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Structure paper

TitleStructural insights into heparanase activity using a fluorogenic heparan sulfate disaccharide.
Journal, issue, pagesChem. Commun. (Camb. ), Vol. 56, Page 13780-13783, Year 2020
Publish dateJun 14, 2020 (structure data deposition date)
AuthorsWu, L. / Wimmer, N. / Davies, G.J. / Ferro, V.
External linksChem. Commun. (Camb. ) / PubMed:33073275
MethodsX-ray diffraction
Resolution1.714 Å
Structure data

PDB-6zdm:
Crystal structure of human heparanase in complex with a N',6O'-bis-sulfated 4-methylumbelliferyl heparan sulfate disaccharide
Method: X-RAY DIFFRACTION / Resolution: 1.714 Å

Chemicals

ChemComp-NAG:
2-acetamido-2-deoxy-beta-D-glucopyranose

ChemComp-EDO:
1,2-ETHANEDIOL

ChemComp-QG2:
(2~{S},3~{S},4~{R},5~{R},6~{S})-3-[(2~{R},3~{R},4~{R},5~{S},6~{R})-4,5-bis(oxidanyl)-3-(sulfoamino)-6-(sulfooxymethyl)oxan-2-yl]oxy-6-(4-methyl-2-oxidanylidene-chromen-7-yl)oxy-4,5-bis(oxidanyl)oxane-2-carboxylic acid

ChemComp-SO4:
SULFATE ION

ChemComp-HOH:
WATER

Source
  • homo sapiens (human)
KeywordsHYDROLASE / heparanase / substrate / fluorogenic / heparan sulfate / poised / 4-methylumbelliferyl

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