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- PDB-1d97: CHIRAL PHOSPHOROTHIOATE ANALOGUES OF B-DNA: THE CRYSTAL STRUCTURE... -
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Open data
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Basic information
Entry | Database: PDB / ID: 1d97 | ||||||||||||||||||
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Title | CHIRAL PHOSPHOROTHIOATE ANALOGUES OF B-DNA: THE CRYSTAL STRUCTURE OF RP-D(GP(S) CPGP(S)CPGP(S)C) | ||||||||||||||||||
![]() | DNA (5'-D(RP*![]() DNA / B-DNA / DOUBLE HELIX / MODIFIED | Function / homology | DNA | ![]() Method | ![]() ![]() Cruse, W.B.T. / Salisbury, S.A. / Brown, T. / Cosstick, R. / Eckstein, F. / Kennard, O. | ![]() ![]() Title: Chiral phosphorothioate analogues of B-DNA. The crystal structure of Rp-d[Gp(S)CpGp(S)CpGp(S)C]. Authors: Cruse, W.B. / Salisbury, S.A. / Brown, T. / Cosstick, R. / Eckstein, F. / Kennard, O. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 14.5 KB | Display | ![]() |
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PDB format | ![]() | 10.1 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 331.8 KB | Display | ![]() |
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Full document | ![]() | 333.2 KB | Display | |
Data in XML | ![]() | 2.3 KB | Display | |
Data in CIF | ![]() | 3.1 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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Unit cell |
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Components
#1: DNA chain | Mass: 1858.403 Da / Num. of mol.: 2 / Source method: obtained synthetically #2: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 1.9 Å3/Da / Density % sol: 35.16 % | ||||||||||||||||||||||||||||||||||||||||||
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Crystal grow | Temperature: 287 K / Method: vapor diffusion / Details: VAPOR DIFFUSION, temperature 287.00K | ||||||||||||||||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS Temperature: 14 ℃ / Method: vapor diffusion | ||||||||||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 291 K |
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Detector | Type: SYNTEX P21 / Detector: DIFFRACTOMETER |
Radiation | Scattering type: x-ray |
Radiation wavelength | Relative weight: 1 |
Reflection | Resolution: 2.17→25 Å / Num. obs: 1954 |
Reflection | *PLUS Highest resolution: 2.17 Å / Lowest resolution: 25 Å / Rmerge(I) obs: 0.24 |
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Processing
Software | Name: NUCLSQ / Classification: refinement | ||||||||||||
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Refinement | Resolution: 2.17→8 Å / σ(F): 2 /
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Refine Biso |
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Refinement step | Cycle: LAST / Resolution: 2.17→8 Å
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Refinement | *PLUS Highest resolution: 2.17 Å / Lowest resolution: 8 Å / σ(F): 2 / Num. reflection obs: 1327 / Rfactor obs: 0.145 | ||||||||||||
Solvent computation | *PLUS | ||||||||||||
Displacement parameters | *PLUS |