PDB-9v7h: Phycobilisome rod R2 from Gloeobacter violaceus PCC 7421

基本情報

• 登録情報: データベース: PDB / ID: 9v7h
• タイトル: Phycobilisome rod R2 from Gloeobacter violaceus PCC 7421

要素

• (Phycocyanin-associated rod linker ...) x 2
• Glr1262 protein
• Phycocyanin alpha chain
• Phycocyanin beta chain

• キーワード: PHOTOSYNTHESIS / Phycobilisome

機能・相同性

分子機能:

phycobilisome / plasma membrane-derived thylakoid membrane / photosynthesis

ドメイン・相同性:

Phycobilisome linker domain / Phycobilisome linker domain superfamily / Phycobilisome Linker polypeptide / Phycobilisome (PBS) linker domain profile. / Phycobilisome, alpha/beta subunit / Phycobilisome, alpha/beta subunit superfamily / Phycobilisome protein / Globin-like superfamily

構成要素:

PHYCOCYANOBILIN / Phycocyanin beta chain / Phycocyanin alpha chain / Glr1262 protein

• 生物種: Gloeobacter violaceus PCC 7421 (バクテリア)
• 手法: 電子顕微鏡法 / 単粒子再構成法 / クライオ電子顕微鏡法 / 解像度: 2.95 Å
• データ登録者: Burtseva, A.D. / Baymukhametov, T.N. / Slonimskiy, Y.B. / Popov, V.O. / Sluchanko, N.N. / Boyko, K.M.

資金援助

ロシア, 1件

組織	認可番号	国
Russian Science Foundation	23-74-00062	ロシア

• 引用: ジャーナル: To Be Published; タイトル: Structure and quenching of a bundle-shaped phycobilisome; 著者: Burtseva, A.D. / Slonimskiy, Y.B. / Baymukhametov, T.N. / Sinetova, M.A. / Maksimov, E.G. / Popov, V.O. / Boyko, K.M. / Sluchanko, N.N.

履歴

登録	2025年5月28日	登録サイト: PDBJ / 処理サイト: PDBJ
改定 1.0	2025年9月24日	Provider: repository / タイプ: Initial release
改定 1.0	2025年9月24日	Data content type: EM metadata / Data content type: EM metadata / Provider: repository / タイプ: Initial release
改定 1.0	2025年9月24日	Data content type: Half map / Part number: 1 / Data content type: Half map / Provider: repository / タイプ: Initial release
改定 1.0	2025年9月24日	Data content type: Half map / Part number: 2 / Data content type: Half map / Provider: repository / タイプ: Initial release
改定 1.0	2025年9月24日	Data content type: Image / Data content type: Image / Provider: repository / タイプ: Initial release
改定 1.0	2025年9月24日	Data content type: Primary map / Data content type: Primary map / Provider: repository / タイプ: Initial release

集合体

登録構造単位

A: Phycocyanin-associated rod linker protein

B: Phycocyanin beta chain

C: Phycocyanin alpha chain

D: Phycocyanin beta chain

E: Phycocyanin alpha chain

F: Phycocyanin beta chain

G: Phycocyanin alpha chain

H: Phycocyanin beta chain

I: Phycocyanin alpha chain

J: Phycocyanin beta chain

K: Phycocyanin alpha chain

L: Phycocyanin beta chain

M: Phycocyanin-associated rod linker protein

N: Phycocyanin alpha chain

O: Phycocyanin beta chain

P: Phycocyanin alpha chain

Q: Phycocyanin beta chain

R: Phycocyanin alpha chain

S: Phycocyanin beta chain

T: Phycocyanin alpha chain

U: Phycocyanin beta chain

V: Phycocyanin alpha chain

W: Phycocyanin beta chain

X: Phycocyanin alpha chain

Y: Phycocyanin beta chain

Z: Glr1262 protein

a: Phycocyanin alpha chain

ヘテロ分子

概要:

• 609 kDa, 27 ポリマー

構成要素の詳細:

	分子量 (理論値)	分子数
合計 (水以外)	609,225	63
ポリマ－	588,032	27
非ポリマー	21,193	36
水	0	0

1

概要:

• 登録構造と同一
• 登録者が定義した集合体
• 根拠: 電子顕微鏡法, not applicable

対称操作:

タイプ	名称	対称操作	数
identity operation	1_555		1

非結晶学的対称性 (NCS)

NCSドメイン:

ID	Ens-ID	詳細
1	1	A
2	1	A
3	2	A
4	2	A
5	3	A
6	3	A
7	4	A
8	4	A
9	5	A
10	5	A
11	6	A
12	6	A
13	7	A
14	7	A
15	8	A
16	8	A
17	9	A
18	9	A
19	10	A
20	10	A
21	11	A
22	11	A
23	12	A
24	12	A
25	13	A
26	13	A
27	14	A
28	14	A
29	15	A
30	15	A
31	16	A
32	16	A
33	17	A
34	17	A
35	18	A
36	18	A
37	19	A
38	19	A
39	20	A
40	20	A
41	21	A
42	21	A
43	22	A
44	22	A
45	23	A
46	23	A
47	24	A
48	24	A
49	25	A
50	25	A
51	26	A
52	26	A
53	27	A
54	27	A
55	28	A
56	28	A
57	29	A
58	29	A
59	30	A
60	30	A
61	31	A
62	31	A
63	32	A
64	32	A
65	33	A
66	33	A
67	34	A
68	34	A
69	35	A
70	35	A
71	36	A
72	36	A
73	37	A
74	37	A
75	38	A
76	38	A
77	39	A
78	39	A
79	40	A
80	40	A
81	41	A
82	41	A
83	42	A
84	42	A
85	43	A
86	43	A
87	44	A
88	44	A
89	45	A
90	45	A
91	46	A
92	46	A
93	47	A
94	47	A
95	48	A
96	48	A
97	49	A
98	49	A
99	50	A
100	50	A
101	51	A
102	51	A
103	52	A
104	52	A
105	53	A
106	53	A
107	54	A
108	54	A
109	55	A
110	55	A
111	56	A
112	56	A
113	57	A
114	57	A
115	58	A
116	58	A
117	59	A
118	59	A
119	60	A
120	60	A
121	61	A
122	61	A
123	62	A
124	62	A
125	63	A
126	63	A
127	64	A
128	64	A
129	65	A
130	65	A
131	66	A
132	66	A
133	67	A
134	67	A
135	68	A
136	68	A
137	69	A
138	69	A
139	70	A
140	70	A
141	71	A
142	71	A
143	72	A
144	72	A
145	73	A
146	73	A
147	74	A
148	74	A
149	75	A
150	75	A
151	76	A
152	76	A
153	77	A
154	77	A
155	78	A
156	78	A
157	79	A
158	79	A
159	80	A
160	80	A
161	81	A
162	81	A
163	82	A
164	82	A
165	83	A
166	83	A
167	84	A
168	84	A
169	85	A
170	85	A
171	86	A
172	86	A
173	87	A
174	87	A
175	88	A
176	88	A
177	89	A
178	89	A
179	90	A
180	90	A
181	91	A
182	91	A
183	92	A
184	92	A
185	93	A
186	93	A
187	94	A
188	94	A
189	95	A
190	95	A
191	96	A
192	96	A
193	97	A
194	97	A
195	98	A
196	98	A
197	99	A
198	99	A
199	100	A
200	100	A
201	101	A
202	101	A
203	102	A
204	102	A
205	103	A
206	103	A
207	104	A
208	104	A
209	105	A
210	105	A
211	106	A
212	106	A
213	107	A
214	107	A
215	108	A
216	108	A
217	109	A
218	109	A
219	110	A
220	110	A
221	111	A
222	111	A
223	112	A
224	112	A
225	113	A
226	113	A
227	114	A
228	114	A
229	115	A
230	115	A
231	116	A
232	116	A
233	117	A
234	117	A
235	118	A
236	118	A
237	119	A
238	119	A
239	120	A
240	120	A
241	121	A
242	121	A
243	122	A
244	122	A
245	123	A
246	123	A
247	124	A
248	124	A
249	125	A
250	125	A
251	126	A
252	126	A
253	127	A
254	127	A
255	128	A
256	128	A
257	129	A
258	129	A
259	130	A
260	130	A
261	131	A
262	131	A
263	132	A
264	132	A

NCSアンサンブル:

ID	詳細
1	Local NCS retraints between domains: 1 2
2	Local NCS retraints between domains: 3 4
3	Local NCS retraints between domains: 5 6
4	Local NCS retraints between domains: 7 8
5	Local NCS retraints between domains: 9 10
6	Local NCS retraints between domains: 11 12
7	Local NCS retraints between domains: 13 14
8	Local NCS retraints between domains: 15 16
9	Local NCS retraints between domains: 17 18
10	Local NCS retraints between domains: 19 20
11	Local NCS retraints between domains: 21 22
12	Local NCS retraints between domains: 23 24
13	Local NCS retraints between domains: 25 26
14	Local NCS retraints between domains: 27 28
15	Local NCS retraints between domains: 29 30
16	Local NCS retraints between domains: 31 32
17	Local NCS retraints between domains: 33 34
18	Local NCS retraints between domains: 35 36
19	Local NCS retraints between domains: 37 38
20	Local NCS retraints between domains: 39 40
21	Local NCS retraints between domains: 41 42
22	Local NCS retraints between domains: 43 44
23	Local NCS retraints between domains: 45 46
24	Local NCS retraints between domains: 47 48
25	Local NCS retraints between domains: 49 50
26	Local NCS retraints between domains: 51 52
27	Local NCS retraints between domains: 53 54
28	Local NCS retraints between domains: 55 56
29	Local NCS retraints between domains: 57 58
30	Local NCS retraints between domains: 59 60
31	Local NCS retraints between domains: 61 62
32	Local NCS retraints between domains: 63 64
33	Local NCS retraints between domains: 65 66
34	Local NCS retraints between domains: 67 68
35	Local NCS retraints between domains: 69 70
36	Local NCS retraints between domains: 71 72
37	Local NCS retraints between domains: 73 74
38	Local NCS retraints between domains: 75 76
39	Local NCS retraints between domains: 77 78
40	Local NCS retraints between domains: 79 80
41	Local NCS retraints between domains: 81 82
42	Local NCS retraints between domains: 83 84
43	Local NCS retraints between domains: 85 86
44	Local NCS retraints between domains: 87 88
45	Local NCS retraints between domains: 89 90
46	Local NCS retraints between domains: 91 92
47	Local NCS retraints between domains: 93 94
48	Local NCS retraints between domains: 95 96
49	Local NCS retraints between domains: 97 98
50	Local NCS retraints between domains: 99 100
51	Local NCS retraints between domains: 101 102
52	Local NCS retraints between domains: 103 104
53	Local NCS retraints between domains: 105 106
54	Local NCS retraints between domains: 107 108
55	Local NCS retraints between domains: 109 110
56	Local NCS retraints between domains: 111 112
57	Local NCS retraints between domains: 113 114
58	Local NCS retraints between domains: 115 116
59	Local NCS retraints between domains: 117 118
60	Local NCS retraints between domains: 119 120
61	Local NCS retraints between domains: 121 122
62	Local NCS retraints between domains: 123 124
63	Local NCS retraints between domains: 125 126
64	Local NCS retraints between domains: 127 128
65	Local NCS retraints between domains: 129 130
66	Local NCS retraints between domains: 131 132
67	Local NCS retraints between domains: 133 134
68	Local NCS retraints between domains: 135 136
69	Local NCS retraints between domains: 137 138
70	Local NCS retraints between domains: 139 140
71	Local NCS retraints between domains: 141 142
72	Local NCS retraints between domains: 143 144
73	Local NCS retraints between domains: 145 146
74	Local NCS retraints between domains: 147 148
75	Local NCS retraints between domains: 149 150
76	Local NCS retraints between domains: 151 152
77	Local NCS retraints between domains: 153 154
78	Local NCS retraints between domains: 155 156
79	Local NCS retraints between domains: 157 158
80	Local NCS retraints between domains: 159 160
81	Local NCS retraints between domains: 161 162
82	Local NCS retraints between domains: 163 164
83	Local NCS retraints between domains: 165 166
84	Local NCS retraints between domains: 167 168
85	Local NCS retraints between domains: 169 170
86	Local NCS retraints between domains: 171 172
87	Local NCS retraints between domains: 173 174
88	Local NCS retraints between domains: 175 176
89	Local NCS retraints between domains: 177 178
90	Local NCS retraints between domains: 179 180
91	Local NCS retraints between domains: 181 182
92	Local NCS retraints between domains: 183 184
93	Local NCS retraints between domains: 185 186
94	Local NCS retraints between domains: 187 188
95	Local NCS retraints between domains: 189 190
96	Local NCS retraints between domains: 191 192
97	Local NCS retraints between domains: 193 194
98	Local NCS retraints between domains: 195 196
99	Local NCS retraints between domains: 197 198
100	Local NCS retraints between domains: 199 200
101	Local NCS retraints between domains: 201 202
102	Local NCS retraints between domains: 203 204
103	Local NCS retraints between domains: 205 206
104	Local NCS retraints between domains: 207 208
105	Local NCS retraints between domains: 209 210
106	Local NCS retraints between domains: 211 212
107	Local NCS retraints between domains: 213 214
108	Local NCS retraints between domains: 215 216
109	Local NCS retraints between domains: 217 218
110	Local NCS retraints between domains: 219 220
111	Local NCS retraints between domains: 221 222
112	Local NCS retraints between domains: 223 224
113	Local NCS retraints between domains: 225 226
114	Local NCS retraints between domains: 227 228
115	Local NCS retraints between domains: 229 230
116	Local NCS retraints between domains: 231 232
117	Local NCS retraints between domains: 233 234
118	Local NCS retraints between domains: 235 236
119	Local NCS retraints between domains: 237 238
120	Local NCS retraints between domains: 239 240
121	Local NCS retraints between domains: 241 242
122	Local NCS retraints between domains: 243 244
123	Local NCS retraints between domains: 245 246
124	Local NCS retraints between domains: 247 248
125	Local NCS retraints between domains: 249 250
126	Local NCS retraints between domains: 251 252
127	Local NCS retraints between domains: 253 254
128	Local NCS retraints between domains: 255 256
129	Local NCS retraints between domains: 257 258
130	Local NCS retraints between domains: 259 260
131	Local NCS retraints between domains: 261 262
132	Local NCS retraints between domains: 263 264

要素

Phycocyanin-associated rod linker ... , 2種, 2分子 A M

#1: タンパク質

A Phycocyanin-associated rod linker protein

詳細:

分子量: 31085.066 Da / 分子数: 1 / 由来タイプ: 天然
由来: (天然) Gloeobacter violaceus PCC 7421 (バクテリア)

#4: タンパク質

M Phycocyanin-associated rod linker protein

詳細:

分子量: 30913.822 Da / 分子数: 1 / 由来タイプ: 天然
由来: (天然) Gloeobacter violaceus PCC 7421 (バクテリア)

タンパク質 , 3種, 25分子 B D F H J L O Q S U W Y C E G I K N P R T V X a Z

#2: タンパク質

B D F H J L O Q S U W Y
Phycocyanin beta chain

詳細:

分子量: 18478.953 Da / 分子数: 12 / 由来タイプ: 天然
由来: (天然) Gloeobacter violaceus PCC 7421 (バクテリア)
参照: UniProt: Q7M7C7

#3: タンパク質

C E G I K N P R T V X a
Phycocyanin alpha chain

詳細:

分子量: 17679.852 Da / 分子数: 12 / 由来タイプ: 天然
由来: (天然) Gloeobacter violaceus PCC 7421 (バクテリア)
参照: UniProt: Q7M7F7

#5: タンパク質

Z Glr1262 protein

詳細:

分子量: 92127.602 Da / 分子数: 1 / 由来タイプ: 天然
由来: (天然) Gloeobacter violaceus PCC 7421 (バクテリア)
参照: UniProt: Q7NL64

非ポリマー , 1種, 36分子

#6: 化合物

B-201 B-202 C-201 D-201 D-202 E-201 F-201 F-202 G-201 H-201 H-202 I-201 J-201 J-202 K-201 L-201 L-202 N-201 O-201 O-202 ...
ChemComp-CYC / PHYCOCYANOBILIN

詳細:

分子量: 588.694 Da / 分子数: 36 / 由来タイプ: 合成 / 式: C₃₃H₄₀N₄O₆ / タイプ: SUBJECT OF INVESTIGATION

詳細

• 研究の焦点であるリガンドがあるか: Y
• Has protein modification: Y

実験情報

実験

• 実験: 手法: 電子顕微鏡法
• EM実験: 試料の集合状態: PARTICLE / ３次元再構成法: 単粒子再構成法

試料調製

• 構成要素: 名称: Bundle-shaped phycobilisome / タイプ: COMPLEX / Entity ID: #1-#5 / 由来: NATURAL
• 由来(天然): 生物種: Gloeobacter violaceus PCC 7421 (バクテリア)
• 緩衝液: pH: 7
• 緩衝液成分: 濃度: 50 mM / 名称: Tris(hydroxymethyl)aminomethane hydrochloride / 式: Tris-HCl
• 試料: 包埋: NO / シャドウイング: NO / 染色: NO / 凍結: YES
• 急速凍結: 凍結剤: ETHANE

電子顕微鏡撮影

• 実験機器: モデル: Titan Krios / 画像提供: FEI Company
• 顕微鏡: モデル: TFS KRIOS / 詳細: Preliminary grid screening was performed manually.
• 電子銃: 電子線源: FIELD EMISSION GUN / 加速電圧: 300 kV / 照射モード: FLOOD BEAM
• 電子レンズ: モード: BRIGHT FIELD / 倍率（公称値）: 85000 X / 最大 デフォーカス（公称値）: 1600 nm / 最小 デフォーカス（公称値）: 600 nm / Cs: 0.01 mm / C2レンズ絞り径: 100 µm / アライメント法: ZEMLIN TABLEAU
• 試料ホルダ: 凍結剤: NITROGEN; 試料ホルダーモデル: FEI TITAN KRIOS AUTOGRID HOLDER
• 撮影: 平均露光時間: 3.9 sec. / 電子線照射量: 66 e/Ų; フィルム・検出器のモデル: GATAN K3 BIOQUANTUM (6k x 4k)
• 電子光学装置: エネルギーフィルター名称: GIF Bioquantum / エネルギーフィルタースリット幅: 20 eV; 球面収差補正装置: Microscope was modified with a Cs corrector (CEOS GmbH, Germany).
• 画像スキャン: 横: 5760 / 縦: 4092

解析

EMソフトウェア

ID	名称	バージョン	カテゴリ
2	SerialEM	4.04	画像取得
4	Warp	1.0.9	CTF補正
11	cryoSPARC	4.7	最終オイラー角割当
13	cryoSPARC	4.7	３次元再構成

• CTF補正: タイプ: NONE
• 対称性: 点対称性: C₁ (非対称)
• 3次元再構成: 解像度: 2.95 Å / 解像度の算出法: FSC 0.143 CUT-OFF / 粒子像の数: 207644 / 対称性のタイプ: POINT

精密化

解像度: 2.95→2.95 Å / Cor.coef. F_o:F_c: 0.948 / WR_factor R_work: 0.306 / SU B: 29.793 / SU ML: 0.499 / Average fsc free: 0 / Average fsc overall: 0.8174 / Average fsc work: 0.8174 / ESU R: 0.69 / 詳細: Hydrogens have been added in their riding positions

	Rfactor	反射数	%反射
Rwork	0.3064	217183	-
all	0.306	-	-
Rfree	-	-	0 %
obs	-	-	100 %

• 溶媒の処理: 溶媒モデル: NONE
• 原子変位パラメータ: B_iso mean: 45.623 Ų

拘束条件

Refine-ID	タイプ	Dev ideal	Dev ideal target	数
ELECTRON MICROSCOPY	r_bond_refined_d	0.008	0.012	37150
ELECTRON MICROSCOPY	r_bond_other_d	0.001	0.016	35230
ELECTRON MICROSCOPY	r_angle_refined_deg	1.737	1.814	50558
ELECTRON MICROSCOPY	r_angle_other_deg	0.666	1.748	80604
ELECTRON MICROSCOPY	r_dihedral_angle_1_deg	6.148	5	4548
ELECTRON MICROSCOPY	r_dihedral_angle_2_deg	15.698	8.529	918
ELECTRON MICROSCOPY	r_dihedral_angle_3_deg	16.86	10	5925
ELECTRON MICROSCOPY	r_dihedral_angle_6_deg	13.903	10	1608
ELECTRON MICROSCOPY	r_chiral_restr	0.07	0.2	5605
ELECTRON MICROSCOPY	r_gen_planes_refined	0.007	0.02	45952
ELECTRON MICROSCOPY	r_gen_planes_other	0.004	0.02	8594
ELECTRON MICROSCOPY	r_nbd_refined	0.318	0.2	11785
ELECTRON MICROSCOPY	r_symmetry_nbd_other	0.223	0.2	34891
ELECTRON MICROSCOPY	r_nbtor_refined	0.208	0.2	20133
ELECTRON MICROSCOPY	r_symmetry_nbtor_other	0.084	0.2	21017
ELECTRON MICROSCOPY	r_xyhbond_nbd_refined	0.178	0.2	1214
ELECTRON MICROSCOPY	r_symmetry_xyhbond_nbd_other	0.152	0.2	38
ELECTRON MICROSCOPY	r_mcbond_it	1.516	4.549	18273
ELECTRON MICROSCOPY	r_mcbond_other	1.516	4.549	18273
ELECTRON MICROSCOPY	r_mcangle_it	2.514	8.156	22794
ELECTRON MICROSCOPY	r_mcangle_other	2.514	8.156	22795
ELECTRON MICROSCOPY	r_scbond_it	1.54	4.649	18877
ELECTRON MICROSCOPY	r_scbond_other	1.54	4.648	18876
ELECTRON MICROSCOPY	r_scangle_it	2.758	8.468	27764
ELECTRON MICROSCOPY	r_scangle_other	2.758	8.468	27765
ELECTRON MICROSCOPY	r_lrange_it	4.476	41.25	47235
ELECTRON MICROSCOPY	r_lrange_other	4.476	41.25	47236
ELECTRON MICROSCOPY	r_ncsr_local_group_1	0.096	0.05	5350
ELECTRON MICROSCOPY	r_ncsr_local_group_2	0.082	0.05	5353
ELECTRON MICROSCOPY	r_ncsr_local_group_3	0.073	0.05	5441
ELECTRON MICROSCOPY	r_ncsr_local_group_4	0.082	0.05	5385
ELECTRON MICROSCOPY	r_ncsr_local_group_5	0.104	0.05	5312
ELECTRON MICROSCOPY	r_ncsr_local_group_6	0.045	0.05	5515
ELECTRON MICROSCOPY	r_ncsr_local_group_7	0.086	0.05	5381
ELECTRON MICROSCOPY	r_ncsr_local_group_8	0.08	0.05	5378
ELECTRON MICROSCOPY	r_ncsr_local_group_9	0.073	0.05	5437
ELECTRON MICROSCOPY	r_ncsr_local_group_10	0.083	0.05	5390
ELECTRON MICROSCOPY	r_ncsr_local_group_11	0.099	0.05	5304
ELECTRON MICROSCOPY	r_ncsr_local_group_12	0.057	0.05	5328
ELECTRON MICROSCOPY	r_ncsr_local_group_13	0.058	0.05	5354
ELECTRON MICROSCOPY	r_ncsr_local_group_14	0.075	0.05	5330
ELECTRON MICROSCOPY	r_ncsr_local_group_15	0.052	0.05	5336
ELECTRON MICROSCOPY	r_ncsr_local_group_16	0.088	0.05	5300
ELECTRON MICROSCOPY	r_ncsr_local_group_17	0.006	0.05	5435
ELECTRON MICROSCOPY	r_ncsr_local_group_18	0.058	0.05	5327
ELECTRON MICROSCOPY	r_ncsr_local_group_19	0.058	0.05	5355
ELECTRON MICROSCOPY	r_ncsr_local_group_20	0.074	0.05	5331
ELECTRON MICROSCOPY	r_ncsr_local_group_21	0.052	0.05	5333
ELECTRON MICROSCOPY	r_ncsr_local_group_22	0.088	0.05	5294
ELECTRON MICROSCOPY	r_ncsr_local_group_23	0.092	0.05	5316
ELECTRON MICROSCOPY	r_ncsr_local_group_24	0.09	0.05	5397
ELECTRON MICROSCOPY	r_ncsr_local_group_25	0.095	0.05	5350
ELECTRON MICROSCOPY	r_ncsr_local_group_26	0.103	0.05	5368
ELECTRON MICROSCOPY	r_ncsr_local_group_27	0.102	0.05	5335
ELECTRON MICROSCOPY	r_ncsr_local_group_28	0.053	0.05	5560
ELECTRON MICROSCOPY	r_ncsr_local_group_29	0.092	0.05	5343
ELECTRON MICROSCOPY	r_ncsr_local_group_30	0.09	0.05	5399
ELECTRON MICROSCOPY	r_ncsr_local_group_31	0.096	0.05	5358
ELECTRON MICROSCOPY	r_ncsr_local_group_32	0.097	0.05	5373
ELECTRON MICROSCOPY	r_ncsr_local_group_33	0.054	0.05	5349
ELECTRON MICROSCOPY	r_ncsr_local_group_34	0.07	0.05	5310
ELECTRON MICROSCOPY	r_ncsr_local_group_35	0.046	0.05	5363
ELECTRON MICROSCOPY	r_ncsr_local_group_36	0.083	0.05	5291
ELECTRON MICROSCOPY	r_ncsr_local_group_37	0.058	0.05	5317
ELECTRON MICROSCOPY	r_ncsr_local_group_38	0.005	0.05	5427
ELECTRON MICROSCOPY	r_ncsr_local_group_39	0.055	0.05	5352
ELECTRON MICROSCOPY	r_ncsr_local_group_40	0.07	0.05	5311
ELECTRON MICROSCOPY	r_ncsr_local_group_41	0.047	0.05	5358
ELECTRON MICROSCOPY	r_ncsr_local_group_42	0.084	0.05	5287
ELECTRON MICROSCOPY	r_ncsr_local_group_43	0.073	0.05	5399
ELECTRON MICROSCOPY	r_ncsr_local_group_44	0.069	0.05	5392
ELECTRON MICROSCOPY	r_ncsr_local_group_45	0.1	0.05	5305
ELECTRON MICROSCOPY	r_ncsr_local_group_46	0.087	0.05	5351
ELECTRON MICROSCOPY	r_ncsr_local_group_47	0.082	0.05	5339
ELECTRON MICROSCOPY	r_ncsr_local_group_48	0.011	0.05	5534
ELECTRON MICROSCOPY	r_ncsr_local_group_49	0.073	0.05	5404
ELECTRON MICROSCOPY	r_ncsr_local_group_50	0.07	0.05	5391
ELECTRON MICROSCOPY	r_ncsr_local_group_51	0.094	0.05	5308
ELECTRON MICROSCOPY	r_ncsr_local_group_52	0.077	0.05	5319
ELECTRON MICROSCOPY	r_ncsr_local_group_53	0.047	0.05	5365
ELECTRON MICROSCOPY	r_ncsr_local_group_54	0.084	0.05	5306
ELECTRON MICROSCOPY	r_ncsr_local_group_55	0.059	0.05	5346
ELECTRON MICROSCOPY	r_ncsr_local_group_56	0.055	0.05	5349
ELECTRON MICROSCOPY	r_ncsr_local_group_57	0.006	0.05	5436
ELECTRON MICROSCOPY	r_ncsr_local_group_58	0.077	0.05	5320
ELECTRON MICROSCOPY	r_ncsr_local_group_59	0.048	0.05	5357
ELECTRON MICROSCOPY	r_ncsr_local_group_60	0.084	0.05	5303
ELECTRON MICROSCOPY	r_ncsr_local_group_61	0.076	0.05	5426
ELECTRON MICROSCOPY	r_ncsr_local_group_62	0.102	0.05	5354
ELECTRON MICROSCOPY	r_ncsr_local_group_63	0.079	0.05	5406
ELECTRON MICROSCOPY	r_ncsr_local_group_64	0.083	0.05	5429
ELECTRON MICROSCOPY	r_ncsr_local_group_65	0.073	0.05	5424
ELECTRON MICROSCOPY	r_ncsr_local_group_66	0.006	0.05	5602
ELECTRON MICROSCOPY	r_ncsr_local_group_67	0.077	0.05	5433
ELECTRON MICROSCOPY	r_ncsr_local_group_68	0.097	0.05	5361
ELECTRON MICROSCOPY	r_ncsr_local_group_69	0.073	0.05	5322
ELECTRON MICROSCOPY	r_ncsr_local_group_70	0.089	0.05	5301
ELECTRON MICROSCOPY	r_ncsr_local_group_71	0.075	0.05	5329
ELECTRON MICROSCOPY	r_ncsr_local_group_72	0.072	0.05	5311
ELECTRON MICROSCOPY	r_ncsr_local_group_73	0.077	0.05	5316
ELECTRON MICROSCOPY	r_ncsr_local_group_74	0.007	0.05	5455
ELECTRON MICROSCOPY	r_ncsr_local_group_75	0.074	0.05	5314
ELECTRON MICROSCOPY	r_ncsr_local_group_76	0.089	0.05	5297
ELECTRON MICROSCOPY	r_ncsr_local_group_77	0.101	0.05	5356
ELECTRON MICROSCOPY	r_ncsr_local_group_78	0.087	0.05	5348
ELECTRON MICROSCOPY	r_ncsr_local_group_79	0.088	0.05	5384
ELECTRON MICROSCOPY	r_ncsr_local_group_80	0.068	0.05	5415
ELECTRON MICROSCOPY	r_ncsr_local_group_81	0.077	0.05	5426
ELECTRON MICROSCOPY	r_ncsr_local_group_82	0.006	0.05	5593
ELECTRON MICROSCOPY	r_ncsr_local_group_83	0.093	0.05	5354
ELECTRON MICROSCOPY	r_ncsr_local_group_84	0.083	0.05	5300
ELECTRON MICROSCOPY	r_ncsr_local_group_85	0.053	0.05	5338
ELECTRON MICROSCOPY	r_ncsr_local_group_86	0.047	0.05	5361
ELECTRON MICROSCOPY	r_ncsr_local_group_87	0.047	0.05	5365
ELECTRON MICROSCOPY	r_ncsr_local_group_88	0.073	0.05	5322
ELECTRON MICROSCOPY	r_ncsr_local_group_89	0.006	0.05	5429
ELECTRON MICROSCOPY	r_ncsr_local_group_90	0.083	0.05	5298
ELECTRON MICROSCOPY	r_ncsr_local_group_91	0.105	0.05	5307
ELECTRON MICROSCOPY	r_ncsr_local_group_92	0.094	0.05	5381
ELECTRON MICROSCOPY	r_ncsr_local_group_93	0.101	0.05	5329
ELECTRON MICROSCOPY	r_ncsr_local_group_94	0.102	0.05	5355
ELECTRON MICROSCOPY	r_ncsr_local_group_95	0.101	0.05	5358
ELECTRON MICROSCOPY	r_ncsr_local_group_96	0.058	0.05	5493
ELECTRON MICROSCOPY	r_ncsr_local_group_97	0.087	0.05	5306
ELECTRON MICROSCOPY	r_ncsr_local_group_98	0.084	0.05	5292
ELECTRON MICROSCOPY	r_ncsr_local_group_99	0.083	0.05	5309
ELECTRON MICROSCOPY	r_ncsr_local_group_100	0.088	0.05	5307
ELECTRON MICROSCOPY	r_ncsr_local_group_101	0.083	0.05	5298
ELECTRON MICROSCOPY	r_ncsr_local_group_102	0.007	0.05	5463
ELECTRON MICROSCOPY	r_ncsr_local_group_103	0.093	0.05	5361
ELECTRON MICROSCOPY	r_ncsr_local_group_104	0.086	0.05	5380
ELECTRON MICROSCOPY	r_ncsr_local_group_105	0.079	0.05	5408
ELECTRON MICROSCOPY	r_ncsr_local_group_106	0.088	0.05	5361
ELECTRON MICROSCOPY	r_ncsr_local_group_107	0.104	0.05	5283
ELECTRON MICROSCOPY	r_ncsr_local_group_108	0.058	0.05	5320
ELECTRON MICROSCOPY	r_ncsr_local_group_109	0.059	0.05	5353
ELECTRON MICROSCOPY	r_ncsr_local_group_110	0.074	0.05	5339
ELECTRON MICROSCOPY	r_ncsr_local_group_111	0.053	0.05	5337
ELECTRON MICROSCOPY	r_ncsr_local_group_112	0.087	0.05	5295
ELECTRON MICROSCOPY	r_ncsr_local_group_113	0.082	0.05	5369
ELECTRON MICROSCOPY	r_ncsr_local_group_114	0.083	0.05	5433
ELECTRON MICROSCOPY	r_ncsr_local_group_115	0.089	0.05	5396
ELECTRON MICROSCOPY	r_ncsr_local_group_116	0.086	0.05	5402
ELECTRON MICROSCOPY	r_ncsr_local_group_117	0.056	0.05	5354
ELECTRON MICROSCOPY	r_ncsr_local_group_118	0.071	0.05	5316
ELECTRON MICROSCOPY	r_ncsr_local_group_119	0.047	0.05	5360
ELECTRON MICROSCOPY	r_ncsr_local_group_120	0.083	0.05	5285
ELECTRON MICROSCOPY	r_ncsr_local_group_121	0.073	0.05	5433
ELECTRON MICROSCOPY	r_ncsr_local_group_122	0.068	0.05	5421
ELECTRON MICROSCOPY	r_ncsr_local_group_123	0.093	0.05	5320
ELECTRON MICROSCOPY	r_ncsr_local_group_124	0.077	0.05	5325
ELECTRON MICROSCOPY	r_ncsr_local_group_125	0.047	0.05	5363
ELECTRON MICROSCOPY	r_ncsr_local_group_126	0.083	0.05	5304
ELECTRON MICROSCOPY	r_ncsr_local_group_127	0.077	0.05	5434
ELECTRON MICROSCOPY	r_ncsr_local_group_128	0.095	0.05	5359
ELECTRON MICROSCOPY	r_ncsr_local_group_129	0.073	0.05	5322
ELECTRON MICROSCOPY	r_ncsr_local_group_130	0.088	0.05	5298
ELECTRON MICROSCOPY	r_ncsr_local_group_131	0.094	0.05	5360
ELECTRON MICROSCOPY	r_ncsr_local_group_132	0.083	0.05	5289

Refine LS restraints NCS

Ens-ID	Dom-ID	Auth asym-ID	Refine-ID	タイプ	Rms dev position (Å)	Weight position
1	1	A	ELECTRON MICROSCOPY	Local ncs	0.09589	0.05009
1	2	A	ELECTRON MICROSCOPY	Local ncs	0.09589	0.05009
2	3	A	ELECTRON MICROSCOPY	Local ncs	0.08197	0.05009
2	4	A	ELECTRON MICROSCOPY	Local ncs	0.08197	0.05009
3	5	A	ELECTRON MICROSCOPY	Local ncs	0.07343	0.05009
3	6	A	ELECTRON MICROSCOPY	Local ncs	0.07343	0.05009
4	7	A	ELECTRON MICROSCOPY	Local ncs	0.08186	0.05009
4	8	A	ELECTRON MICROSCOPY	Local ncs	0.08186	0.05009
5	9	A	ELECTRON MICROSCOPY	Local ncs	0.10393	0.05008
5	10	A	ELECTRON MICROSCOPY	Local ncs	0.10393	0.05008
6	11	A	ELECTRON MICROSCOPY	Local ncs	0.0453	0.0501
6	12	A	ELECTRON MICROSCOPY	Local ncs	0.0453	0.0501
7	13	A	ELECTRON MICROSCOPY	Local ncs	0.08618	0.05009
7	14	A	ELECTRON MICROSCOPY	Local ncs	0.08618	0.05009
8	15	A	ELECTRON MICROSCOPY	Local ncs	0.08042	0.05009
8	16	A	ELECTRON MICROSCOPY	Local ncs	0.08042	0.05009
9	17	A	ELECTRON MICROSCOPY	Local ncs	0.07316	0.05009
9	18	A	ELECTRON MICROSCOPY	Local ncs	0.07316	0.05009
10	19	A	ELECTRON MICROSCOPY	Local ncs	0.08302	0.05009
10	20	A	ELECTRON MICROSCOPY	Local ncs	0.08302	0.05009
11	21	A	ELECTRON MICROSCOPY	Local ncs	0.09898	0.05008
11	22	A	ELECTRON MICROSCOPY	Local ncs	0.09898	0.05008
12	23	A	ELECTRON MICROSCOPY	Local ncs	0.05727	0.0501
12	24	A	ELECTRON MICROSCOPY	Local ncs	0.05727	0.0501
13	25	A	ELECTRON MICROSCOPY	Local ncs	0.05812	0.0501
13	26	A	ELECTRON MICROSCOPY	Local ncs	0.05812	0.0501
14	27	A	ELECTRON MICROSCOPY	Local ncs	0.0746	0.0501
14	28	A	ELECTRON MICROSCOPY	Local ncs	0.0746	0.0501
15	29	A	ELECTRON MICROSCOPY	Local ncs	0.0516	0.0501
15	30	A	ELECTRON MICROSCOPY	Local ncs	0.0516	0.0501
16	31	A	ELECTRON MICROSCOPY	Local ncs	0.0877	0.0501
16	32	A	ELECTRON MICROSCOPY	Local ncs	0.0877	0.0501
17	33	A	ELECTRON MICROSCOPY	Local ncs	0.00582	0.05011
17	34	A	ELECTRON MICROSCOPY	Local ncs	0.00582	0.05011
18	35	A	ELECTRON MICROSCOPY	Local ncs	0.0581	0.0501
18	36	A	ELECTRON MICROSCOPY	Local ncs	0.0581	0.0501
19	37	A	ELECTRON MICROSCOPY	Local ncs	0.05795	0.0501
19	38	A	ELECTRON MICROSCOPY	Local ncs	0.05795	0.0501
20	39	A	ELECTRON MICROSCOPY	Local ncs	0.07449	0.0501
20	40	A	ELECTRON MICROSCOPY	Local ncs	0.07449	0.0501
21	41	A	ELECTRON MICROSCOPY	Local ncs	0.0519	0.0501
21	42	A	ELECTRON MICROSCOPY	Local ncs	0.0519	0.0501
22	43	A	ELECTRON MICROSCOPY	Local ncs	0.08776	0.0501
22	44	A	ELECTRON MICROSCOPY	Local ncs	0.08776	0.0501
23	45	A	ELECTRON MICROSCOPY	Local ncs	0.09226	0.05008
23	46	A	ELECTRON MICROSCOPY	Local ncs	0.09226	0.05008
24	47	A	ELECTRON MICROSCOPY	Local ncs	0.0902	0.05009
24	48	A	ELECTRON MICROSCOPY	Local ncs	0.0902	0.05009
25	49	A	ELECTRON MICROSCOPY	Local ncs	0.09475	0.05009
25	50	A	ELECTRON MICROSCOPY	Local ncs	0.09475	0.05009
26	51	A	ELECTRON MICROSCOPY	Local ncs	0.10337	0.05009
26	52	A	ELECTRON MICROSCOPY	Local ncs	0.10337	0.05009
27	53	A	ELECTRON MICROSCOPY	Local ncs	0.10224	0.05008
27	54	A	ELECTRON MICROSCOPY	Local ncs	0.10224	0.05008
28	55	A	ELECTRON MICROSCOPY	Local ncs	0.05308	0.0501
28	56	A	ELECTRON MICROSCOPY	Local ncs	0.05308	0.0501
29	57	A	ELECTRON MICROSCOPY	Local ncs	0.09154	0.05009
29	58	A	ELECTRON MICROSCOPY	Local ncs	0.09154	0.05009
30	59	A	ELECTRON MICROSCOPY	Local ncs	0.08991	0.05009
30	60	A	ELECTRON MICROSCOPY	Local ncs	0.08991	0.05009
31	61	A	ELECTRON MICROSCOPY	Local ncs	0.09551	0.05009
31	62	A	ELECTRON MICROSCOPY	Local ncs	0.09551	0.05009
32	63	A	ELECTRON MICROSCOPY	Local ncs	0.09662	0.05009
32	64	A	ELECTRON MICROSCOPY	Local ncs	0.09662	0.05009
33	65	A	ELECTRON MICROSCOPY	Local ncs	0.05421	0.05011
33	66	A	ELECTRON MICROSCOPY	Local ncs	0.05421	0.05011
34	67	A	ELECTRON MICROSCOPY	Local ncs	0.0705	0.0501
34	68	A	ELECTRON MICROSCOPY	Local ncs	0.0705	0.0501
35	69	A	ELECTRON MICROSCOPY	Local ncs	0.04634	0.0501
35	70	A	ELECTRON MICROSCOPY	Local ncs	0.04634	0.0501
36	71	A	ELECTRON MICROSCOPY	Local ncs	0.08314	0.0501
36	72	A	ELECTRON MICROSCOPY	Local ncs	0.08314	0.0501
37	73	A	ELECTRON MICROSCOPY	Local ncs	0.05773	0.0501
37	74	A	ELECTRON MICROSCOPY	Local ncs	0.05773	0.0501
38	75	A	ELECTRON MICROSCOPY	Local ncs	0.0051	0.05011
38	76	A	ELECTRON MICROSCOPY	Local ncs	0.0051	0.05011
39	77	A	ELECTRON MICROSCOPY	Local ncs	0.05466	0.0501
39	78	A	ELECTRON MICROSCOPY	Local ncs	0.05466	0.0501
40	79	A	ELECTRON MICROSCOPY	Local ncs	0.06995	0.0501
40	80	A	ELECTRON MICROSCOPY	Local ncs	0.06995	0.0501
41	81	A	ELECTRON MICROSCOPY	Local ncs	0.04663	0.0501
41	82	A	ELECTRON MICROSCOPY	Local ncs	0.04663	0.0501
42	83	A	ELECTRON MICROSCOPY	Local ncs	0.08408	0.0501
42	84	A	ELECTRON MICROSCOPY	Local ncs	0.08408	0.0501
43	85	A	ELECTRON MICROSCOPY	Local ncs	0.07275	0.05009
43	86	A	ELECTRON MICROSCOPY	Local ncs	0.07275	0.05009
44	87	A	ELECTRON MICROSCOPY	Local ncs	0.0695	0.05009
44	88	A	ELECTRON MICROSCOPY	Local ncs	0.0695	0.05009
45	89	A	ELECTRON MICROSCOPY	Local ncs	0.10022	0.05008
45	90	A	ELECTRON MICROSCOPY	Local ncs	0.10022	0.05008
46	91	A	ELECTRON MICROSCOPY	Local ncs	0.08687	0.05009
46	92	A	ELECTRON MICROSCOPY	Local ncs	0.08687	0.05009
47	93	A	ELECTRON MICROSCOPY	Local ncs	0.08223	0.05009
47	94	A	ELECTRON MICROSCOPY	Local ncs	0.08223	0.05009
48	95	A	ELECTRON MICROSCOPY	Local ncs	0.01142	0.0501
48	96	A	ELECTRON MICROSCOPY	Local ncs	0.01142	0.0501
49	97	A	ELECTRON MICROSCOPY	Local ncs	0.07251	0.05009
49	98	A	ELECTRON MICROSCOPY	Local ncs	0.07251	0.05009
50	99	A	ELECTRON MICROSCOPY	Local ncs	0.06952	0.05009
50	100	A	ELECTRON MICROSCOPY	Local ncs	0.06952	0.05009
51	101	A	ELECTRON MICROSCOPY	Local ncs	0.09361	0.05008
51	102	A	ELECTRON MICROSCOPY	Local ncs	0.09361	0.05008
52	103	A	ELECTRON MICROSCOPY	Local ncs	0.07721	0.0501
52	104	A	ELECTRON MICROSCOPY	Local ncs	0.07721	0.0501
53	105	A	ELECTRON MICROSCOPY	Local ncs	0.04715	0.0501
53	106	A	ELECTRON MICROSCOPY	Local ncs	0.04715	0.0501
54	107	A	ELECTRON MICROSCOPY	Local ncs	0.08423	0.0501
54	108	A	ELECTRON MICROSCOPY	Local ncs	0.08423	0.0501
55	109	A	ELECTRON MICROSCOPY	Local ncs	0.05943	0.0501
55	110	A	ELECTRON MICROSCOPY	Local ncs	0.05943	0.0501
56	111	A	ELECTRON MICROSCOPY	Local ncs	0.05547	0.0501
56	112	A	ELECTRON MICROSCOPY	Local ncs	0.05547	0.0501
57	113	A	ELECTRON MICROSCOPY	Local ncs	0.00576	0.05011
57	114	A	ELECTRON MICROSCOPY	Local ncs	0.00576	0.05011
58	115	A	ELECTRON MICROSCOPY	Local ncs	0.07705	0.0501
58	116	A	ELECTRON MICROSCOPY	Local ncs	0.07705	0.0501
59	117	A	ELECTRON MICROSCOPY	Local ncs	0.04765	0.0501
59	118	A	ELECTRON MICROSCOPY	Local ncs	0.04765	0.0501
60	119	A	ELECTRON MICROSCOPY	Local ncs	0.08421	0.0501
60	120	A	ELECTRON MICROSCOPY	Local ncs	0.08421	0.0501
61	121	A	ELECTRON MICROSCOPY	Local ncs	0.07561	0.05009
61	122	A	ELECTRON MICROSCOPY	Local ncs	0.07561	0.05009
62	123	A	ELECTRON MICROSCOPY	Local ncs	0.10224	0.05009
62	124	A	ELECTRON MICROSCOPY	Local ncs	0.10224	0.05009
63	125	A	ELECTRON MICROSCOPY	Local ncs	0.0794	0.05009
63	126	A	ELECTRON MICROSCOPY	Local ncs	0.0794	0.05009
64	127	A	ELECTRON MICROSCOPY	Local ncs	0.08348	0.05009
64	128	A	ELECTRON MICROSCOPY	Local ncs	0.08348	0.05009
65	129	A	ELECTRON MICROSCOPY	Local ncs	0.0729	0.05009
65	130	A	ELECTRON MICROSCOPY	Local ncs	0.0729	0.05009
66	131	A	ELECTRON MICROSCOPY	Local ncs	0.0057	0.0501
66	132	A	ELECTRON MICROSCOPY	Local ncs	0.0057	0.0501
67	133	A	ELECTRON MICROSCOPY	Local ncs	0.07718	0.05009
67	134	A	ELECTRON MICROSCOPY	Local ncs	0.07718	0.05009
68	135	A	ELECTRON MICROSCOPY	Local ncs	0.09723	0.05009
68	136	A	ELECTRON MICROSCOPY	Local ncs	0.09723	0.05009
69	137	A	ELECTRON MICROSCOPY	Local ncs	0.07334	0.0501
69	138	A	ELECTRON MICROSCOPY	Local ncs	0.07334	0.0501
70	139	A	ELECTRON MICROSCOPY	Local ncs	0.08928	0.0501
70	140	A	ELECTRON MICROSCOPY	Local ncs	0.08928	0.0501
71	141	A	ELECTRON MICROSCOPY	Local ncs	0.07468	0.0501
71	142	A	ELECTRON MICROSCOPY	Local ncs	0.07468	0.0501
72	143	A	ELECTRON MICROSCOPY	Local ncs	0.07162	0.0501
72	144	A	ELECTRON MICROSCOPY	Local ncs	0.07162	0.0501
73	145	A	ELECTRON MICROSCOPY	Local ncs	0.07704	0.0501
73	146	A	ELECTRON MICROSCOPY	Local ncs	0.07704	0.0501
74	147	A	ELECTRON MICROSCOPY	Local ncs	0.0066	0.05011
74	148	A	ELECTRON MICROSCOPY	Local ncs	0.0066	0.05011
75	149	A	ELECTRON MICROSCOPY	Local ncs	0.07356	0.0501
75	150	A	ELECTRON MICROSCOPY	Local ncs	0.07356	0.0501
76	151	A	ELECTRON MICROSCOPY	Local ncs	0.08902	0.0501
76	152	A	ELECTRON MICROSCOPY	Local ncs	0.08902	0.0501
77	153	A	ELECTRON MICROSCOPY	Local ncs	0.10081	0.05009
77	154	A	ELECTRON MICROSCOPY	Local ncs	0.10081	0.05009
78	155	A	ELECTRON MICROSCOPY	Local ncs	0.08707	0.05009
78	156	A	ELECTRON MICROSCOPY	Local ncs	0.08707	0.05009
79	157	A	ELECTRON MICROSCOPY	Local ncs	0.0879	0.05009
79	158	A	ELECTRON MICROSCOPY	Local ncs	0.0879	0.05009
80	159	A	ELECTRON MICROSCOPY	Local ncs	0.06822	0.05009
80	160	A	ELECTRON MICROSCOPY	Local ncs	0.06822	0.05009
81	161	A	ELECTRON MICROSCOPY	Local ncs	0.07671	0.05009
81	162	A	ELECTRON MICROSCOPY	Local ncs	0.07671	0.05009
82	163	A	ELECTRON MICROSCOPY	Local ncs	0.00628	0.0501
82	164	A	ELECTRON MICROSCOPY	Local ncs	0.00628	0.0501
83	165	A	ELECTRON MICROSCOPY	Local ncs	0.09297	0.05009
83	166	A	ELECTRON MICROSCOPY	Local ncs	0.09297	0.05009
84	167	A	ELECTRON MICROSCOPY	Local ncs	0.08329	0.0501
84	168	A	ELECTRON MICROSCOPY	Local ncs	0.08329	0.0501
85	169	A	ELECTRON MICROSCOPY	Local ncs	0.05295	0.0501
85	170	A	ELECTRON MICROSCOPY	Local ncs	0.05295	0.0501
86	171	A	ELECTRON MICROSCOPY	Local ncs	0.04679	0.0501
86	172	A	ELECTRON MICROSCOPY	Local ncs	0.04679	0.0501
87	173	A	ELECTRON MICROSCOPY	Local ncs	0.04705	0.0501
87	174	A	ELECTRON MICROSCOPY	Local ncs	0.04705	0.0501
88	175	A	ELECTRON MICROSCOPY	Local ncs	0.07282	0.0501
88	176	A	ELECTRON MICROSCOPY	Local ncs	0.07282	0.0501
89	177	A	ELECTRON MICROSCOPY	Local ncs	0.00631	0.05011
89	178	A	ELECTRON MICROSCOPY	Local ncs	0.00631	0.05011
90	179	A	ELECTRON MICROSCOPY	Local ncs	0.08286	0.0501
90	180	A	ELECTRON MICROSCOPY	Local ncs	0.08286	0.0501
91	181	A	ELECTRON MICROSCOPY	Local ncs	0.10482	0.05008
91	182	A	ELECTRON MICROSCOPY	Local ncs	0.10482	0.05008
92	183	A	ELECTRON MICROSCOPY	Local ncs	0.09439	0.05009
92	184	A	ELECTRON MICROSCOPY	Local ncs	0.09439	0.05009
93	185	A	ELECTRON MICROSCOPY	Local ncs	0.10095	0.05009
93	186	A	ELECTRON MICROSCOPY	Local ncs	0.10095	0.05009
94	187	A	ELECTRON MICROSCOPY	Local ncs	0.1018	0.05009
94	188	A	ELECTRON MICROSCOPY	Local ncs	0.1018	0.05009
95	189	A	ELECTRON MICROSCOPY	Local ncs	0.10136	0.05009
95	190	A	ELECTRON MICROSCOPY	Local ncs	0.10136	0.05009
96	191	A	ELECTRON MICROSCOPY	Local ncs	0.0578	0.05009
96	192	A	ELECTRON MICROSCOPY	Local ncs	0.0578	0.05009
97	193	A	ELECTRON MICROSCOPY	Local ncs	0.08728	0.0501
97	194	A	ELECTRON MICROSCOPY	Local ncs	0.08728	0.0501
98	195	A	ELECTRON MICROSCOPY	Local ncs	0.08352	0.0501
98	196	A	ELECTRON MICROSCOPY	Local ncs	0.08352	0.0501
99	197	A	ELECTRON MICROSCOPY	Local ncs	0.08303	0.0501
99	198	A	ELECTRON MICROSCOPY	Local ncs	0.08303	0.0501
100	199	A	ELECTRON MICROSCOPY	Local ncs	0.08835	0.0501
100	200	A	ELECTRON MICROSCOPY	Local ncs	0.08835	0.0501
101	201	A	ELECTRON MICROSCOPY	Local ncs	0.08338	0.0501
101	202	A	ELECTRON MICROSCOPY	Local ncs	0.08338	0.0501
102	203	A	ELECTRON MICROSCOPY	Local ncs	0.00706	0.05011
102	204	A	ELECTRON MICROSCOPY	Local ncs	0.00706	0.05011
103	205	A	ELECTRON MICROSCOPY	Local ncs	0.09331	0.05009
103	206	A	ELECTRON MICROSCOPY	Local ncs	0.09331	0.05009
104	207	A	ELECTRON MICROSCOPY	Local ncs	0.08636	0.05009
104	208	A	ELECTRON MICROSCOPY	Local ncs	0.08636	0.05009
105	209	A	ELECTRON MICROSCOPY	Local ncs	0.07912	0.05009
105	210	A	ELECTRON MICROSCOPY	Local ncs	0.07912	0.05009
106	211	A	ELECTRON MICROSCOPY	Local ncs	0.08796	0.05009
106	212	A	ELECTRON MICROSCOPY	Local ncs	0.08796	0.05009
107	213	A	ELECTRON MICROSCOPY	Local ncs	0.1043	0.05008
107	214	A	ELECTRON MICROSCOPY	Local ncs	0.1043	0.05008
108	215	A	ELECTRON MICROSCOPY	Local ncs	0.05839	0.0501
108	216	A	ELECTRON MICROSCOPY	Local ncs	0.05839	0.0501
109	217	A	ELECTRON MICROSCOPY	Local ncs	0.05905	0.0501
109	218	A	ELECTRON MICROSCOPY	Local ncs	0.05905	0.0501
110	219	A	ELECTRON MICROSCOPY	Local ncs	0.07439	0.0501
110	220	A	ELECTRON MICROSCOPY	Local ncs	0.07439	0.0501
111	221	A	ELECTRON MICROSCOPY	Local ncs	0.05303	0.0501
111	222	A	ELECTRON MICROSCOPY	Local ncs	0.05303	0.0501
112	223	A	ELECTRON MICROSCOPY	Local ncs	0.08749	0.0501
112	224	A	ELECTRON MICROSCOPY	Local ncs	0.08749	0.0501
113	225	A	ELECTRON MICROSCOPY	Local ncs	0.08151	0.05009
113	226	A	ELECTRON MICROSCOPY	Local ncs	0.08151	0.05009
114	227	A	ELECTRON MICROSCOPY	Local ncs	0.08294	0.05009
114	228	A	ELECTRON MICROSCOPY	Local ncs	0.08294	0.05009
115	229	A	ELECTRON MICROSCOPY	Local ncs	0.08871	0.05009
115	230	A	ELECTRON MICROSCOPY	Local ncs	0.08871	0.05009
116	231	A	ELECTRON MICROSCOPY	Local ncs	0.08596	0.05009
116	232	A	ELECTRON MICROSCOPY	Local ncs	0.08596	0.05009
117	233	A	ELECTRON MICROSCOPY	Local ncs	0.05573	0.0501
117	234	A	ELECTRON MICROSCOPY	Local ncs	0.05573	0.0501
118	235	A	ELECTRON MICROSCOPY	Local ncs	0.07089	0.0501
118	236	A	ELECTRON MICROSCOPY	Local ncs	0.07089	0.0501
119	237	A	ELECTRON MICROSCOPY	Local ncs	0.0468	0.0501
119	238	A	ELECTRON MICROSCOPY	Local ncs	0.0468	0.0501
120	239	A	ELECTRON MICROSCOPY	Local ncs	0.08347	0.0501
120	240	A	ELECTRON MICROSCOPY	Local ncs	0.08347	0.0501
121	241	A	ELECTRON MICROSCOPY	Local ncs	0.07259	0.05009
121	242	A	ELECTRON MICROSCOPY	Local ncs	0.07259	0.05009
122	243	A	ELECTRON MICROSCOPY	Local ncs	0.06807	0.0501
122	244	A	ELECTRON MICROSCOPY	Local ncs	0.06807	0.0501
123	245	A	ELECTRON MICROSCOPY	Local ncs	0.09333	0.05009
123	246	A	ELECTRON MICROSCOPY	Local ncs	0.09333	0.05009
124	247	A	ELECTRON MICROSCOPY	Local ncs	0.07679	0.0501
124	248	A	ELECTRON MICROSCOPY	Local ncs	0.07679	0.0501
125	249	A	ELECTRON MICROSCOPY	Local ncs	0.04733	0.0501
125	250	A	ELECTRON MICROSCOPY	Local ncs	0.04733	0.0501
126	251	A	ELECTRON MICROSCOPY	Local ncs	0.08315	0.0501
126	252	A	ELECTRON MICROSCOPY	Local ncs	0.08315	0.0501
127	253	A	ELECTRON MICROSCOPY	Local ncs	0.07706	0.05009
127	254	A	ELECTRON MICROSCOPY	Local ncs	0.07706	0.05009
128	255	A	ELECTRON MICROSCOPY	Local ncs	0.0954	0.05009
128	256	A	ELECTRON MICROSCOPY	Local ncs	0.0954	0.05009
129	257	A	ELECTRON MICROSCOPY	Local ncs	0.07283	0.0501
129	258	A	ELECTRON MICROSCOPY	Local ncs	0.07283	0.0501
130	259	A	ELECTRON MICROSCOPY	Local ncs	0.08822	0.0501
130	260	A	ELECTRON MICROSCOPY	Local ncs	0.08822	0.0501
131	261	A	ELECTRON MICROSCOPY	Local ncs	0.09359	0.05009
131	262	A	ELECTRON MICROSCOPY	Local ncs	0.09359	0.05009
132	263	A	ELECTRON MICROSCOPY	Local ncs	0.0832	0.0501
132	264	A	ELECTRON MICROSCOPY	Local ncs	0.0832	0.0501

LS精密化 シェル

Refine-ID: ELECTRON MICROSCOPY / Num. reflection R_free: _ / Total num. of bins used: 20 / % reflection obs: 100 %

解像度 (Å)	Rfactor Rwork	Num. reflection Rwork	Rfactor all	Num. reflection all	Fsc work	WRfactor Rwork
3.15-3.232	0.62	16091	0.62	16091	0.571	0.62
3.232-3.32	0.436	15581	0.436	15581	0.677	0.436
3.32-3.417	0.399	15274	0.399	15274	0.73	0.399
3.417-3.522	0.388	14841	0.388	14841	0.756	0.388
3.522-3.637	0.366	14269	0.366	14269	0.789	0.366
3.637-3.765	0.339	13908	0.339	13908	0.827	0.339
3.765-3.907	0.324	13387	0.324	13387	0.847	0.324
3.907-4.066	0.315	12916	0.315	12916	0.856	0.315
4.066-4.247	0.299	12257	0.299	12257	0.878	0.299
4.247-4.454	0.289	11832	0.289	11832	0.889	0.289
4.454-4.695	0.282	11220	0.282	11220	0.894	0.282
4.695-4.979	0.278	10583	0.278	10583	0.894	0.278
4.979-5.323	0.278	9964	0.278	9964	0.891	0.278
5.323-5.748	0.299	9314	0.299	9314	0.885	0.299
5.748-6.296	0.331	8555	0.331	8555	0.873	0.331
6.296-7.038	0.306	7708	0.306	7708	0.884	0.306
7.038-8.124	0.269	6837	0.269	6837	0.897	0.269
8.124-9.943	0.24	5727	0.24	5727	0.93	0.24
9.943-14.034	0.224	4463	0.224	4463	0.947	0.224
14.034-157.32	0.231	2455	0.231	2455	0.983	0.231