2.9704 9.3312 2.686 11.9168 0.2469 -0.1829 -0.3193 -0.6692 -0.1397 -0.1517 -0.0597 -0.6861 -0.1072 0.0459 0.0917 -0.0341 0.033 -0.0051 -0.0307 11.9388 14.1089 23.152 18 6.9396 2.6453 8.7196 15.8916 -0.6897 15.4734 -0.5122 0.9798 0.1417 -0.3947 0.3818 -1.4598 -1.1929 1.115 0.1303 0.2287 -0.0355 0.0805 0.1722 0.0056 0.2107 25.445 23.2812 25.761 19 40.4566 10.4188 -5.4086 8.943 -1.3573 7.9639 -0.2069 -0.3521 0.1249 -0.639 0.1078 -0.0408 -0.1076 0.4958 0.0992 0.0882 0.0144 0.0148 0.1133 -0.0231 0.0071 19.9279 15.946 27.4603 20 80.5526 8.7094 -29.0257 6.059 0.2414 13.8523 -0.6959 -0.2344 -1.9443 0.1628 -0.082 -0.3709 1.8233 -0.2013 0.7779 0.1087 -0.093 0.007 0.2323 -0.0029 0.0631 3.4196 12.9812 31.4917
精密化 TLSグループ Refine-ID : X-RAY DIFFRACTION / Selection : ALL
大きな表を表示 (6 x 20) 大きな表を隠す ID Refine TLS-ID Auth asym-ID Label asym-ID Auth seq-ID Label seq-ID 1 1 AA1 - 5 1 - 5 2 2 AA6 - 10 6 - 10 3 3 AA11 - 16 11 - 16 4 4 AA17 - 25 17 - 25 5 5 AA26 - 31 26 - 31 6 6 AA32 - 37 32 - 37 7 7 AA38 - 42 38 - 42 8 8 AA43 - 47 43 - 47 9 9 AA48 - 54 48 - 54 10 10 AA55 - 59 55 - 59 11 11 BB1 - 6 1 - 6 12 12 BB7 - 11 7 - 11 13 13 BB12 - 17 12 - 17 14 14 BB18 - 25 18 - 25 15 15 BB26 - 31 26 - 31 16 16 BB32 - 36 32 - 36 17 17 BB37 - 42 37 - 42 18 18 BB43 - 48 43 - 48 19 19 BB49 - 54 49 - 54 20 20 BB55 - 60 55 - 60