構造決定の手法: 分子置換 開始モデル: inhouse model 解像度: 1.44→44.11 Å / Cor.coef. Fo:Fc: 0.97 / Cor.coef. Fo:Fc free: 0.96 / SU B: 2.001 / SU ML: 0.071 / 交差検証法: THROUGHOUT / σ(F): 0 / ESU R: 0.079 / ESU R Free: 0.079 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: 30 vol-% glycerol (3.26M) soaked into crystal, two molecules bind at surface but none at ligand binding site. test performed upon request based on hypothesis that glycerol in protein ...詳細: 30 vol-% glycerol (3.26M) soaked into crystal, two molecules bind at surface but none at ligand binding site. test performed upon request based on hypothesis that glycerol in protein preparation might influence binding and/or in vivo results. No binding of glycerol at ligand binding site.
Rfactor
反射数
%反射
Selection details
Rfree
0.226
1284
5.2 %
RANDOM
Rwork
0.1994
-
-
-
obs
0.2008
23574
92.6 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK