The authors conducted crystallization experiments under aerobic conditions, and they were unable to ...The authors conducted crystallization experiments under aerobic conditions, and they were unable to confirm the valence state of FE in the structure.
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 3.78 Å3/Da / 溶媒含有率: 67.5 %
結晶化
温度: 293 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 7.5 詳細: 0.085 M HEPES sodium pH 7.5, 1.7% v/v Polyethylene glycol 400, 1.7 M Ammonium sulfate, 15% v/v Glycerol