SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN ... SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN THE SHEET RECORDS BELOW, TWO SHEETS ARE DEFINED.
THE FIRST 21 RESIDUES OF THE GENE CORRESPOND TO A SIGNAL PEPTIDE SEQUENCE AND WERE NOT CLONED INTO ...THE FIRST 21 RESIDUES OF THE GENE CORRESPOND TO A SIGNAL PEPTIDE SEQUENCE AND WERE NOT CLONED INTO THE VECTOR. NUMBERING IN THE PDB CORRESPONDS TO THE FULL LENGTH GENE ( IE. STARTS AT GLN22). THE FIRST 10 RESIDUES OF THE SEQUENCE CRYSTALLISED CORRESPOND TO A HIS TAG INTRODUCED DURING THE CLONING PROCEDURE.
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2.9 Å3/Da / 溶媒含有率: 58 % / 解説: NONE
結晶化
詳細: 18-22% POLYETHYLENE GLYCOL 3350, 0.02 M SODIUM/POTASSIUM PHOSPHATE
解像度: 1.7→100.5 Å / Cor.coef. Fo:Fc: 0.966 / Cor.coef. Fo:Fc free: 0.954 / SU B: 1.602 / SU ML: 0.054 / 交差検証法: THROUGHOUT / ESU R: 0.09 / ESU R Free: 0.09 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.187
9229
5 %
RANDOM
Rwork
0.155
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obs
0.157
174582
99.7 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK