PDB-9rtc: Okeania NrnC bound to pGG

Basic information

• Entry: Database: PDB / ID: 9rtc
• Title: Okeania NrnC bound to pGG

Components

• RNA (5'-R(P*GP*G)-3')
• nanoRNase C

• Keywords: HYDROLASE / nuclease / NrnC
• Function / homology: GUANOSINE-5'-MONOPHOSPHATE / RNA
• Biological species: Okenia (invertebrata); Escherichia coli (E. coli)
• Method: X-RAY DIFFRACTION / SYNCHROTRON / MOLECULAR REPLACEMENT / Resolution: 3 Å
• Authors: Mortensen, S. / Burnim, A. / Dufault-Thompson, K. / Jiang, X. / Lipka, A.E. / Sondermann, H.

Funding support

United States, 1items

Organization	Grant number	Country
National Institutes of Health/National Human Genome Research Institute (NIH/NHGRI)	R01 AI142400	United States

• Citation: Journal: Sci Adv / Year: 2026; Title: Ancestral proteins trace the emergence of substrate specificity and oligomerization within bacterial DEDDy dinucleases.; Authors: Mortensen, S. / Burnim, A.A. / Dufault-Thompson, K. / Lipka, A.E. / Jiang, X. / Sondermann, H.

History

Deposition	Jul 2, 2025	Deposition site: PDBE / Processing site: PDBE
Revision 1.0	Jul 15, 2026	Provider: repository / Type: Initial release
Revision 1.1	Aug 26, 2026	Group: Database references / Category: citation / citation_author Item: _citation.country / _citation.journal_abbrev / _citation.journal_id_CSD / _citation.journal_id_ISSN / _citation.journal_volume / _citation.page_first / _citation.page_last / _citation.pdbx_database_id_DOI / _citation.pdbx_database_id_PubMed / _citation.title / _citation.year / _citation_author.identifier_ORCID / _citation_author.name

Assembly

Deposited unit

A: nanoRNase C

N: nanoRNase C

B: nanoRNase C

C: nanoRNase C

D: nanoRNase C

E: nanoRNase C

F: nanoRNase C

G: nanoRNase C

H: nanoRNase C

I: nanoRNase C

J: nanoRNase C

K: nanoRNase C

L: nanoRNase C

M: nanoRNase C

O: nanoRNase C

P: nanoRNase C

Q: nanoRNase C

R: nanoRNase C

S: nanoRNase C

T: nanoRNase C

U: nanoRNase C

V: nanoRNase C

W: nanoRNase C

X: nanoRNase C

Y: nanoRNase C

Z: nanoRNase C

AA: nanoRNase C

BB: nanoRNase C

CC: nanoRNase C

DD: nanoRNase C

EE: nanoRNase C

FF: nanoRNase C

bb: RNA (5'-R(P*GP*G)-3')

cc: RNA (5'-R(P*GP*G)-3')

ff: RNA (5'-R(P*GP*G)-3')

hetero molecules

Summary:

• 788 kDa, 35 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	788,472	118
Polymers	766,818	35
Non-polymers	21,654	83
Water	0	0

1

A: nanoRNase C

N: nanoRNase C

J: nanoRNase C

K: nanoRNase C

hetero molecules

B: nanoRNase C

C: nanoRNase C

D: nanoRNase C

E: nanoRNase C

hetero molecules

Summary:

• defined by author
• Evidence: light scattering
• 197 kDa, 8 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	197,193	31
Polymers	191,220	8
Non-polymers	5,972	23
Water	0

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1
crystal symmetry operation	2_545	-x,y-1/2,-z	1

Calculated values:

Buried area	34360 Å2
ΔGint	-258 kcal/mol
Surface area	62060 Å2

2

F: nanoRNase C

G: nanoRNase C

L: nanoRNase C

M: nanoRNase C

W: nanoRNase C

X: nanoRNase C

EE: nanoRNase C

FF: nanoRNase C

ff: RNA (5'-R(P*GP*G)-3')

hetero molecules

Summary:

• defined by author
• 197 kDa, 9 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	197,158	32
Polymers	191,866	9
Non-polymers	5,292	23
Water	0

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Buried area	34110 Å2
ΔGint	-283 kcal/mol
Surface area	61990 Å2

3

H: nanoRNase C

I: nanoRNase C

Q: nanoRNase C

R: nanoRNase C

S: nanoRNase C

T: nanoRNase C

hetero molecules

O: nanoRNase C

P: nanoRNase C

hetero molecules

Summary:

• defined by author
• 197 kDa, 8 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	197,170	30
Polymers	191,220	8
Non-polymers	5,949	22
Water	0

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1
crystal symmetry operation	2_445	-x-1,y-1/2,-z	1

Calculated values:

Buried area	34010 Å2
ΔGint	-236 kcal/mol
Surface area	62230 Å2

4

U: nanoRNase C

V: nanoRNase C

Y: nanoRNase C

Z: nanoRNase C

AA: nanoRNase C

BB: nanoRNase C

CC: nanoRNase C

DD: nanoRNase C

bb: RNA (5'-R(P*GP*G)-3')

cc: RNA (5'-R(P*GP*G)-3')

hetero molecules

Summary:

• defined by author
• 197 kDa, 10 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	196,951	25
Polymers	192,511	10
Non-polymers	4,440	15
Water	0

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Buried area	33180 Å2
ΔGint	-190 kcal/mol
Surface area	63210 Å2

Unit cell

Length a, b, c (Å)	142.480, 176.177, 159.671
Angle α, β, γ (deg.)	90.000, 94.851, 90.000
Int Tables number	4
Space group name H-M	P1211
Space group name Hall	P2yb
Symmetry operation	#1: x,y,z #2: -x,y+1/2,-z

Components

#1: Protein

A N B C D E F G H I J K L M O P Q R S ...
nanoRNase C

Details:

Mass: 23902.539 Da / Num. of mol.: 32
Source method: isolated from a genetically manipulated source
Source: (gene. exp.) Okenia (invertebrata) / Production host: Escherichia coli (E. coli)

#2: RNA chain

bb cc ff RNA (5'-R(P*GP*G)-3')

Details:

Mass: 645.454 Da / Num. of mol.: 3 / Source method: obtained synthetically / Source: (synth.) Escherichia coli (E. coli)

#3: Chemical

A-301 A-302 N-301 N-302 B-301 B-302 B-303 C-301 D-301 D-302 E-301 E-302 F-301 F-302 G-301 G-302 H-301 H-302 H-303 I-301 ...
ChemComp-G / GUANOSINE-5'-MONOPHOSPHATE

Details:

Type: RNA linking / Mass: 363.221 Da / Num. of mol.: 58 / Source method: obtained synthetically / Formula: C₁₀H₁₄N₅O₈P

#4: Chemical

A-303 A-304 N-303 C-302 D-303 G-303 H-304 H-305 J-303 J-304 L-304 Q-303 Q-304 R-303 R-304 V-303 V-304 W-303 W-304 X-303 ...
ChemComp-NA / SODIUM ION

Details:

Mass: 22.990 Da / Num. of mol.: 24 / Source method: obtained synthetically / Formula: Na

#5: Chemical

U-303 ChemComp-CL / CHLORIDE ION

Details:

Mass: 35.453 Da / Num. of mol.: 1 / Source method: obtained synthetically / Formula: Cl

• Has ligand of interest: N
• Has protein modification: N

Experimental details

Experiment

• Experiment: Method: X-RAY DIFFRACTION / Number of used crystals: 1

Sample preparation

• Crystal: Density Matthews: 2.6 ų/Da / Density % sol: 52.77 %
• Crystal grow: Temperature: 292 K / Method: vapor diffusion, sitting drop / Details: 0.2 M lithium chloride, 20% PEG 3350

Data collection

• Diffraction: Mean temperature: 100 K / Serial crystal experiment: N
• Diffraction source: Source: SYNCHROTRON / Site: PETRA III, DESY / Beamline: P11 / Wavelength: 1.0332 Å
• Detector: Type: DECTRIS EIGER2 X 16M / Detector: PIXEL / Date: May 29, 2021
• Radiation: Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
• Radiation wavelength: Wavelength: 1.0332 Å / Relative weight: 1
• Reflection: Resolution: 3→49.09 Å / Num. obs: 155358 / % possible obs: 99.04 % / Redundancy: 7.1 % / B_iso Wilson estimate: 71.31 Ų / CC_1/2: 0.997 / CC star: 0.999 / R_merge(I) obs: 0.1781 / Net I/σ(I): 9.64
• Reflection shell: Resolution: 3→3.107 Å / R_merge(I) obs: 1.429 / Num. unique obs: 15598 / CC_1/2: 0.644 / % possible all: 99.87

Processing

Software

Name	Version	Classification
PHENIX	1.19.2_4158	refinement
PHENIX	1.19.2_4158	refinement
XDS		data reduction
XDS		data scaling
PHASER		phasing

Refinement

Method to determine structure: MOLECULAR REPLACEMENT / Resolution: 3→49.09 Å / SU ML: 0.5514 / Cross valid method: FREE R-VALUE / σ(F): 1.34 / Phase error: 36.909
Stereochemistry target values: GeoStd + Monomer Library + CDL v1.2

	Rfactor	Num. reflection	% reflection
Rfree	0.2976	1805	0.59 %
Rwork	0.2347	304130	-
obs	0.235	155358	98.79 %

• Solvent computation: Shrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å / Solvent model: FLAT BULK SOLVENT MODEL
• Displacement parameters: B_iso mean: 81.64 Ų

Refinement step

Cycle: LAST / Resolution: 3→49.09 Å

	Protein	Nucleic acid	Ligand	Solvent	Total
Num. atoms	52912	141	1417	0	54470

Refine LS restraints

Refine-ID	Type	Dev ideal	Number
X-RAY DIFFRACTION	f_bond_d	0.0032	55463
X-RAY DIFFRACTION	f_angle_d	0.7197	75111
X-RAY DIFFRACTION	f_chiral_restr	0.0471	8573
X-RAY DIFFRACTION	f_plane_restr	0.0049	9321
X-RAY DIFFRACTION	f_dihedral_angle_d	7.4522	7582

LS refinement shell

Resolution (Å)	Rfactor Rfree	Num. reflection Rfree	Rfactor Rwork	Num. reflection Rwork	Refine-ID	% reflection obs (%)
3-3.08	0.4515	146	0.393	23499	X-RAY DIFFRACTION	99.59
3.08-3.17	0.4307	150	0.3696	23613	X-RAY DIFFRACTION	99.63
3.17-3.27	0.4654	133	0.3348	23450	X-RAY DIFFRACTION	99.05
3.27-3.39	0.3257	133	0.3107	23518	X-RAY DIFFRACTION	99.02
3.39-3.53	0.3577	143	0.3078	23377	X-RAY DIFFRACTION	98.9
3.53-3.69	0.3399	131	0.282	23326	X-RAY DIFFRACTION	98.59
3.69-3.88	0.3181	138	0.257	22954	X-RAY DIFFRACTION	96.66
3.88-4.12	0.2779	138	0.2432	22262	X-RAY DIFFRACTION	94.18
4.12-4.44	0.3132	134	0.2046	23706	X-RAY DIFFRACTION	99.8
4.44-4.89	0.2973	130	0.1942	23644	X-RAY DIFFRACTION	99.85
4.89-5.6	0.2584	146	0.2089	23586	X-RAY DIFFRACTION	99.85
5.6-7.05	0.2629	151	0.2257	23674	X-RAY DIFFRACTION	99.79
7.05-49.09	0.1965	132	0.1547	23521	X-RAY DIFFRACTION	99.37

Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°2)	L12 (°2)	L13 (°2)	L22 (°2)	L23 (°2)	L33 (°2)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å2)	T12 (Å2)	T13 (Å2)	T22 (Å2)	T23 (Å2)	T33 (Å2)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	9.16612065164	4.67430251536	4.68015382437	3.18955578978	5.0119346466	1.99654533198	0.372661753664	-0.00540649619622	-0.834213763749	0.547111774232	1.42695416248	0.216807094124	1.6085016014	-0.393973631488	-1.31244052942	0.620697885884	-0.438986969285	0.385536008963	0.439491821555	0.491059124996	2.61602531398	-60.2540875924	10.8007443711	21.6361248186
2	8.20079771264	8.41122837629	4.05274383427	9.57458972208	2.26415192532	5.77256008443	-0.354968482781	-1.75536841958	-2.30371949118	-0.199400945317	-0.619385706923	-0.497304198404	-0.304044794355	0.949979383086	0.741412003036	0.362008050501	0.0889131043632	0.278542110484	0.534539525543	-0.0513565656956	1.13648863478	-57.7386128821	6.25550013004	23.9534926489
3	6.17973871178	0.390057311147	-6.17067397748	0.0374881946861	-0.174116436812	9.14427207567	0.788812993641	-0.340579523215	-0.226540548897	-1.25414210426	0.333760927589	-1.27637695274	-1.60008836817	0.707481118289	-0.850448056498	1.04353474919	0.153934695754	-0.276575154273	0.276258228109	0.389690957447	2.69217916753	-58.2073413383	3.8436710229	-15.5167470785
4	4.64396942802	-2.77688566921	-0.618011002044	4.50982466254	4.63869618535	6.52363953053	-0.253180403308	-0.301657671013	0.455867311555	-0.0652777977431	0.104984849878	-0.949691747163	-0.81710293672	1.16120642589	0.197563400171	0.749837983417	-0.256044042653	-0.0665232209659	1.01978293313	0.0161705791641	1.29194499977	-55.5094177398	8.71220404145	-17.7313748146
5	9.52997247873	0.104475967807	1.06716083155	9.65277269722	3.58903863313	2.00184925726	-1.55903443248	0.173376846261	0.909745312117	-0.127312438021	-0.953763868851	0.129986267619	0.528837574102	1.55047287766	2.23267643306	0.757149908287	-0.141589007329	-0.100727156726	1.18659074165	0.628720091749	1.85035884988	-85.7883495601	-8.47459946374	-9.48249411487
6	1.99754549431	2.007180663	9.93128929697	2.00493619056	1.99556006144	1.9963653999	-0.797144554633	-1.99443303334	-1.24420771966	0.777730701321	-0.368151273624	1.38075095296	-0.956034351618	1.32778052413	1.07763298209	0.551382348333	-0.27670941214	0.0825567567207	0.920332637415	-0.0838823885817	0.926970097434	-88.5518978051	-12.0679102334	-6.05767404289
7	2.00223993064	-3.0010834595	0.36943234979	2.01096909062	3.22895676168	1.99991687134	-0.582168337579	1.24488944645	0.374167391487	0.445799460218	1.15253358404	-1.68535297085	-0.236211333298	0.860793790726	-0.738777271294	0.621214399172	0.180686636851	0.25972956537	0.740242604565	-0.018780975993	1.1559624801	20.9656677366	31.1322380381	-75.7831695992
8	9.5830807332	5.26782155616	-3.7921373115	1.99935374563	-6.96448348046	5.88256818929	0.83436001487	1.30444521456	0.474032835686	0.114963981015	-0.418192939541	0.118232730802	-0.0833397433764	0.16456003048	-0.400057168369	1.11567931548	-0.524304248047	0.188139823096	2.05241506589	-0.21079441566	0.720018561456	-52.3243496128	55.0551357344	-93.4116728718
9	1.62046991285	1.28109303834	-3.08803603576	7.10162610413	3.7822002112	1.99590594171	-0.954123436084	1.2214657626	-0.835495340466	0.320429102986	-0.764541755118	0.0355332630245	0.462047740119	-0.242697156705	1.63471845581	0.402715037335	0.0509821616823	0.121172438043	0.719090329762	-0.143238960835	1.10869187005	-82.9875745526	28.2903313334	-89.4416558061
10	4.05680962469	0.203412548423	3.16101252929	9.76823666737	-6.32307739478	6.76092083935	1.13511768477	0.515984717554	0.225901434546	0.328171658988	-1.09298115328	-0.70694650701	-0.194989034741	0.529417232755	0.097029787375	0.913057624777	0.0864575909053	-0.01282267361	0.597978437596	-0.0521201298412	1.34333487621	19.21838302	48.6322635697	-99.3495344793
11	1.78894620828	-0.569291645396	-0.697110155611	6.87874831839	3.11739905446	3.2806734666	-0.803321447107	-0.430894540692	-0.267326875024	0.409959590144	0.973599935655	0.570504333157	0.469771488274	-0.229045339477	-0.0374198443672	0.851646923139	0.683919243775	0.520814449286	1.53564773925	0.797642928317	1.56336491978	-11.5584983013	28.4088811799	-81.7330811882
12	6.1207839585	3.57357697433	7.84914009851	9.15129849591	4.45231063846	2.00317168212	-0.666297334017	-0.275618682794	-0.500085687817	-1.77489223984	1.04246448811	-2.89315123286	-0.078750919835	-0.585679022861	-0.201891226845	0.946705900843	-0.138114461698	0.140793185292	0.77032060967	-0.217647661417	1.52627364315	16.5246086247	70.1112344832	-83.4834714371
13	9.33205157114	-8.66817461291	-5.79783854806	2.00155707519	1.394003894	8.96049241131	-0.633337981134	-0.833141667174	1.11937768772	0.631037811265	1.60269437313	-1.84746338873	-0.630496786893	-0.731415349378	-1.11821632663	0.766379440611	-0.00100844490619	0.181751523095	0.823848651873	-0.277434861477	1.52041305653	-12.3800357929	54.7028934462	-96.8856590155
14	8.02143013746	1.1085685006	2.7182416222	9.49179050753	1.49362542992	2.00741278848	0.496297245636	0.0541711640256	1.03743938005	0.375724879961	-0.37213190847	0.262119584402	0.39848891849	1.63389681599	-0.333667112922	0.937716924323	0.208779932744	0.230603551732	1.43562597192	0.264610190626	0.913085565559	19.4613351461	54.2185088977	-58.3560240441
15	6.30910977956	-5.2766705408	1.36960054842	9.37331129938	5.00447005822	7.93230386611	-0.592534933096	0.0397618710373	-0.026159506801	-0.500788595768	0.542590579964	0.574408736946	0.029238801728	0.142390512777	-0.0181082495618	2.2390652912	1.52893655273	-0.405249222323	0.924990488019	0.362222619716	0.5850499526	-14.8910119905	69.0250612798	-74.3304516092
16	1.50211385789	-2.02358055923	-3.68000260644	5.84074223886	6.59027400505	9.90734220407	-0.0678008062737	-0.0767932680508	1.44885690671	-0.335661835873	0.769316204804	1.41641217787	-0.0205431888633	0.972854835141	-0.500485319249	0.793257437291	-0.228651330193	-0.0726730278561	0.964194418923	-0.220041882186	1.17331931761	-83.8570296583	58.3045565682	-86.4902096582
17	3.9427195254	1.06121309807	-0.176607625344	5.84336982465	-1.9928988327	7.1935331165	0.207537285579	-0.312133501793	-0.834661633571	0.544743583004	0.36268376927	-0.403273695037	1.46050549448	-0.47324757959	-0.487168466726	1.093788998	0.043972531732	-0.964830452765	0.543758334303	-0.661501810582	1.37311493571	-52.7682102842	63.600846868	-65.468359745
18	2.1817381855	-0.959431563981	1.57440426476	4.47991506994	1.31551277669	4.83401715162	-0.165241383179	-0.0778720432147	0.240698582402	0.202111769855	0.280594127016	-0.292861848433	-0.268767975465	0.589229202501	0.0292160886826	0.424346073993	0.0358770630227	0.0266057225537	0.57468853282	0.138565289147	0.826198622186	19.4034610266	35.6543208751	17.7286283106
19	1.84110916531	0.325121197379	0.379288942688	2.36178566601	1.1028312004	5.30908234375	0.0628997268557	0.304568231489	0.36434174624	0.0598783840661	0.0332888509159	0.150802742987	-0.383720079361	0.177340871813	-0.15213484782	0.357431219374	0.0110275908023	0.0376348259057	0.418873229969	0.0892687192506	0.584895496599	15.2675802869	34.3898057868	9.48830435564
20	4.8951155241	2.01703040124	-5.00169167197	5.53058057484	-3.38413922131	2.07890375568	-0.226284337822	-0.0950628519753	-1.26854869981	0.0235853838945	-0.493360878051	0.0194154274783	0.288127230067	0.862340030852	0.869239839619	0.523514688068	0.0649319821476	0.124668594231	0.839275185083	-0.0115882665448	0.720892744037	26.0852348884	24.7963609528	13.5349346262
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35	5.25755807277	-0.154641804088	2.37943802245	2.39182914651	-3.31442196668	5.79895623983	-0.276910520779	0.53183036086	-1.36707938489	-1.03125490801	-0.188302080236	-1.21835733169	0.745409425562	1.26620989245	-0.0249519522573	0.590071987436	0.110677754569	0.266892504328	0.820905740394	-0.0733936109405	1.92994687205	26.1007606066	56.0364469402	-11.8270399058
36	4.63883734537	-0.703222732255	-1.13769831122	9.16878434231	-1.13177158546	3.00319314051	-0.0850301597057	-1.09255803507	0.0767945600761	-0.744272832649	0.0492411797129	-0.729320842688	0.490774468506	-0.0261760319752	0.393657263743	0.507393938528	-0.0437646971345	0.160381768696	0.852151768876	-0.151651328372	1.69391921805	19.8121838897	60.5453395667	-3.12373979886
37	1.63141108045	2.12586206474	-1.68331088178	6.49909759212	-1.89732250821	2.30715746982	-0.161860159483	0.0892875036386	0.151284613089	-0.691644113452	0.305638153079	0.944058970773	0.412374076115	-0.610045727043	0.126649944608	0.453516621975	-0.0659409582108	0.0862084606186	0.772506972063	-0.101491969722	1.14057226385	14.2733524521	70.3077965706	-13.2157532621
38	0.597214903069	1.29510157792	-0.326706852762	3.89110538601	-0.320932814329	6.06207484902	-0.757203681751	0.742699922461	-1.70363860466	-0.0662392268693	0.00121706863296	0.633330618566	0.260410232668	0.975882395505	0.519710605741	0.478937747189	0.0508419508862	0.357341293631	0.727307323516	-0.392395593312	1.57151570102	20.0281157907	59.1650701053	-12.3550075367
39	3.41286921423	0.436695660166	0.463097363869	0.727765168365	0.945112798366	6.2044269358	0.330461523639	-0.0467272749865	-0.193614341229	-0.246884418304	0.0092229468201	0.312977149769	0.222530962083	0.423673282868	-0.187270884427	0.466594074365	0.052907351045	0.00605186121567	0.591090562682	-0.0191813780832	1.42170269686	11.5924832982	63.094483593	-5.54506833071
40	2.14766569828	-0.124791213252	-1.15265798725	3.53745901458	3.44794379697	4.5132092564	-0.417965575528	-0.0761778704648	0.123219201704	-0.0955105907127	0.352641870197	-0.412294835133	-0.289681756347	0.199237363342	-0.248560153594	0.635896548188	0.0647176197333	-0.00371945689282	0.443385437864	0.0466268918668	0.888093387013	15.391471233	70.4699186833	6.22045529646
41	2.06878203056	-1.30214058491	5.40576958724	1.52971647907	-2.01967226438	2.02859733583	-0.319063599538	0.662008774804	0.708181045969	-0.148098136057	-0.297312587818	-1.07158623319	-0.50366673724	1.75963159495	0.49318645284	0.701153100368	-0.0756275218012	0.203886095564	0.795657291986	-0.137372856039	1.44374179538	25.7333030368	75.9344703782	-9.60586707576
42	1.74902218958	-0.909790615216	2.02842976275	0.512904660323	-0.968929438994	7.48277494273	-0.380607371547	0.251549224794	0.0872296359054	-0.457596724565	-0.428466704376	-1.04615302634	-0.136356373802	0.764584065766	1.14569621826	0.721838863359	-0.0924423139854	0.0272745376298	0.791834922892	-0.0580729071292	1.09090324415	28.2219512309	70.9365747976	-5.39885399942
43	2.10392179773	0.280727621882	-7.54542112626	1.56226283156	-1.3309447497	2.10453875826	-0.974873963794	-0.0498873297241	-1.16729435955	0.159294850998	-0.031230796573	-0.496839754427	0.662247670553	-0.194703888467	0.725339893199	0.4880788944	-0.00805705076262	-0.0793508239105	0.710202842616	0.00374774375672	0.986603591087	16.6422563469	64.6783897171	14.4159708793
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45	8.08779003347	-0.452181817259	-5.32926760644	2.05546795524	7.11419823209	8.29511291167	-0.0897824139377	0.590689061382	-0.280780654996	-1.30927398917	0.365414626324	-1.48006156564	-0.959430553002	0.783444728602	-0.602214027604	0.74717253123	-0.120695988854	0.263273288558	0.958002906364	-0.00946886659692	0.955559870426	27.4244650966	109.065833283	-35.5772991313
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50	4.27746262731	-2.59687440714	1.79575367065	1.78073633872	-0.309999966971	3.71534547934	-1.44474085019	0.744431429939	0.520847517734	0.392303159202	1.08834546309	-0.758400322757	-0.425864337405	-0.324222399188	0.274226916352	0.656115019792	-0.178835275301	0.259278202338	0.916465779078	-0.457426758109	1.10787974629	25.6744436943	115.667097984	-17.4917655705
51	5.84879004725	7.57991783459	6.49985680932	2.01427197158	8.2847527509	7.46160017871	-0.16659047152	0.78701051003	-0.226794815794	1.3678333679	1.5362699735	-0.137443815663	0.593785754367	0.743689094416	-1.03132652867	0.884575254307	-0.142094776324	0.152897310744	0.64587564322	-0.0288830149638	0.890772107116	29.3896991614	103.155823404	-20.1219468502
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53	8.43537783536	-5.80912154767	-1.48641547679	5.36232156979	0.00281677901537	1.06358068478	-0.196803181145	0.203615381421	1.31903729288	0.733606881678	0.62865155416	-0.960206765659	0.682280457253	-0.0137705314516	-0.318599502521	0.479174224812	-0.125453951256	0.155423543806	0.640912964331	-0.198513157172	0.873319013394	2.5131427324	94.3377262792	-25.6000892557
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56	2.74098663879	0.943521150649	1.1457220024	3.62599935409	-1.83187841616	2.59008063202	-0.0265795227024	-0.0217898705491	0.0832710830259	0.175711038519	-0.0230894932101	0.0623614291315	0.140865148111	-0.0270755610605	0.104591134293	0.397624921818	-0.0925555582923	0.0352476048737	0.418181573717	-0.0619322200004	0.528391769171	-15.3357610989	89.3986196282	-22.3829223471
57	5.69780223696	-6.5843294463	-2.85934579305	2.02407852168	-0.300794734141	6.24631803161	-1.57381546056	-0.119371152635	-2.0762590841	0.355366038354	0.519725060232	1.37440708229	0.0823940903364	-0.450413918477	0.683249993677	0.521833301797	-0.0215607010625	0.224452053054	1.16876605639	-0.086314770505	1.34292784959	-24.1163326114	70.8116409676	-16.2643118898
58	5.90407101297	-7.89574052784	5.12987168037	1.99879258131	1.91128125742	8.31908170829	-0.82325488878	-0.687847003967	-1.25718159803	2.36190288286	1.29202814668	0.885251882273	-0.937337034939	-1.08767030339	-0.781873758211	0.830353851382	-0.0786950640641	0.130231638722	0.6687401057	-0.0630752542477	0.707267613459	-27.5490046291	81.8975287497	-21.3406251092
59	1.68785640267	0.174406697795	-0.316178598158	3.5047922134	-1.1583980835	0.821237590034	-0.255353642642	0.947778239779	-0.358335417684	-0.00273500458552	-0.355562686775	-1.05377947434	-0.035111226355	0.201947098472	0.265765233862	0.558665286216	0.0583682382754	0.0806189022457	0.847784619782	-0.145720428807	0.218354901666	-6.3227565434	94.0634660298	-27.2648196841
60	3.00977091985	-0.15146039982	-1.52615819218	4.55022773277	-2.01207457663	6.58785802603	0.272420970695	-0.0515613094054	0.327629338102	0.582435118604	-0.367982196413	1.65450680269	-1.11376973533	-0.783655247897	-0.201749345395	0.887584150005	0.0276766603571	0.297104323796	0.640371084114	-0.206453556132	1.67453967372	-94.748622149	66.3688353404	-41.1769133582
61	2.14473910142	0.597058574431	-1.32633549051	5.94749641901	-2.29455093413	8.03114627093	-0.504595555071	-0.262912599878	-0.339624228113	0.435322151866	-1.26240832597	-0.458149114817	-0.172077308481	-0.537831552555	1.5354273267	0.519585809048	0.0151647748814	0.00155549893201	0.771077656544	-0.213174072523	1.14463817338	-88.2861926217	57.3506591674	-43.1273765717
62	3.55118898897	1.92224061356	-2.15158960992	5.13092107639	-3.30153007668	5.75045931346	0.187496158931	0.143265693978	0.279870665281	-0.0476784956844	-0.213821217087	0.504217406011	-0.291622573301	-0.186007226976	-0.141318692093	0.442027892385	0.0495244171433	-0.0420286963511	0.479168685785	-0.0418911064596	0.945953536399	-87.4008697562	63.0059571479	-51.2309032228
63	2.28678747587	2.93446123406	0.594552200028	3.96014500929	-0.0596368425717	2.73461171826	0.277638880057	-0.0346591219656	0.743474884534	0.251374653667	-0.0883247713016	0.439392589927	-0.438577779109	-0.00340709874543	-0.18686697	0.486818617347	0.066533208271	0.148061257712	0.555868490447	-0.081027755091	1.34818564817	-83.4978623612	63.5320240237	-42.9751733611
64	1.29347450111	0.406396873826	-0.351162231915	0.39701346687	-0.641354857474	2.34900409463	-0.134646785264	0.164635951428	0.237565359387	-0.0941559260694	-0.124470305404	-0.154853877658	-0.113877615905	-0.0477136675044	0.198536319764	0.524125797747	0.0654046893368	-0.0233825471526	0.385898143796	-0.010761121085	0.748268599422	-84.2261521356	50.1959709195	-52.3316582353
65	5.10522961034	2.93511504062	1.79056296732	9.64312232296	2.98353270255	7.18440336	-0.251637228602	-0.615634225748	0.837555364618	-0.11318695632	0.0361923307468	1.10616078546	-0.419837393902	-0.0479155718648	0.655951808658	0.661989304638	0.146178200736	0.0677366341909	0.671645694107	0.251921063789	1.08389809942	-95.4339696043	67.5046803597	-59.7523084518
66	7.59447661833	-1.17205847667	0.956408460066	3.75656888338	-1.23677734074	1.72461674027	0.370051599304	-0.624961381547	1.34336002636	-0.538558616596	-0.100402535143	0.604701625749	0.754168032534	-0.700894087418	-0.145289779449	0.4846049637	-0.0551814572795	0.136874917039	0.463044724301	-0.121088441561	0.62450624343	-90.4795239287	46.6025738555	-47.6499107639
67	6.54605392558	-0.144448449264	-0.308557424941	3.44216452352	1.10796564678	0.923015828255	0.0487791047451	-0.175625463118	0.391830511788	0.0790589547108	-0.0934211503445	-0.368016074782	0.328651129843	-0.122905360566	0.123486858097	0.422130469344	-0.0420782561624	0.0116809054305	0.433980445083	0.0398194188149	0.49943055146	-69.7219224944	49.4868501958	-47.8989456813
68	4.95404125693	-2.60919062383	-1.42668862156	7.63741335958	5.15559270528	5.68882227865	-0.00116328177565	-0.746664648728	-0.534382771803	0.50116652877	0.707534956151	-0.990432906852	0.127087451004	0.88779104939	-0.666541080673	0.467299899815	0.0227350138515	-0.15314200385	0.695988982212	0.0614600166767	0.89311955231	-39.8487984615	34.873695749	-37.3674298556
69	4.69850925571	0.432478507108	-0.172822258989	4.56258760974	0.79421115049	3.58580323643	0.269883274097	-0.416015198467	-0.329086962654	0.505715582153	0.0642939658343	-0.440890880013	0.0660819065713	0.886144639308	-0.213248201678	0.482970950763	-0.00331453560738	0.0236228553027	0.690911740234	-0.156936739319	0.364713018433	-47.064137426	41.9458923817	-41.6745013348
70	2.15263065243	-0.49586236972	-0.505613972335	5.7678656652	-0.0785540322288	5.54096166937	0.0515107323237	-0.192448691851	-0.402187684254	-0.223539792534	0.114500013124	-0.772955180652	-0.0612656786918	-0.0833291091576	0.158071402156	0.408973975543	0.00676003460312	0.0394558029546	0.412279527821	0.00980465831222	0.644618645097	-49.052707029	32.4623330987	-43.6038944521
71	2.89014145998	-1.10772330447	-0.364645349745	3.8395983825	-0.872850309769	3.82435222805	-0.102913526157	0.0890390538454	0.23957576675	-0.00312544434543	0.0975628105421	-0.038067023051	-0.105040605591	-0.22879636236	-0.076077552049	0.432132672668	-0.014160348197	0.0188047479529	0.321372366665	-0.0452886552616	0.626031041831	-53.1491020984	46.1575957285	-48.1739179845
72	4.38988469982	2.36296911261	-3.41491842154	7.81667218608	-3.69057639532	3.50448558553	0.605073744227	-0.480400640516	0.315186698126	0.142577091223	-0.664056788285	-0.742131058554	0.447052420464	0.400255604034	-0.0153857751515	0.642484320373	0.0382359801595	-0.171636468027	0.65176503964	-0.0194250492184	0.507304780025	-41.2214824248	34.9096649629	-56.0372960751
73	0.448346990191	0.167629266948	-0.112171880997	1.6282965211	-0.74666678372	1.48902054956	-0.103543375612	-0.720721624575	0.280981515315	-0.23313641836	0.537619673609	-0.421413130193	0.134599490053	0.584519824923	-0.116023190582	0.693525555944	0.0366049459138	-0.0687220424677	0.643753330655	-0.175474666936	0.478876968741	-43.6866744573	49.0539173544	-48.8473933898
74	6.5820900155	-0.939773696554	-2.27620707462	3.67596554317	-2.78934091424	2.44646553273	0.185626557091	-0.0965334147578	0.299464637529	-0.814246613634	-0.23355710452	-0.201295395627	-0.0318474869348	0.301347197704	0.0268707428786	0.540133777262	0.0673636926545	-0.0192384138253	0.339632595547	-0.0342220555339	0.520343965993	-65.3334187094	48.6226400698	-47.893714976
75	4.1869520065	1.46393295543	-0.643004701105	3.17924810487	0.370436793758	5.77594355242	0.08525358933	0.182569339464	0.0271470661549	0.0921922637691	0.309486665536	0.218681125569	-0.461001162253	-0.384980160691	-0.369411386031	0.441600023202	-0.0284926381356	0.184814247871	0.603871636298	-0.0272451770518	1.20681902705	-49.443872267	45.1630957144	-3.89878885259
76	1.53613461239	-0.879284104558	0.0881562825022	3.11956474357	0.0597822467445	4.87513646762	-0.0137007640496	-0.258549824921	0.230569566006	0.0835584356229	0.178104129674	0.366821878849	-0.0579024041475	-0.160095561548	-0.221225109009	0.34249146724	-0.0176309254337	0.0538910052043	0.443566168453	0.0273803978119	0.909606122483	-56.3536244877	40.9977319072	-0.647334289743
77	0.733403436521	1.28237199328	1.37650162524	2.5698558993	1.67131488744	2.88027445664	-0.0546558035403	-0.0125914808221	-0.57155261909	-0.156204804463	0.209324784702	-0.72209982204	0.119080426363	0.425278084873	-0.349001879906	0.451506616551	-0.0816608425872	0.0949054123737	0.454372604143	0.0146043706106	0.849933931775	-56.1652040001	28.4664711731	-7.10161162382
78	4.67314671755	-0.882935137792	-0.487993247017	1.43543254094	1.22716701769	6.9835638977	0.0341698914485	-0.141122814649	-0.0751549694426	0.502809806868	-0.16691503913	-0.000148679160428	0.813010567945	0.668751597233	0.210789264093	0.59656473642	-0.0640489605467	0.0368671226998	0.515417001622	0.0139067477164	0.835334647079	-46.3771459241	33.5643486771	5.28254460451
79	5.07623184644	-2.39407817199	2.40061576617	5.94560651207	4.35362240551	8.82439282273	0.235760788676	0.466401484225	0.561052183092	0.309991473952	0.0120034289531	0.179864634087	-0.683094168213	0.492410487745	0.0561134957642	0.534376439748	-0.0965734310483	0.082340136316	0.644486763001	0.109282768115	0.474009654851	-53.7122301381	27.8301358844	-21.4096533654
80	2.60383855944	0.188451043671	-0.420825770236	1.55360192899	1.50426254954	2.29881638456	-0.0574102161738	-0.030665662687	0.28783226232	-0.0362016074694	-0.101106333446	-0.110134565924	0.094016704276	0.11270905348	0.0141031982884	0.358918536471	0.0450787180812	0.0530722392264	0.504698743507	0.0477256493301	0.764214903871	-71.2291733934	31.0960760601	-10.754103496
81	1.21502923756	1.22912775485	2.73114553352	2.00611042363	0.247369443824	6.80949385478	0.341867040302	-0.400746153406	0.395117655509	-1.16967327439	-1.30111450705	0.909945557954	0.563591570139	-2.45701931757	1.22289639595	0.480704515669	-0.259801363833	-0.145383776117	1.1027029194	-0.128761217002	1.01821540817	-98.1263882139	24.2390910305	-34.1771632134
82	3.48515590648	1.92741685825	-0.884333788422	5.66975468955	3.59535291957	4.0217016526	0.0277884424709	0.119411885218	0.669430195059	-0.300824639965	0.30503496671	0.91422443736	-0.530643638064	-0.667249181314	-0.205741745655	0.452162124464	0.0116870373274	0.0295430056021	0.643599284933	0.12906333311	0.684740755045	-93.5890570407	31.5175304828	-28.8957082771
83	5.14999746111	3.19746631441	1.15283373552	6.90730342201	-0.200263496903	7.08574866942	0.0689858461782	-0.0139529227332	-1.22711696191	-0.844987264621	0.304724336295	-0.263751309683	-0.214239613796	0.849103265333	-0.33729710661	0.581373957296	-0.0860826385084	0.0499155382787	0.493623530582	0.039461351933	0.585675959216	-85.4412970086	16.1661569726	-25.7638497967
84	4.02065613373	1.77770276805	2.84841006935	8.48489375199	-2.10837354822	3.01057861959	-0.490742546136	-0.214403613437	0.0320197570757	-0.338382778658	0.307030030113	0.405532553587	0.361600728091	0.335185723248	0.312853006698	0.576032956163	0.0299471296307	0.100079968283	0.54900876638	-0.0782713974023	0.519416651802	-90.7978381016	25.3991264596	-32.5636676053
85	0.754599395761	-0.31245875176	0.899116964911	1.24268817374	0.69583833832	1.83050097515	-0.131453320382	-0.0580008593781	-0.40233372754	-0.0655948446412	-0.0707540935078	-0.177616526075	0.0243039650547	-0.137362554855	0.15210860571	0.465723234365	-0.0108546446825	0.0741500357881	0.510555648806	0.148931761338	0.832323427477	-86.1980706928	27.3876314712	-16.1495779784
86	7.74593560483	-2.77608481437	-3.60256743779	7.3466364219	2.93332763112	6.44482144661	-0.469744838909	-0.11655344329	-1.6320193175	0.63237232157	0.32944616228	0.351619380785	0.615278267487	0.0545530151028	0.184317520635	0.417625389388	-0.0365870749405	0.108019636378	0.67102308163	0.0512515592049	0.780047472343	-98.584115688	16.6457840571	-20.2925658918
87	8.68270958277	-2.15438869824	-3.97678470389	1.04188080787	0.426328242661	1.36747447885	0.329103444767	0.0927083721502	0.821833892071	-0.159056584106	-0.117669078277	-0.696273173281	-0.133079251778	-0.186613145471	-0.127904893571	0.411056676757	-0.00336375985911	0.0140488074576	0.529426641412	-0.0437741698993	0.805218857702	-79.9923970617	31.82376982	-12.0211181257
88	7.30121052338	-0.197178727063	-1.26639060864	7.57246289791	4.03382406326	2.29632907407	-0.244183309095	0.491657616237	-0.25966197701	-0.207267368957	1.16951429051	-1.98601679364	-0.3161108281	1.09196761141	-0.78887358181	0.582187025893	-0.00514670892477	0.172988192583	0.640099928786	-0.18383423322	1.14687041266	28.5038724898	26.5612558725	-35.8655007995
89	5.63727012983	-0.337905303222	-2.82145238619	4.15412675652	3.55265101048	8.97200186266	0.613804387872	0.454540018626	0.739890009286	-0.0607119016516	-0.189627081305	-0.0315347870923	-0.741898318202	-0.650223603794	-0.521815183796	0.388500290886	-0.000123295523512	0.0251388854936	0.491183833849	0.113629488088	0.746073111036	17.6581655148	23.2175083506	-25.8427813631
90	2.1063703994	0.188866473506	-0.870958932298	5.07567312335	-1.31665008599	5.37967857918	-0.148743433966	0.0201137422828	0.459237865474	-0.421431762841	0.285391907099	-0.785564987518	-0.0980166796836	0.0455392030568	-0.274167719376	0.305149041065	0.0272759384667	0.0384688260249	0.568066965774	0.113404355798	0.858350859537	17.4579774073	23.36312936	-31.6689546123
91	2.1548794574	1.41826650087	-1.78935893667	3.22202088175	0.822274117827	2.85713338323	-0.178292191315	-0.0539273179073	-0.280704746494	0.0565923820516	-0.1168707901	-1.32411932034	0.289386036318	0.666172390958	0.223535423617	0.430503183762	0.0103236906568	0.0916314156175	0.511276843107	0.110602643647	0.919981453072	19.9231040711	8.44710586801	-22.6798215635
92	5.53184340054	-2.57065223503	-2.99375533475	5.92813761078	5.15240299313	9.65448911734	-0.201698279072	-0.767985268266	-0.000311829410565	0.519090657535	0.702159587628	-0.754957632618	0.349637667581	1.59042690344	-0.509027914459	0.516516949983	0.0896552815414	-0.00985722475157	0.878056402483	0.0611289938568	0.976925311821	27.977555978	24.2819973289	-19.6698103488
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94	5.19504217584	-2.52041432044	-1.92047960542	5.8788530321	1.19189925066	2.14995828573	0.137191768584	0.107649509147	0.48966200212	0.513618023948	0.505802698634	-1.07915851778	0.315495514003	0.246869279933	-0.821528652483	0.45254735061	0.0346548965412	-0.0151264525887	0.700714276788	-0.1122747519	0.837691806803	2.28753932099	11.4446826074	-28.0071993397
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247	2.00735990749	3.53140733495	1.7444941146	2.00459275314	-2.39147808695	2.00350022658	-1.75171192629	0.224552925022	1.04169329217	-0.166545059732	-1.80337882922	-1.5392375879	0.29766291266	0.862901520663	3.07087232125	1.32485400584	-0.656378877181	0.0500732907415	1.27802425421	0.299228784503	0.784054764949	17.3985590236	19.9362640319	-16.3334143008
248	1.4513436578	-2.01308886565	-3.36021125519	2.85490702491	4.61553243587	7.81966247547	0.151161055044	-0.319933806067	0.0306076846078	0.805195599965	-1.03996986003	-1.74220870287	1.96065534148	0.381188955083	0.837556731624	0.999134482978	0.461154227735	0.121916586269	0.896703970075	0.211775317165	1.82298866347	-12.2838915879	0.35573054589	-20.2441468375
249	7.31410475314	-0.13287429532	5.61640517879	2.92418267667	-0.768976246565	5.20150096534	-0.130688437772	-0.034182287034	-0.661338046377	0.33906904548	-0.98817002788	-0.95360710998	-0.333186792462	0.786932937304	0.95854897463	0.491443044676	-0.177020612542	0.162057220692	1.05338973415	-0.253506868542	1.53325985482	-14.7080862181	-4.79690237668	-19.8737185075
250	7.01152414831	2.7283130808	4.75937681317	1.60328495971	-0.38679182244	2.00109566198	0.712205911406	-0.0813839126836	-0.137106924336	-0.271376025109	0.676347530155	1.27236790134	-0.469696024277	-2.02120708432	-1.23486521038	0.913558168923	0.126474387094	-0.318435259479	0.871447644738	0.151777912185	0.968465107409	-52.6726842211	27.1158922176	-79.5720569785
251	7.81081708017	7.70679989709	3.07382066163	1.99496683784	4.68475375226	2.00076695458	0.881173812	1.16932287287	0.998195780365	-0.0757030181806	2.4378916081	-0.0349224282898	-2.02068331712	0.296612896925	-3.29258702845	0.570899955342	-0.149642219862	0.179166559699	1.06467600747	-0.0439564784267	0.832158424896	-50.1890228324	27.5217804942	-84.7470862344
252	2.21852714911	1.65891752305	1.34669632276	2.33690562189	1.24811302971	1.88377029886	-0.367511018306	-0.854742641521	0.572010215738	1.61952235637	0.625194659943	-0.359659226525	-0.513705729844	1.0466398195	-0.00630941720145	0.690121315092	-0.0563659487132	-0.0789501649142	0.997329972401	-0.480846523731	0.965219408569	-79.7097295321	27.1728878697	-65.5112453524
253	1.02080869914	1.45947464446	0.892426754815	2.19073974658	1.77636589142	3.63719530588	0.156959193632	-0.153243095356	-0.21034395087	0.033172307365	-0.0496502744371	0.152019996729	0.567524007834	-0.630541281975	-0.0296376481266	0.762711335454	0.0903186733728	-0.0405290558405	0.812830267599	-0.0391703101363	0.310675138481	-82.5282221202	28.7296338433	-60.3201041378
254	4.70604365925	5.9930629609	0.432849630544	8.50856722402	3.14045368891	7.81069236212	-0.17095939039	1.19921776628	-1.7118102322	-0.442435100358	0.923486342124	-0.99089317255	-0.314912741791	-0.189674808225	-0.683673340343	0.556735640819	-0.208696979965	-0.0853881887731	0.985885237318	0.212366147351	1.53018493418	-55.3909580965	84.4848639979	-16.9428889498
255	1.6212580865	-3.04204812198	-0.69863119927	5.99535960488	2.30717816395	3.64930655514	-0.167423459872	1.58813856485	-0.737025317521	0.344014872346	0.0666237691359	0.287415812865	-0.0785540660724	0.718449362552	0.0616332533388	0.341851263717	0.0161817321424	0.0417481420851	0.940673346139	-0.0199986189583	1.23345639801	-52.226208429	88.0632654834	-20.7202755045
256	5.11289580656	4.81446853602	-3.64050375055	1.99846136445	0.457709363062	5.29500919369	0.333498841412	-0.387897416992	0.428641320074	0.582051365625	-0.220593304677	1.46575006053	0.17104658789	0.372839119027	-0.222913618865	0.667976285106	0.139993507399	-0.0106339787167	1.40171896686	0.118259634047	1.46955198995	-83.392604469	76.9431714103	-7.14709988436
257	2.46225113247	1.47003479991	3.31039615591	2.31259334691	0.0327103310205	7.09262656897	0.990696883159	-0.183487059989	1.38180549593	0.1454091164	0.935698710277	0.453557258085	-1.54597000688	-0.333629035456	-1.83943022542	0.508254318654	-0.17967480206	0.573866803593	1.29347945681	0.00629738414017	2.02633918866	-86.2683393718	75.0198347656	-2.72370397752
258	2.00000088271	5.29230653511	-1.52742121562	1.99872578452	5.97000350885	2.00442476628	-1.2416001928	0.704486084065	1.66408859971	-1.84232919663	-2.70738998962	-1.69055173999	-0.990184148926	2.64238458379	3.57215437631	1.64349053595	-0.465985279397	-0.165963718355	1.08797301622	0.302130041824	1.44434810887	-87.2985462288	22.4232933428	12.3579855849
259	1.99434465857	-3.68253273699	1.99759354775	6.11010010922	4.72322673659	2.0058622013	-0.532634292916	0.542527532812	0.760833741162	-0.597479713612	-1.23683750013	1.31849412144	1.32683368743	0.764158106205	1.62150953221	0.653615745224	0.135712897539	0.0276884796213	1.23742868917	-0.149434237409	0.722953899251	-89.8518825919	25.9715530753	8.58355428394

Refinement TLS group

Refine-ID: X-RAY DIFFRACTION

ID	Refine TLS-ID	Selection details	Auth asym-ID	Label asym-ID	Auth seq-ID	Label seq-ID
1	1	chain 'R' and (resid 301 through 301 )	R	EC	301
2	2	chain 'R' and (resid 302 through 302 )	R	FC	302
3	3	chain 'S' and (resid 301 through 301 )	S	CA	301
4	4	chain 'S' and (resid 302 through 302 )	S	CB	302
5	5	chain 'T' and (resid 301 through 301 )	T	CC	301
6	6	chain 'T' and (resid 302 through 302 )	T	CD	302
7	7	chain 'V' and (resid 302 through 302 )	V	QC	302
8	8	chain 'W' and (resid 302 through 302 )	W	UC	302
9	9	chain 'X' and (resid 302 through 302 )	X	YC	302
10	10	chain 'Y' and (resid 303 through 303 )	Y	CD	303
11	11	chain 'Z' and (resid 301 through 301 )	Z	DD	301
12	12	chain 'bb' and (resid 657 through 658 )	bb	GA	657 - 658
13	13	chain 'cc' and (resid 659 through 660 )	cc	HA	659 - 660
14	14	chain 'CC' and (resid 302 through 302 )	CC	FD	302
15	15	chain 'DD' and (resid 302 through 302)	DD	HD	302
16	16	chain 'ff' and (resid 665 through 666 )	ff	IA	665 - 666
17	17	chain 'FF' and (resid 302 through 302 )	FF	LD	302
18	18	chain 'A' and (resid 2 through 47 )	A	A	2 - 47	1 - 46
19	19	chain 'A' and (resid 48 through 128 )	A	A	48 - 128	47 - 127
20	20	chain 'A' and (resid 129 through 162 )	A	A	129 - 162	128 - 161
21	21	chain 'A' and (resid 163 through 207 )	A	A	163 - 207	162 - 206
22	22	chain 'N' and (resid 3 through 12 )	N	B	3 - 12	1 - 10
23	23	chain 'N' and (resid 13 through 31 )	N	B	13 - 31	11 - 29
24	24	chain 'N' and (resid 32 through 72 )	N	B	32 - 72	30 - 70
25	25	chain 'N' and (resid 73 through 139 )	N	B	73 - 139	71 - 137
26	26	chain 'N' and (resid 140 through 149 )	N	B	140 - 149	138 - 147
27	27	chain 'N' and (resid 150 through 207 )	N	B	150 - 207	148 - 205
28	28	chain 'B' and (resid 3 through 19 )	B	C	3 - 19	1 - 17
29	29	chain 'B' and (resid 20 through 31 )	B	C	20 - 31	18 - 29
30	30	chain 'B' and (resid 32 through 73 )	B	C	32 - 73	30 - 71
31	31	chain 'B' and (resid 74 through 139 )	B	C	74 - 139	72 - 137
32	32	chain 'B' and (resid 140 through 149 )	B	C	140 - 149	138 - 147
33	33	chain 'B' and (resid 150 through 179 )	B	C	150 - 179	148 - 177
34	34	chain 'B' and (resid 180 through 207 )	B	C	180 - 207	178 - 205
35	35	chain 'C' and (resid 3 through 19 )	C	D	3 - 19	1 - 17
36	36	chain 'C' and (resid 20 through 31 )	C	D	20 - 31	18 - 29
37	37	chain 'C' and (resid 32 through 47 )	C	D	32 - 47	30 - 45
38	38	chain 'C' and (resid 48 through 72 )	C	D	48 - 72	46 - 70
39	39	chain 'C' and (resid 73 through 95 )	C	D	73 - 95	71 - 93
40	40	chain 'C' and (resid 96 through 129 )	C	D	96 - 129	94 - 127
41	41	chain 'C' and (resid 130 through 149 )	C	D	130 - 149	128 - 147
42	42	chain 'C' and (resid 150 through 162 )	C	D	150 - 162	148 - 160
43	43	chain 'C' and (resid 163 through 179 )	C	D	163 - 179	161 - 177
44	44	chain 'C' and (resid 180 through 207 )	C	D	180 - 207	178 - 205
45	45	chain 'D' and (resid 3 through 20 )	D	E	3 - 20	1 - 18
46	46	chain 'D' and (resid 21 through 31 )	D	E	21 - 31	19 - 29
47	47	chain 'D' and (resid 32 through 73 )	D	E	32 - 73	30 - 71
48	48	chain 'D' and (resid 74 through 95 )	D	E	74 - 95	72 - 93
49	49	chain 'D' and (resid 96 through 139 )	D	E	96 - 139	94 - 137
50	50	chain 'D' and (resid 140 through 149 )	D	E	140 - 149	138 - 147
51	51	chain 'D' and (resid 150 through 162 )	D	E	150 - 162	148 - 160
52	52	chain 'D' and (resid 163 through 179 )	D	E	163 - 179	161 - 177
53	53	chain 'D' and (resid 180 through 207 )	D	E	180 - 207	178 - 205
54	54	chain 'E' and (resid 3 through 31 )	E	F	3 - 31	1 - 29
55	55	chain 'E' and (resid 32 through 83 )	E	F	32 - 83	30 - 81
56	56	chain 'E' and (resid 84 through 138 )	E	F	84 - 138	82 - 136
57	57	chain 'E' and (resid 139 through 149 )	E	F	139 - 149	137 - 147
58	58	chain 'E' and (resid 150 through 162 )	E	F	150 - 162	148 - 160
59	59	chain 'E' and (resid 163 through 207 )	E	F	163 - 207	161 - 205
60	60	chain 'F' and (resid 3 through 19 )	F	G	3 - 19	1 - 17
61	61	chain 'F' and (resid 20 through 31 )	F	G	20 - 31	18 - 29
62	62	chain 'F' and (resid 32 through 57 )	F	G	32 - 57	30 - 55
63	63	chain 'F' and (resid 58 through 83 )	F	G	58 - 83	56 - 81
64	64	chain 'F' and (resid 84 through 139 )	F	G	84 - 139	82 - 137
65	65	chain 'F' and (resid 140 through 151 )	F	G	140 - 151	138 - 149
66	66	chain 'F' and (resid 152 through 177 )	F	G	152 - 177	150 - 175
67	67	chain 'F' and (resid 178 through 207 )	F	G	178 - 207	176 - 205
68	68	chain 'G' and (resid 0 through 20 )	G	H	0 - 20	1 - 21
69	69	chain 'G' and (resid 21 through 31 )	G	H	21 - 31	22 - 32
70	70	chain 'G' and (resid 32 through 72 )	G	H	32 - 72	33 - 73
71	71	chain 'G' and (resid 73 through 129 )	G	H	73 - 129	74 - 129
72	72	chain 'G' and (resid 130 through 149 )	G	H	130 - 149	130 - 149
73	73	chain 'G' and (resid 150 through 176 )	G	H	150 - 176	150 - 176
74	74	chain 'G' and (resid 177 through 207 )	G	H	177 - 207	177 - 207
75	75	chain 'H' and (resid 3 through 31 )	H	I	3 - 31	1 - 29
76	76	chain 'H' and (resid 32 through 83 )	H	I	32 - 83	30 - 81
77	77	chain 'H' and (resid 84 through 139 )	H	I	84 - 139	82 - 137
78	78	chain 'H' and (resid 140 through 162 )	H	I	140 - 162	138 - 160
79	79	chain 'H' and (resid 163 through 179 )	H	I	163 - 179	161 - 177
80	80	chain 'H' and (resid 180 through 207 )	H	I	180 - 207	178 - 205
81	81	chain 'I' and (resid 2 through 12 )	I	J	2 - 12	1 - 11
82	82	chain 'I' and (resid 13 through 31 )	I	J	13 - 31	12 - 30
83	83	chain 'I' and (resid 32 through 47 )	I	J	32 - 47	31 - 46
84	84	chain 'I' and (resid 48 through 72 )	I	J	48 - 72	47 - 71
85	85	chain 'I' and (resid 73 through 128 )	I	J	73 - 128	72 - 127
86	86	chain 'I' and (resid 129 through 162 )	I	J	129 - 162	128 - 161
87	87	chain 'I' and (resid 163 through 207 )	I	J	163 - 207	162 - 206
88	88	chain 'J' and (resid 1 through 20 )	J	K	1 - 20	1 - 20
89	89	chain 'J' and (resid 21 through 47 )	J	K	21 - 47	21 - 47
90	90	chain 'J' and (resid 48 through 95 )	J	K	48 - 95	48 - 95
91	91	chain 'J' and (resid 96 through 139 )	J	K	96 - 139	96 - 139
92	92	chain 'J' and (resid 140 through 162 )	J	K	140 - 162	140 - 162
93	93	chain 'J' and (resid 163 through 180 )	J	K	163 - 180	163 - 180
94	94	chain 'J' and (resid 181 through 207 )	J	K	181 - 207	181 - 207
95	95	chain 'K' and (resid 3 through 31 )	K	L	3 - 31	1 - 29
96	96	chain 'K' and (resid 32 through 72 )	K	L	32 - 72	30 - 70
97	97	chain 'K' and (resid 73 through 139 )	K	L	73 - 139	71 - 137
98	98	chain 'K' and (resid 140 through 149 )	K	L	140 - 149	138 - 147
99	99	chain 'K' and (resid 150 through 162 )	K	L	150 - 162	148 - 160
100	100	chain 'K' and (resid 163 through 207 )	K	L	163 - 207	161 - 205
101	101	chain 'L' and (resid 3 through 19 )	L	M	3 - 19	1 - 17
102	102	chain 'L' and (resid 20 through 31 )	L	M	20 - 31	18 - 29
103	103	chain 'L' and (resid 32 through 72 )	L	M	32 - 72	30 - 70
104	104	chain 'L' and (resid 73 through 129 )	L	M	73 - 129	71 - 127
105	105	chain 'L' and (resid 130 through 149 )	L	M	130 - 149	128 - 147
106	106	chain 'L' and (resid 150 through 162 )	L	M	150 - 162	148 - 160
107	107	chain 'L' and (resid 163 through 207 )	L	M	163 - 207	161 - 205
108	108	chain 'M' and (resid 3 through 18 )	M	N	3 - 18	1 - 16
109	109	chain 'M' and (resid 19 through 31 )	M	N	19 - 31	17 - 29
110	110	chain 'M' and (resid 32 through 72 )	M	N	32 - 72	30 - 70
111	111	chain 'M' and (resid 73 through 128 )	M	N	73 - 128	71 - 126
112	112	chain 'M' and (resid 129 through 149 )	M	N	129 - 149	127 - 145
113	113	chain 'M' and (resid 150 through 162 )	M	N	150 - 162	146 - 158
114	114	chain 'M' and (resid 163 through 207 )	M	N	163 - 207	159 - 203
115	115	chain 'O' and (resid 3 through 47 )	O	O	3 - 47	1 - 45
116	116	chain 'O' and (resid 48 through 72 )	O	O	48 - 72	46 - 70
117	117	chain 'O' and (resid 73 through 129 )	O	O	73 - 129	71 - 127
118	118	chain 'O' and (resid 130 through 162 )	O	O	130 - 162	128 - 160
119	119	chain 'O' and (resid 163 through 207 )	O	O	163 - 207	161 - 205
120	120	chain 'P' and (resid 0 through 12 )	P	P	0 - 12	1 - 13
121	121	chain 'P' and (resid 13 through 31 )	P	P	13 - 31	14 - 32
122	122	chain 'P' and (resid 32 through 47 )	P	P	32 - 47	33 - 48
123	123	chain 'P' and (resid 48 through 72 )	P	P	48 - 72	49 - 73
124	124	chain 'P' and (resid 73 through 138 )	P	P	73 - 138	74 - 139
125	125	chain 'P' and (resid 139 through 149 )	P	P	139 - 149	140 - 150
126	126	chain 'P' and (resid 150 through 162 )	P	P	150 - 162	151 - 163
127	127	chain 'P' and (resid 163 through 207 )	P	P	163 - 207	164 - 208
128	128	chain 'Q' and (resid 3 through 31 )	Q	Q	3 - 31	1 - 29
129	129	chain 'Q' and (resid 32 through 129 )	Q	Q	32 - 129	30 - 127
130	130	chain 'Q' and (resid 130 through 149 )	Q	Q	130 - 149	128 - 147
131	131	chain 'Q' and (resid 150 through 176 )	Q	Q	150 - 176	148 - 174
132	132	chain 'Q' and (resid 177 through 207 )	Q	Q	177 - 207	175 - 205
133	133	chain 'R' and (resid 3 through 20 )	R	R	3 - 20	1 - 18
134	134	chain 'R' and (resid 21 through 46 )	R	R	21 - 46	19 - 44
135	135	chain 'R' and (resid 47 through 72 )	R	R	47 - 72	45 - 70
136	136	chain 'R' and (resid 73 through 128 )	R	R	73 - 128	71 - 126
137	137	chain 'R' and (resid 129 through 162 )	R	R	129 - 162	127 - 160
138	138	chain 'R' and (resid 163 through 207 )	R	R	163 - 207	161 - 205
139	139	chain 'S' and (resid 3 through 31 )	S	S	3 - 31	1 - 29
140	140	chain 'S' and (resid 32 through 139 )	S	S	32 - 139	30 - 137
141	141	chain 'S' and (resid 140 through 162 )	S	S	140 - 162	138 - 160
142	142	chain 'S' and (resid 163 through 207 )	S	S	163 - 207	161 - 205
143	143	chain 'T' and (resid 3 through 31 )	T	T	3 - 31	1 - 29
144	144	chain 'T' and (resid 32 through 47 )	T	T	32 - 47	30 - 45
145	145	chain 'T' and (resid 48 through 72 )	T	T	48 - 72	46 - 70
146	146	chain 'T' and (resid 73 through 138 )	T	T	73 - 138	71 - 136
147	147	chain 'T' and (resid 139 through 149 )	T	T	139 - 149	137 - 147
148	148	chain 'T' and (resid 150 through 179 )	T	T	150 - 179	148 - 177
149	149	chain 'T' and (resid 180 through 207 )	T	T	180 - 207	178 - 205
150	150	chain 'U' and (resid 1 through 31 )	U	U	1 - 31	1 - 31
151	151	chain 'U' and (resid 32 through 129 )	U	U	32 - 129	32 - 129
152	152	chain 'U' and (resid 130 through 180 )	U	U	130 - 180	130 - 180
153	153	chain 'U' and (resid 181 through 207 )	U	U	181 - 207	181 - 207
154	154	chain 'V' and (resid 3 through 46 )	V	V	3 - 46	1 - 44
155	155	chain 'V' and (resid 47 through 129 )	V	V	47 - 129	45 - 127
156	156	chain 'V' and (resid 130 through 162 )	V	V	130 - 162	128 - 160
157	157	chain 'V' and (resid 163 through 207 )	V	V	163 - 207	161 - 205
158	158	chain 'W' and (resid 5 through 19 )	W	W	5 - 19	1 - 15
159	159	chain 'W' and (resid 20 through 31 )	W	W	20 - 31	16 - 27
160	160	chain 'W' and (resid 32 through 73 )	W	W	32 - 73	28 - 69
161	161	chain 'W' and (resid 74 through 139 )	W	W	74 - 139	70 - 135
162	162	chain 'W' and (resid 140 through 160 )	W	W	140 - 160	136 - 154
163	163	chain 'W' and (resid 161 through 179 )	W	W	161 - 179	155 - 173
164	164	chain 'W' and (resid 180 through 207 )	W	W	180 - 207	174 - 201
165	165	chain 'X' and (resid 3 through 12 )	X	X	3 - 12	1 - 10
166	166	chain 'X' and (resid 13 through 46 )	X	X	13 - 46	11 - 44
167	167	chain 'X' and (resid 47 through 72 )	X	X	47 - 72	45 - 70
168	168	chain 'X' and (resid 73 through 129 )	X	X	73 - 129	71 - 127
169	169	chain 'X' and (resid 130 through 149 )	X	X	130 - 149	128 - 147
170	170	chain 'X' and (resid 150 through 162 )	X	X	150 - 162	148 - 160
171	171	chain 'X' and (resid 163 through 207 )	X	X	163 - 207	161 - 205
172	172	chain 'Y' and (resid 3 through 20 )	Y	Y	3 - 20	1 - 18
173	173	chain 'Y' and (resid 21 through 31 )	Y	Y	21 - 31	19 - 29
174	174	chain 'Y' and (resid 32 through 73 )	Y	Y	32 - 73	30 - 71
175	175	chain 'Y' and (resid 74 through 129 )	Y	Y	74 - 129	72 - 127
176	176	chain 'Y' and (resid 130 through 149 )	Y	Y	130 - 149	128 - 147
177	177	chain 'Y' and (resid 150 through 162 )	Y	Y	150 - 162	148 - 160
178	178	chain 'Y' and (resid 163 through 207 )	Y	Y	163 - 207	161 - 205
179	179	chain 'Z' and (resid 3 through 12 )	Z	Z	3 - 12	1 - 10
180	180	chain 'Z' and (resid 13 through 31 )	Z	Z	13 - 31	11 - 29
181	181	chain 'Z' and (resid 32 through 46 )	Z	Z	32 - 46	30 - 44
182	182	chain 'Z' and (resid 47 through 128 )	Z	Z	47 - 128	45 - 126
183	183	chain 'Z' and (resid 129 through 149 )	Z	Z	129 - 149	127 - 147
184	184	chain 'Z' and (resid 150 through 160 )	Z	Z	150 - 160	148 - 158
185	185	chain 'Z' and (resid 161 through 207 )	Z	Z	161 - 207	159 - 205
186	186	chain 'AA' and (resid 5 through 21 )	AA	AA	5 - 21	1 - 17
187	187	chain 'AA' and (resid 22 through 31 )	AA	AA	22 - 31	18 - 27
188	188	chain 'AA' and (resid 32 through 83 )	AA	AA	32 - 83	28 - 79
189	189	chain 'AA' and (resid 84 through 129 )	AA	AA	84 - 129	80 - 125
190	190	chain 'AA' and (resid 130 through 207 )	AA	AA	130 - 207	126 - 202
191	191	chain 'BB' and (resid 3 through 17 )	BB	AB	3 - 17	1 - 15
192	192	chain 'BB' and (resid 18 through 31 )	BB	AB	18 - 31	16 - 29
193	193	chain 'BB' and (resid 32 through 57 )	BB	AB	32 - 57	30 - 55
194	194	chain 'BB' and (resid 58 through 83 )	BB	AB	58 - 83	56 - 81
195	195	chain 'BB' and (resid 84 through 129 )	BB	AB	84 - 129	82 - 127
196	196	chain 'BB' and (resid 130 through 149 )	BB	AB	130 - 149	128 - 147
197	197	chain 'BB' and (resid 150 through 162 )	BB	AB	150 - 162	148 - 160
198	198	chain 'BB' and (resid 163 through 207 )	BB	AB	163 - 207	161 - 205
199	199	chain 'CC' and (resid 3 through 19 )	CC	AC	3 - 19	1 - 17
200	200	chain 'CC' and (resid 20 through 31 )	CC	AC	20 - 31	18 - 29
201	201	chain 'CC' and (resid 32 through 139 )	CC	AC	32 - 139	30 - 137
202	202	chain 'CC' and (resid 140 through 151 )	CC	AC	140 - 151	138 - 149
203	203	chain 'CC' and (resid 152 through 207 )	CC	AC	152 - 207	150 - 205
204	204	chain 'DD' and (resid 3 through 31 )	DD	AD	3 - 31	1 - 26
205	205	chain 'DD' and (resid 32 through 149 )	DD	AD	32 - 149	27 - 141
206	206	chain 'DD' and (resid 150 through 207 )	DD	AD	150 - 207	142 - 199
207	207	chain 'EE' and (resid 3 through 46 )	EE	EA	3 - 46	1 - 44
208	208	chain 'EE' and (resid 47 through 129 )	EE	EA	47 - 129	45 - 127
209	209	chain 'EE' and (resid 130 through 162 )	EE	EA	130 - 162	128 - 160
210	210	chain 'EE' and (resid 163 through 207 )	EE	EA	163 - 207	161 - 205
211	211	chain 'FF' and (resid 3 through 31 )	FF	FA	3 - 31	1 - 29
212	212	chain 'FF' and (resid 32 through 47 )	FF	FA	32 - 47	30 - 45
213	213	chain 'FF' and (resid 48 through 139 )	FF	FA	48 - 139	46 - 137
214	214	chain 'FF' and (resid 140 through 149 )	FF	FA	140 - 149	138 - 147
215	215	chain 'FF' and (resid 150 through 207 )	FF	FA	150 - 207	148 - 205
216	216	chain 'U' and (resid 301 through 301 )	U	MC	301
217	217	chain 'U' and (resid 302 through 302 )	U	NC	302
218	218	chain 'V' and (resid 301 through 301 )	V	PC	301
219	219	chain 'N' and (resid 301 through 301 )	N	NA	301
220	220	chain 'A' and (resid 301 through 301 )	A	JA	301
221	221	chain 'W' and (resid 301 through 301 )	W	TC	301
222	222	chain 'A' and (resid 302 through 302 )	A	KA	302
223	223	chain 'N' and (resid 302 through 302 )	N	OA	302
224	224	chain 'X' and (resid 301 through 301 )	X	XC	301
225	225	chain 'B' and (resid 301 through 301 )	B	QA	301
226	226	chain 'B' and (resid 302 through 302 )	B	RA	302
227	227	chain 'Y' and (resid 301 through 301)	Y	AD	301
228	228	chain 'B' and (resid 303 through 303)	B	SA	303
229	229	chain 'C' and (resid 301 through 301 )	C	TA	301
230	230	chain 'Y' and (resid 302 through 302 )	Y	BD	302
231	231	chain 'D' and (resid 301 through 301 )	D	VA	301
232	232	chain 'D' and (resid 302 through 302 )	D	WA	302
233	233	chain 'E' and (resid 301 through 301 )	E	YA	301
234	234	chain 'E' and (resid 302 through 302 )	E	ZA	302
235	235	chain 'F' and (resid 301 through 301 )	F	AB	301
236	236	chain 'F' and (resid 302 through 302 )	F	BB	302
237	237	chain 'DD' and (resid 301 through 301 )	DD	GD	301
238	238	chain 'G' and (resid 301 through 301 )	G	CB	301
239	239	chain 'G' and (resid 302 through 302 )	G	DB	302
240	240	chain 'CC' and (resid 301 through 301 )	CC	ED	301
241	241	chain 'H' and (resid 301 through 301 )	H	FB	301
242	242	chain 'H' and (resid 302 through 302 )	H	GB	302
243	243	chain 'H' and (resid 303 through 303 )	H	HB	303
244	244	chain 'I' and (resid 301 through 301 )	I	KB	301
245	245	chain 'FF' and (resid 301 through 301 )	FF - KD	KD	301
246	246	chain 'K' and (resid 301 through 301 )	K	PB	301
247	247	chain 'J' and (resid 301 through 301 )	J	LB	301
248	248	chain 'J' and (resid 302 through 302 )	J	MB	302
249	249	chain 'K' and (resid 302 through 302 )	K	QB	302
250	250	chain 'L' and (resid 301 through 301 )	L	RB	301
251	251	chain 'L' and (resid 302 through 302 )	L	SB	302
252	252	chain 'L' and (resid 303 through 303 )	L	TB	303
253	253	chain 'M' and (resid 301 through 301 )	M	VB	301
254	254	chain 'O' and (resid 301 through 301 )	O	WB	301
255	255	chain 'O' and (resid 302 through 302 )	O	XB	302
256	256	chain 'P' and (resid 301 through 301 )	P	YB	301
257	257	chain 'P' and (resid 302 through 302 )	P	ZB	302
258	258	chain 'Q' and (resid 301 through 301 )	Q	AC	301
259	259	chain 'Q' and (resid 302 through 302 )	Q	BC	302