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Structure paper

TitleThe neutron structure of urate oxidase resolves a long-standing mechanistic conundrum and reveals unexpected changes in protonation.
Journal, issue, pagesPlos One, Vol. 9, Page e86651-e86651, Year 2014
Publish dateOct 7, 2013 (structure data deposition date)
AuthorsOksanen, E. / Blakeley, M.P. / El-Hajji, M. / Ryde, U. / Budayova-Spano, M.
External linksPlos One / PubMed:24466188
Methodsneutron diffraction / X-ray diffraction
Resolution1.06 - 2.023 Å
Structure data

PDB-4n3m:
Joint neutron/X-ray structure of urate oxidase in complex with 8-azaxanthine
Method: NEUTRON DIFFRACTION / X-RAY DIFFRACTION / Resolution: 1.919 Å

PDB-4n9m:
Joint neutron/x-ray structure of urate oxidase in complex with 8-hydroxyxanthine
Method: NEUTRON DIFFRACTION / X-RAY DIFFRACTION / Resolution: 2.023 Å

PDB-4n9s:
High resolution X-RAY STRUCTURE OF URATE OXIDASE IN COMPLEX WITH 8-HYDROXYXANTHINE
Method: X-RAY DIFFRACTION / Resolution: 1.06 Å

PDB-4n9v:
High resolution x-ray structure of urate oxidase in complex with 8-azaxanthine
Method: X-RAY DIFFRACTION / Resolution: 1.1 Å

Chemicals

ChemComp-AZA:
8-AZAXANTHINE

ChemComp-CL:
Unknown entry

ChemComp-NA:
Unknown entry

ChemComp-DOD:
DEUTERATED WATER

ChemComp-8HX:
8-hydroxy-3,9-dihydro-1H-purine-2,6-dione

ChemComp-GOL:
GLYCEROL

ChemComp-HOH:
WATER

ChemComp-ZN:
Unknown entry

Source
  • aspergillus flavus (mold)
KeywordsOXIDOREDUCTASE / urate oxidase / uricase / uricase oxidoreductase

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