ENGINEERED RESIDUE IN CHAIN A, GLU 57 TO ARG ENGINEERED RESIDUE IN CHAIN A, TYR 148 TO LYS ...ENGINEERED RESIDUE IN CHAIN A, GLU 57 TO ARG ENGINEERED RESIDUE IN CHAIN A, TYR 148 TO LYS ENGINEERED RESIDUE IN CHAIN A, ARG 184 TO GLU ENGINEERED RESIDUE IN CHAIN B, GLU 57 TO ARG ENGINEERED RESIDUE IN CHAIN B, TYR 148 TO LYS ENGINEERED RESIDUE IN CHAIN B, ARG 184 TO GLU ENGINEERED RESIDUE IN CHAIN C, GLU 57 TO ARG ENGINEERED RESIDUE IN CHAIN C, TYR 148 TO LYS ENGINEERED RESIDUE IN CHAIN C, ARG 184 TO GLU ENGINEERED RESIDUE IN CHAIN D, GLU 57 TO ARG ENGINEERED RESIDUE IN CHAIN D, TYR 148 TO LYS ENGINEERED RESIDUE IN CHAIN D, ARG 184 TO GLU
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 4.2 Å3/Da / 溶媒含有率: 70 %
結晶化
pH: 7.6 / 詳細: pH 7.60
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データ収集
回折
平均測定温度: 100 K
放射光源
由来: シンクロトロン / サイト: SLS / ビームライン: X06SA / 波長: 0.82
検出器
タイプ: MARRESEARCH / 検出器: CCD
放射
プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 0.82 Å / 相対比: 1
反射
解像度: 2.1→100 Å / Num. obs: 123872 / % possible obs: 99.8 % / Observed criterion σ(I): 2 / 冗長度: 3.9 % / Rmerge(I) obs: 0.06 / Net I/σ(I): 14.9