SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN ... SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN THE SHEET RECORDS BELOW, TWO SHEETS ARE DEFINED.
THE STRAIN USED IN THIS WORK HAS NOT BEEN DEPOSITED WITH A SEQUENCE DATABASE, BUT IS EXTREMELY ...THE STRAIN USED IN THIS WORK HAS NOT BEEN DEPOSITED WITH A SEQUENCE DATABASE, BUT IS EXTREMELY CLOSE TO UNIPROT ENTRY Q83WA5. ALL SEQUENCE DIFFERENCES OCCUR IN THE N-TERMINAL PART OF THE MOLECULE, WHICH IS COMPLETELY DISORDERED IN THIS STRUCTURE.
モノクロメーター: CRYSTAL / プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 0.933 Å / 相対比: 1
反射
解像度: 1.36→40 Å / Num. obs: 48836 / % possible obs: 99.3 % / Observed criterion σ(I): 0 / 冗長度: 18.5 % / Rmerge(I) obs: 0.05 / Net I/σ(I): 35.4
反射 シェル
解像度: 1.36→1.45 Å / 冗長度: 9.9 % / Rmerge(I) obs: 0.45 / Mean I/σ(I) obs: 4.24 / % possible all: 96
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解析
ソフトウェア
名称
バージョン
分類
REFMAC
5.2.0005
精密化
XDS
データ削減
XSCALE
データスケーリング
autoSHARP
位相決定
精密化
構造決定の手法: 単一同系置換・異常分散 / 解像度: 1.36→81.65 Å / Cor.coef. Fo:Fc: 0.969 / Cor.coef. Fo:Fc free: 0.969 / SU B: 0.669 / SU ML: 0.027 / 交差検証法: THROUGHOUT / ESU R: 0.042 / ESU R Free: 0.042 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. 79 N-TERMINAL RESIDUES AND 5 C-TERMINAL RESIDUES (HIS-TAG) ARE DISORDERED
Rfactor
反射数
%反射
Selection details
Rfree
0.19
2474
5.1 %
RANDOM
Rwork
0.179
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obs
0.179
46407
99.3 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK