温度: 291.15 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 4.6 詳細: DzFer crystals were grown in 0.2 M ammonium sulfate, 0.1 M sodium acetate trihydrate pH 4.6, 30% w/v PEG monomethyl ether 2000, followed by soaking for 10 min with 20% glycerol and 100 mM AgNO3.
構造決定の手法: 分子置換 / 解像度: 1.9→104.8 Å / Cor.coef. Fo:Fc: 0.976 / Cor.coef. Fo:Fc free: 0.964 / SU B: 2.349 / SU ML: 0.068 / 交差検証法: THROUGHOUT / ESU R: 0.096 / ESU R Free: 0.101 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.18965
1107
5 %
RANDOM
Rwork
0.1508
-
-
-
obs
0.15273
21003
99.95 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK