Method to determine structure: MOLECULAR REPLACEMENT / Resolution: 2.76→47.21 Å / Cor.coef. Fo:Fc: 0.879 / Cor.coef. Fo:Fc free: 0.859 / SU B: 17.632 / SU ML: 0.337 / Cross valid method: THROUGHOUT / ESU R Free: 0.381 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.26609
2666
5 %
RANDOM
Rwork
0.24755
-
-
-
obs
0.24849
50269
99.6 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK