Software Name Version Classification XDSdata scaling PHENIX1.20_4459refinement PDB_EXTRACT3.27 data extraction XDSdata reduction PHASERphasing
Refinement Method to determine structure : MOLECULAR REPLACEMENTStarting model : 5ggsResolution : 1.98→29.61 Å / SU ML : 0.23 / Cross valid method : THROUGHOUT / σ(F) : 1.99 / Phase error : 25.39 / Stereochemistry target values : MLRfactor Num. reflection % reflection Rfree 0.2355 3418 5 % Rwork 0.187 64968 - obs 0.1894 68386 94.71 %
Solvent computation Shrinkage radii : 0.9 Å / VDW probe radii : 1.1 Å / Solvent model : FLAT BULK SOLVENT MODELDisplacement parameters Biso max : 101.08 Å2 / Biso mean : 38.297 Å2 / Biso min : 20.47 Å2 Refinement step Cycle : final / Resolution : 1.98→29.61 ÅProtein Nucleic acid Ligand Solvent Total Num. atoms 8210 0 0 644 8854 Biso mean - - - 41.61 - Num. residues - - - - 1074
LS refinement shell Refine-ID : X-RAY DIFFRACTION / Rfactor Rfree error : 0 / Total num. of bins used : 24
Show large table (7 x 24) Hide large table Resolution (Å)Rfactor Rfree Num. reflection Rfree Rfactor Rwork Num. reflection Rwork Num. reflection all % reflection obs (%)1.98-2.01 0.3109 143 0.2768 2713 2856 95 2.01-2.04 0.3443 142 0.2742 2712 2854 94 2.04-2.07 0.2831 142 0.2649 2682 2824 96 2.07-2.1 0.2846 145 0.2466 2765 2910 95 2.1-2.14 0.3109 144 0.2304 2738 2882 95 2.14-2.18 0.2794 144 0.2431 2727 2871 95 2.18-2.22 0.3161 141 0.2289 2675 2816 94 2.22-2.27 0.2797 145 0.2273 2762 2907 96 2.27-2.32 0.3096 143 0.2271 2706 2849 94 2.32-2.37 0.2702 141 0.2075 2687 2828 95 2.37-2.43 0.2291 142 0.216 2690 2832 95 2.43-2.49 0.2736 143 0.2061 2717 2860 94 2.49-2.57 0.248 138 0.2017 2631 2769 94 2.57-2.65 0.2504 140 0.2054 2655 2795 91 2.65-2.75 0.2575 138 0.2017 2619 2757 91 2.75-2.86 0.2182 144 0.1871 2742 2886 97 2.86-2.98 0.2326 145 0.2003 2738 2883 96 2.98-3.14 0.2615 144 0.1924 2753 2897 96 3.14-3.34 0.2178 144 0.1826 2728 2872 96 3.34-3.6 0.2387 144 0.1699 2734 2878 95 3.6-3.96 0.2144 144 0.167 2731 2875 95 3.96-4.53 0.1882 142 0.1405 2694 2836 94 4.53-5.7 0.1869 136 0.1448 2591 2727 91 5.7-29.61 0.1986 144 0.1742 2778 2922 97
Refinement TLS params. Method : refined / Refine-ID : X-RAY DIFFRACTION
Show large table (25 x 33) Hide large table ID L11 (°2 )L12 (°2 )L13 (°2 )L22 (°2 )L23 (°2 )L33 (°2 )S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T11 (Å2 )T12 (Å2 )T13 (Å2 )T22 (Å2 )T23 (Å2 )T33 (Å2 )Origin x (Å)Origin y (Å)Origin z (Å)1 5.1672 0.2106 -1.0917 0.6808 -0.3009 2.2667 -0.0346 -0.6695 0.0968 0.2106 -0.0282 -0.045 -0.0367 0.1564 0.0582 0.2452 0.0308 -0.046 0.254 -0.0205 0.2151 44.5055 5.5193 63.5792 2 4.4539 -0.636 -0.7582 5.0502 -1.2469 3.2337 -0.0337 0.1377 0.2254 -0.1335 0.0745 -0.0284 -0.107 0.1206 -0.0541 0.172 0.0011 -0.0398 0.2016 -0.0195 0.2421 60.1608 19.2712 36.846 3 1.4353 1.5377 -2.0506 3.3352 -1.4313 3.4088 0.0302 0.2508 -0.3099 -0.263 -0.1674 -0.0985 0.4494 0.2573 0.168 0.2658 0.049 -0.062 0.3166 -0.0879 0.277 28.2426 6.3087 42.4134 4 3.0327 -0.1105 -0.5735 3.0205 -1.6065 3.9138 -0.082 0.0847 -0.0351 -0.0273 0.0662 0.0547 0.0015 -0.1279 -0.0677 0.1875 0.046 -0.0189 0.1957 -0.0323 0.2285 25.0289 8.6558 51.8277 5 2.6101 0.2035 -0.8097 2.7867 -1.4641 4.1302 0.0292 0.0808 0.0366 0.1138 -0.0048 -0.1045 -0.0768 0.0633 0.0615 0.1687 0.0355 -0.0348 0.1706 -0.0477 0.2606 29.7977 8.5094 50.1158 6 1.4641 1.2517 -1.5193 1.9019 -2.9856 6.6918 -0.1306 0.1205 -0.115 0.5008 0.1799 0.167 0.1064 0 -0.0676 0.3012 0.099 0.0077 0.2552 -0.0208 0.2923 34.421 16.019 31.413 7 8.519 -2.7817 0.7994 4.6084 0.7094 5.2112 -0.4757 0.6968 0.4907 0.3489 0.3292 -0.5322 -0.2325 0.9988 0.1321 0.3272 0.0147 0.0122 0.4787 0.0566 0.3379 64.5253 12.2324 27.5091 8 6.6895 -1.7553 -0.376 2.0984 0.4167 3.1498 0.1718 0.6134 -0.2021 -0.1787 -0.4025 0.1646 0.0229 0.0281 0.1773 0.2077 -0.0035 -0.0646 0.2449 -0.0054 0.2033 48.8765 9.4836 28.9515 9 5.4587 -1.3782 0.0775 2.2731 0.4026 3.3653 0.2011 1.0668 -0.2889 -0.1638 -0.2834 -0.1231 0.2371 0.3326 0.0899 0.2858 0.0627 -0.0109 0.4438 -0.0376 0.2869 56.9917 5.9753 21.7288 10 5.7584 0.5074 -0.664 1.1885 0.4092 5.8669 -0.3092 -0.0458 -0.4715 -0.0682 0.0618 -0.3324 0.3601 -0.0301 0.3068 0.2788 0.0045 0.0048 0.2748 0.0395 0.233 10.6022 7.4661 82.4874 11 5.5558 -1.2125 -1.0498 0.29 -0.0283 2.676 -0.3658 -0.2341 -1.8257 0.0091 -0.0761 -0.2317 1.3347 1.0999 0.4809 0.7907 0.2419 0.1094 0.7542 0.1252 0.5891 26.0129 -2.0711 77.3843 12 9.1999 -0.9422 -1.1847 2.5139 0.353 6.5713 -0.1084 0.6956 -0.3416 -0.3272 -0.0335 0.304 0.0764 0.0826 0.2837 0.4332 -0.0204 -0.0113 0.3659 -0.0204 0.2656 15.7166 8.8296 73.1509 13 5.3212 -0.7597 5.1137 2.2419 -0.0286 5.6733 -0.3561 1.6618 0.0906 -0.3121 -0.0472 0.1765 -0.3772 0.5202 0.4098 0.3451 -0.0987 0.0354 0.5124 0.0327 0.3115 11.2757 12.3067 69.449 14 8.0234 -3.608 -3.211 5.4302 0.4285 5.6515 -0.1013 -0.4226 0.1016 -0.1135 0.2465 -0.6899 -0.6735 0.751 -0.2316 0.3584 0.05 -0.0495 0.4708 -0.0105 0.3477 20.536 15.0939 79.7909 15 2.7313 -4.0368 -1.5563 6.425 1.8662 5.9397 0.0033 -0.1066 0.4372 -0.3713 0.2283 -0.2693 -0.2474 -0.1583 -0.1794 0.2472 0.0049 0.0036 0.3092 0.0566 0.3839 14.1605 13.0709 83.024 16 9.8994 -5.9143 -6.2894 3.7881 4.4513 5.7602 -0.2805 -0.1876 -0.5273 0.1423 -0.0174 0.3902 0.4037 -0.0709 0.2584 0.3278 -0.0194 0.037 0.3016 0.0184 0.2485 17.9814 2.9563 71.154 17 4.4825 -3.2584 -6.2041 5.6695 3.6226 9.3794 -0.2516 1.1957 -1.2695 -0.6494 -0.3915 0.4441 0.3098 -0.4799 0.5755 0.3812 -0.0831 0.0307 0.364 -0.0938 0.4432 12.673 0.3184 71.313 18 8.8685 -2.8985 -3.3919 9.3121 3.7272 5.6667 -0.0542 -0.1536 0.7389 0.0992 -0.1169 0.7351 -0.4752 -0.7406 0.0996 0.3692 0.133 -0.0334 0.5508 0.0117 0.3778 1.0341 17.2867 83.9491 19 4.1029 0.2067 -0.6769 0.5257 -0.0484 2.0258 0.06 -0.4751 0.3566 0.1831 0.0256 -0.052 -0.1255 0.1481 -0.0805 0.2534 0.0316 -0.0517 0.2225 -0.0834 0.289 19.3264 -26.1878 63.6009 20 2.1348 -0.31 0.4041 3.5668 -1.3195 4.369 0.0069 -0.3336 0.5716 0.0383 0.076 0.0044 -0.2871 0.1343 -0.0712 0.2189 -0.0213 -0.0227 0.3263 -0.0877 0.4236 35.5783 -13.3707 35.0317 21 2.7318 -0.1555 -0.7397 2.073 -0.8571 3.8697 -0.0783 0.2329 0.0335 -0.2384 0.0442 -0.0069 0.1568 -0.3078 0.0312 0.1893 0.036 -0.0406 0.2257 -0.0547 0.2859 1.413 -25.6823 47.5168 22 2.5282 -0.7209 -0.3025 2.5617 -0.8825 3.5766 -0.0766 0.1488 0.377 0.0492 0.0354 0.0691 -0.2876 -0.1206 -0.0286 0.2111 0.0552 -0.0276 0.2399 -0.0456 0.3597 0.0136 -18.4577 52.5901 23 2.6073 -0.067 -0.6713 1.8509 -0.8812 3.9102 0.0551 0.1001 0.3702 -0.0739 -0.029 -0.0668 -0.1658 0.0336 0.083 0.178 0.0295 -0.027 0.2087 -0.0306 0.3274 4.9181 -22.0864 50.2302 24 3.3505 1.6605 -3.0284 0.9946 -1.6091 2.7627 0.1851 0.3857 0.7199 0.0466 0.328 0.4416 -0.7136 -0.4553 -0.5076 0.3226 0.0511 0.0058 0.3438 0.0716 0.3068 9.7567 -14.2538 30.8037 25 2.6005 -3.4573 2.1962 7.5007 0.5941 7.6726 -0.2282 0.256 0.4463 0.5769 0.4448 -1.1006 -0.1041 1.1305 -0.0891 0.3287 -0.0313 -0.0531 0.3972 0.0268 0.3699 38.9388 -21.5699 25.986 26 7.466 -4.3625 -2.2578 6.1495 2.1233 1.4039 0.0367 0.1785 0.1014 0.0134 -0.1978 0.1821 0.018 -0.077 0.1869 0.2695 -0.0097 -0.0266 0.3219 0.0566 0.2035 23.6509 -23.4671 26.7362 27 1.1637 -0.8509 -1.2989 7.9359 6.4731 5.6839 0.222 0.0226 -0.1951 -0.4203 -0.4458 0.2775 -0.1137 -0.5492 0.2676 0.3686 0.0009 -0.0769 0.3704 0.0108 0.3018 28.1133 -31.8484 26.9093 28 3.6335 -3.5582 -1.2956 3.499 0.9888 6.5727 -0.2534 -0.4959 0.9425 0.5851 0.0978 0.2107 -1.196 0.2073 0.1522 0.3625 0.014 -0.0265 0.2803 -0.0314 0.4099 16.8104 -11.7681 34.1554 29 7.9058 -3.5828 -1.6492 3.9033 1.1014 3.6977 0.2291 0.6603 -0.2685 -0.1568 -0.2245 -0.0089 0.1714 0.0976 -0.0582 0.2499 -0.0479 -0.0329 0.2653 0.0102 0.2554 30.5124 -27.3233 21.1757 30 6.2872 -1.0021 -1.2773 2.9072 1.565 4.4436 -0.2415 0.1699 -0.271 0.0159 0.0461 0.117 0.1285 -0.1027 0.177 0.2438 -0.0007 -0.0054 0.2534 0.0141 0.2183 -10.941 -24.1001 77.3855 31 8.2678 4.0436 -2.633 2.1298 -2.3907 8.922 0.2629 0.1127 0.8106 0.194 -0.354 -0.1319 -1.6073 1.4377 0.1335 0.9353 0.0788 -0.143 0.8426 0.0485 0.8967 -1.8647 -9.9054 75.0237 32 4.2814 -0.0576 -2.2046 2.0735 2.4383 5.7773 -0.2158 -0.3619 0.4433 0.1874 0.112 -0.2715 0.0405 0.0592 0.0864 0.2708 0.0511 -0.039 0.3468 -0.0081 0.2766 -10.3319 -19.1422 80.828 33 5.3848 -3.4339 -5.1525 4.4256 4.2533 6.5712 -0.2417 0.8494 -0.3596 0.2043 -0.4698 0.6358 0.0981 -1.1707 0.6813 0.2909 -0.0076 -0.0488 0.3674 -0.0405 0.2932 -14.6565 -24.786 75.8908
Refinement TLS group Show large table (6 x 33) Hide large table ID Refine-ID Refine TLS-ID Selection details Auth asym-ID Auth seq-ID 1 X-RAY DIFFRACTION 1 chain 'A' and (resid 1 through 123 )A1 - 123 2 X-RAY DIFFRACTION 2 chain 'A' and (resid 124 through 218 )A124 - 218 3 X-RAY DIFFRACTION 3 chain 'B' and (resid 1 through 18 )B1 - 18 4 X-RAY DIFFRACTION 4 chain 'B' and (resid 19 through 75 )B19 - 75 5 X-RAY DIFFRACTION 5 chain 'B' and (resid 76 through 101 )B76 - 101 6 X-RAY DIFFRACTION 6 chain 'B' and (resid 102 through 113 )B102 - 113 7 X-RAY DIFFRACTION 7 chain 'B' and (resid 114 through 128 )B114 - 128 8 X-RAY DIFFRACTION 8 chain 'B' and (resid 129 through 174 )B129 - 174 9 X-RAY DIFFRACTION 9 chain 'B' and (resid 175 through 212 )B175 - 212 10 X-RAY DIFFRACTION 10 chain 'Q' and (resid 31 through 55 )Q31 - 55 11 X-RAY DIFFRACTION 11 chain 'Q' and (resid 56 through 62 )Q56 - 62 12 X-RAY DIFFRACTION 12 chain 'Q' and (resid 63 through 70 )Q63 - 70 13 X-RAY DIFFRACTION 13 chain 'Q' and (resid 71 through 82 )Q