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TitleMechanistic manifold in a hemoprotein-catalyzed cyclopropanation reaction with diazoketone.
Journal, issue, pagesNat Commun, Vol. 14, Page 7985-7985, Year 2023
Publish dateOct 14, 2022 (structure data deposition date)
AuthorsNam, D. / Bacik, J.P. / Khade, R.L. / Aguilera, M.C. / Wei, Y. / Villada, J.D. / Neidig, M.L. / Zhang, Y. / Ando, N. / Fasan, R.
External linksNat Commun / PubMed:38042860
MethodsX-ray diffraction
Resolution1.04 - 1.4 Å
Structure data

PDB-8ess:
Myoglobin variant Mb-cIII complex
Method: X-RAY DIFFRACTION / Resolution: 1.4 Å

PDB-8esu:
Myoglobin variant Mb-imi complex
Method: X-RAY DIFFRACTION / Resolution: 1.04 Å

Chemicals

ChemComp-SO4:
SULFATE ION

ChemComp-WRK:
[2,18-bis(2-carboxyethyl)-7,12-diethenyl-3,8,13,17-tetramethyl-21-(2-oxo-3-phenylpropyl)porphyrin-21-iumato(2-)-kappa~3~N~22~,N~23~,N~24~]iron(2+)

ChemComp-HOH:
WATER

ChemComp-HEM:
PROTOPORPHYRIN IX CONTAINING FE

ChemComp-IMD:
IMIDAZOLE

Source
  • physeter catodon (sperm whale)
KeywordsOXYGEN STORAGE / HEME / METALLOPROTEIN / MYOGLOBIN / DIAZOKETONE / IMIDAZOLE

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