Details | Solution-ID | Contents | Solvent system |
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1 | 1.2 mM Duck HBV apical loop, 10 mM sodium phosphate buffer, 0.1 mM EDTA, 95% H2O, 5% D2O, 95% H2O/5% D2O95% H2O/5% D2O2 | 1.2 mM Duck HBV apical loop, 10 mM sodium phosphate buffer, 0.1 mM EDTA, 100% D2O, 100% D2O100% D2O3 | 1 mM [U-13C; U-15N]-Ura Duck HBV apical loop, 10 mM sodium phosphate buffer, 0.1 mM EDTA, 5% D2O, 95% H2O, 95% H2O/5% D2O | 95% H2O/5% D2O4 | 1 mM [U-13C; U-15N]-Ura Duck HBV apical loop, 10 mM sodium phosphate buffer, 0.1 mM EDTA, 100% D2O, 100% D2O | 100% D2O5 | 0.7 mM [U-13C; U-15N] Duck HBV apical loop, 10 mM sodium phosphate buffer, 0.1 mM EDTA, 5% D2O, 95% H2O, 1 mM DSS, 95% H2O/5% D2O | 95% H2O/5% D2O6 | 0.7 mM [U-13C; U-15N] Duck HBV apical loop, 10 mM sodium phosphate buffer, 0.1 mM EDTA, 5% D2O, 95% H2O, 15 mg/mL Pf1 phage, 95% H2O/5% D2O | 95% H2O/5% D2O | | | | | | | |
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Sample | Conc. (mg/ml) | Component | Isotopic labeling | Solution-ID |
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1.2 mMDuck HBV apical loop | 1 | 10 mMsodium phosphate buffer | 1 | 0.1 mMEDTA | 1 | 95 %H2O | 1 | 5 %D2O | 1 | 1.2 mMDuck HBV apical loop | 2 | 10 mMsodium phosphate buffer | 2 | 0.1 mMEDTA | 2 | 100 %D2O | 2 | 1 mMDuck HBV apical loop[U-13C; U-15N]-Ura | 3 | 10 mMsodium phosphate buffer | 3 | 0.1 mMEDTA | 3 | 5 %D2O | 3 | 95 %H2O | 3 | 1 mMDuck HBV apical loop[U-13C; U-15N]-Ura | 4 | 10 mMsodium phosphate buffer | 4 | 0.1 mMEDTA | 4 | 100 %D2O | 4 | 0.7 mMDuck HBV apical loop[U-13C; U-15N] | 5 | 10 mMsodium phosphate buffer | 5 | 0.1 mMEDTA | 5 | 5 | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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