SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AB" IN EACH CHAIN ON SHEET RECORDS BELOW ... SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AB" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 8-STRANDED BARREL THIS IS REPRESENTED BY A 9-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL. THE SHEETS PRESENTED AS "BA" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 8-STRANDED BARREL THIS IS REPRESENTED BY A 9-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL.
Mass: 18.015 Da / Num. of mol.: 154 / Source method: isolated from a natural source / Formula: H2O
-
Details
Nonpolymer details
L-TYROSINE (TYR): 3 TYROSINE LIGANDS ARE BOUND IN THE TWO MONOMERS OF THE ASYMMETRIC UNIT, 1 IN ...L-TYROSINE (TYR): 3 TYROSINE LIGANDS ARE BOUND IN THE TWO MONOMERS OF THE ASYMMETRIC UNIT, 1 IN SUBUNIT A AND 2 IN SUBUNIT B.
-
Experimental details
-
Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
-
Sample preparation
Crystal
Density Matthews: 3.92 Å3/Da / Density % sol: 68.6 % / Description: NONE
Crystal grow
pH: 7.5 Details: 0.1 M TRIS-HCL PH 7.5, 1.5 M AMMONIUM SULFATE, 12% V/V GLYCEROL
Resolution: 2.3→44.02 Å / Cor.coef. Fo:Fc: 0.955 / Cor.coef. Fo:Fc free: 0.939 / SU B: 6.144 / SU ML: 0.078 / Cross valid method: THROUGHOUT / ESU R: 0.032 / ESU R Free: 0.028 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. CHAIN A RESIDUES 11-12 AND CHAIN B RESIDUES 10-12 ARE DISORDERED.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.16375
3380
5 %
RANDOM
Rwork
0.13923
-
-
-
obs
0.14046
64572
96.94 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK