分子量: 30292.252 Da / 分子数: 1 / 由来タイプ: 組換発現 詳細: We have reported the complete sequence but the discrepancies are due to the fact that the N-Terminal portion /1-45 residues) and the loop (residues 236 to 242) are highly mobile and therefore ...詳細: We have reported the complete sequence but the discrepancies are due to the fact that the N-Terminal portion /1-45 residues) and the loop (residues 236 to 242) are highly mobile and therefore we were not able to reconstruct these segments. 由来: (組換発現) Homo sapiens (ヒト) / 遺伝子: PNPO / 発現宿主: Escherichia coli (大腸菌) / 参照: UniProt: Q9NVS9, pyridoxal 5'-phosphate synthase
構造決定の手法: 分子置換 / 解像度: 2.746→41.47 Å / Cor.coef. Fo:Fc: 0.959 / Cor.coef. Fo:Fc free: 0.938 / SU B: 15.464 / SU ML: 0.294 / 交差検証法: THROUGHOUT / ESU R Free: 0.358 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN USED IF PRESENT IN THE INPUT
Rfactor
反射数
%反射
Selection details
Rfree
0.23894
343
5.3 %
RANDOM
Rwork
0.19836
-
-
-
obs
0.20054
6175
99.68 %
-
溶媒の処理
イオンプローブ半径: 0.9 Å / 減衰半径: 0.9 Å / VDWプローブ半径: 1.1 Å / 溶媒モデル: MASK