Mass: 18.015 Da / Num. of mol.: 95 / Source method: isolated from a natural source / Formula: H2O
Has ligand of interest
N
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 1.92 Å3/Da / Density % sol: 35.97 %
Crystal grow
Temperature: 293 K / Method: vapor diffusion, sitting drop Details: 0.1 M MES pH 6.0, 20 mM NaCl, and 20-24% (w/v) PEG 6000, soaked in 0.25 M neutralised galacturonic acid.
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Data collection
Diffraction
Mean temperature: 100 K / Serial crystal experiment: N
Diffraction source
Source: SYNCHROTRON / Site: MAX IV / Beamline: BioMAX / Wavelength: 0.9762 Å
Detector
Type: DECTRIS EIGER X 16M / Detector: PIXEL / Date: Dec 17, 2022
Radiation
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.9762 Å / Relative weight: 1
Reflection
Resolution: 2.16→85.43 Å / Num. obs: 28249 / % possible obs: 93 % / Redundancy: 6.8 % / CC1/2: 0.986 / Net I/σ(I): 6.7