Text: Constraints for structure calculations were collected from standard homonuclear NMR experiments. Site-specific imino-assignments were obtained from 1D HMQC with presaturation. 2D NOESY in water ...Text: Constraints for structure calculations were collected from standard homonuclear NMR experiments. Site-specific imino-assignments were obtained from 1D HMQC with presaturation. 2D NOESY in water used jump-and-return solvent suppression. The average RMSD is 0.880531.
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内容
溶媒系
1
0.2-3mM DNA oligonucleotides, 25mM potassium-phosphate,70mM potassium-chloride,pH7.0 buffer, 10% D2O/90% H2O
10% D2O/90% H2O
2
0.2-3mM DNA oligonucleotides, 25mM potassium-phosphate,70mM potassium-chloride,pH7.0 buffer, 99.96% D2O