Method to determine structure: MOLECULAR REPLACEMENT / Resolution: 3.5→93.61 Å / Cor.coef. Fo:Fc: 0.912 / Cor.coef. Fo:Fc free: 0.874 / SU B: 44.38 / SU ML: 0.629 / Cross valid method: THROUGHOUT / ESU R Free: 0.682 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.25727
692
4.9 %
RANDOM
Rwork
0.20762
-
-
-
obs
0.21008
13295
99.9 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK