ソフトウェア | 名称 | バージョン | 分類 |
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REFMAC | 5.8.0419精密化 | DIALS | | データ削減 | XSCALE | | データスケーリング | MOLREP | | 位相決定 | |
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精密化 | 構造決定の手法: 分子置換 / 解像度: 2→118.389 Å / Cor.coef. Fo:Fc: 0.965 / Cor.coef. Fo:Fc free: 0.951 / SU B: 6.433 / SU ML: 0.159 / 交差検証法: FREE R-VALUE / ESU R: 0.163 / ESU R Free: 0.148 / 詳細: Hydrogens have been added in their riding positions
| Rfactor | 反射数 | %反射 |
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Rfree | 0.2311 | 5611 | 4.971 % |
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Rwork | 0.198 | 107265 | - |
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all | 0.2 | - | - |
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obs | - | 112876 | 99.927 % |
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溶媒の処理 | イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK BULK SOLVENT |
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原子変位パラメータ | Biso mean: 59.081 Å2
| Baniso -1 | Baniso -2 | Baniso -3 |
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1- | 1.83 Å2 | 0 Å2 | 5.267 Å2 |
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2- | - | -2.876 Å2 | 0 Å2 |
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3- | - | - | -0.256 Å2 |
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精密化ステップ | サイクル: LAST / 解像度: 2→118.389 Å
| タンパク質 | 核酸 | リガンド | 溶媒 | 全体 |
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原子数 | 7146 | 2983 | 130 | 325 | 10584 |
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拘束条件 | Refine-ID | タイプ | Dev ideal | Dev ideal target | 数 |
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X-RAY DIFFRACTION | r_bond_refined_d0.006 | 0.011 | 10745 | X-RAY DIFFRACTION | r_bond_other_d0.003 | 0.016 | 8442 | X-RAY DIFFRACTION | r_angle_refined_deg1.615 | 1.724 | 15142 | X-RAY DIFFRACTION | r_angle_other_deg0.577 | 1.593 | 19627 | X-RAY DIFFRACTION | r_dihedral_angle_1_deg6.809 | 5 | 896 | X-RAY DIFFRACTION | r_dihedral_angle_2_deg7.091 | 5 | 55 | X-RAY DIFFRACTION | r_dihedral_angle_other_2_deg1.445 | 5 | 104 | X-RAY DIFFRACTION | r_dihedral_angle_3_deg14.901 | 10 | 1329 | X-RAY DIFFRACTION | r_dihedral_angle_6_deg16.061 | 10 | 353 | X-RAY DIFFRACTION | r_chiral_restr0.069 | 0.2 | 1775 | X-RAY DIFFRACTION | r_gen_planes_refined0.009 | 0.02 | 10308 | X-RAY DIFFRACTION | r_gen_planes_other0.002 | 0.02 | 2257 | X-RAY DIFFRACTION | r_nbd_refined0.175 | 0.2 | 1738 | X-RAY DIFFRACTION | r_symmetry_nbd_other0.154 | 0.2 | 7621 | X-RAY DIFFRACTION | r_nbtor_refined0.187 | 0.2 | 4723 | X-RAY DIFFRACTION | r_symmetry_nbtor_other0.071 | 0.2 | 4990 | X-RAY DIFFRACTION | r_xyhbond_nbd_refined0.142 | 0.2 | 494 | X-RAY DIFFRACTION | r_symmetry_xyhbond_nbd_other0.04 | 0.2 | 1 | X-RAY DIFFRACTION | r_symmetry_nbd_refined0.143 | 0.2 | 23 | X-RAY DIFFRACTION | r_nbd_other0.116 | 0.2 | 103 | X-RAY DIFFRACTION | r_symmetry_xyhbond_nbd_refined0.131 | 0.2 | 26 | X-RAY DIFFRACTION | r_mcbond_it4.487 | 5.705 | 3573 | X-RAY DIFFRACTION | r_mcbond_other4.487 | 5.705 | 3573 | X-RAY DIFFRACTION | r_mcangle_it6.158 | 10.261 | 4459 | X-RAY DIFFRACTION | r_mcangle_other6.159 | 10.262 | 4460 | X-RAY DIFFRACTION | r_scbond_it5.319 | 6.212 | 7172 | X-RAY DIFFRACTION | r_scbond_other5.267 | 6.197 | 7136 | X-RAY DIFFRACTION | r_scangle_it7.688 | 11.27 | 10678 | X-RAY DIFFRACTION | r_scangle_other7.636 | 11.246 | 10625 | X-RAY DIFFRACTION | r_lrange_it9.625 | 63.003 | 12520 | X-RAY DIFFRACTION | r_lrange_other9.456 | 62.608 | 12453 | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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LS精密化 シェル | Refine-ID: X-RAY DIFFRACTION / Total num. of bins used: 20 解像度 (Å) | Rfactor Rfree | Num. reflection Rfree | Rfactor Rwork | Num. reflection Rwork | Rfactor all | Num. reflection all | Fsc free | Fsc work | % reflection obs (%) | WRfactor Rwork |
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2-2.052 | 0.353 | 412 | 0.352 | 7848 | 0.352 | 8288 | 0.821 | 0.825 | 99.6622 | 0.334 | 2.052-2.108 | 0.33 | 404 | 0.328 | 7682 | 0.328 | 8098 | 0.904 | 0.893 | 99.8518 | 0.3 | 2.108-2.169 | 0.326 | 392 | 0.308 | 7519 | 0.309 | 7921 | 0.902 | 0.907 | 99.8737 | 0.274 | 2.169-2.236 | 0.271 | 379 | 0.281 | 7276 | 0.28 | 7667 | 0.933 | 0.925 | 99.8435 | 0.24 | 2.236-2.309 | 0.283 | 370 | 0.261 | 7083 | 0.262 | 7459 | 0.933 | 0.936 | 99.9196 | 0.218 | 2.309-2.39 | 0.244 | 357 | 0.242 | 6789 | 0.242 | 7151 | 0.944 | 0.948 | 99.9301 | 0.196 | 2.39-2.481 | 0.285 | 350 | 0.243 | 6596 | 0.245 | 6950 | 0.942 | 0.954 | 99.9424 | 0.198 | 2.481-2.582 | 0.237 | 330 | 0.221 | 6382 | 0.222 | 6712 | 0.957 | 0.964 | 100 | 0.181 | 2.582-2.697 | 0.261 | 333 | 0.214 | 6037 | 0.217 | 6370 | 0.951 | 0.97 | 100 | 0.177 | 2.697-2.828 | 0.265 | 307 | 0.202 | 5849 | 0.205 | 6156 | 0.958 | 0.975 | 100 | 0.17 | 2.828-2.981 | 0.255 | 298 | 0.201 | 5505 | 0.204 | 5803 | 0.957 | 0.975 | 100 | 0.172 | 2.981-3.162 | 0.228 | 257 | 0.182 | 5275 | 0.184 | 5534 | 0.967 | 0.979 | 99.9639 | 0.163 | 3.162-3.38 | 0.225 | 282 | 0.185 | 4934 | 0.187 | 5217 | 0.97 | 0.981 | 99.9808 | 0.175 | 3.38-3.65 | 0.223 | 216 | 0.188 | 4600 | 0.189 | 4816 | 0.968 | 0.98 | 100 | 0.181 | 3.65-3.998 | 0.196 | 210 | 0.169 | 4253 | 0.171 | 4463 | 0.974 | 0.984 | 100 | 0.169 | 3.998-4.47 | 0.183 | 211 | 0.15 | 3819 | 0.151 | 4030 | 0.98 | 0.987 | 100 | 0.156 | 4.47-5.16 | 0.189 | 173 | 0.158 | 3446 | 0.16 | 3619 | 0.981 | 0.987 | 100 | 0.172 | 5.16-6.317 | 0.234 | 156 | 0.191 | 2851 | 0.193 | 3007 | 0.973 | 0.984 | 100 | 0.206 | 6.317-8.92 | 0.228 | 114 | 0.174 | 2241 | 0.177 | 2355 | 0.975 | 0.984 | 100 | 0.199 | 8.92-118.389 | 0.19 | 60 | 0.192 | 1280 | 0.192 | 1343 | 0.984 | 0.97 | 99.7766 | 0.236 |
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