+Open data
-Basic information
Entry | Database: PDB / ID: 7.0E+85 | ||||||
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Title | SnoaL-like domain-containing protein | ||||||
Components | SnoaL-like domain-containing protein | ||||||
Keywords | UNKNOWN FUNCTION / SnoaL-like domain-containing protein / hypothetical protein | ||||||
Function / homology | SnoaL-like domain / SnoaL-like domain / NTF2-like domain superfamily / SnoaL-like domain-containing protein Function and homology information | ||||||
Biological species | Mycobacterium tuberculosis (bacteria) | ||||||
Method | X-RAY DIFFRACTION / SYNCHROTRON / SAD / Resolution: 2.424 Å | ||||||
Authors | Zhuang, J. | ||||||
Citation | Journal: To Be Published Title: SnoaL-like domain-containing protein Authors: Zhuang, J. | ||||||
History |
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-Structure visualization
Structure viewer | Molecule: MolmilJmol/JSmol |
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-Downloads & links
-Download
PDBx/mmCIF format | 7e85.cif.gz | 82.1 KB | Display | PDBx/mmCIF format |
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PDB format | pdb7e85.ent.gz | 62.2 KB | Display | PDB format |
PDBx/mmJSON format | 7e85.json.gz | Tree view | PDBx/mmJSON format | |
Others | Other downloads |
-Validation report
Summary document | 7e85_validation.pdf.gz | 443.3 KB | Display | wwPDB validaton report |
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Full document | 7e85_full_validation.pdf.gz | 449.1 KB | Display | |
Data in XML | 7e85_validation.xml.gz | 16.6 KB | Display | |
Data in CIF | 7e85_validation.cif.gz | 23.3 KB | Display | |
Arichive directory | https://data.pdbj.org/pub/pdb/validation_reports/e8/7e85 ftp://data.pdbj.org/pub/pdb/validation_reports/e8/7e85 | HTTPS FTP |
-Related structure data
Similar structure data |
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-Links
-Assembly
Deposited unit |
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2 |
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Unit cell |
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-Components
#1: Protein | Mass: 13180.716 Da / Num. of mol.: 3 Source method: isolated from a genetically manipulated source Source: (gene. exp.) Mycobacterium tuberculosis (strain ATCC 25618 / H37Rv) (bacteria) Gene: Rv3768 / Production host: Escherichia coli (E. coli) / References: UniProt: P72035 #2: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: X-RAY DIFFRACTION / Number of used crystals: 1 |
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-Sample preparation
Crystal | Density Matthews: 3.4 Å3/Da / Density % sol: 63.84 % |
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Crystal grow | Temperature: 295.15 K / Method: vapor diffusion, hanging drop Details: 0.1M Sodium acetate hydrate (pH 5.2), 2.4M Ammonium sulfate |
-Data collection
Diffraction | Mean temperature: 100 K / Serial crystal experiment: N |
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Diffraction source | Source: SYNCHROTRON / Site: SSRF / Beamline: BL19U1 / Wavelength: 0.97852 Å |
Detector | Type: DECTRIS PILATUS3 6M / Detector: PIXEL / Date: Jun 1, 2019 |
Radiation | Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength: 0.97852 Å / Relative weight: 1 |
Reflection | Resolution: 2.42→28.99 Å / Num. obs: 21425 / % possible obs: 99.5 % / Redundancy: 1 % / CC1/2: 0.939 / Net I/σ(I): 16.9 |
Reflection shell | Resolution: 2.42→2.52 Å / Num. unique obs: 2215 / CC1/2: 0.939 |
-Processing
Software |
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Refinement | Method to determine structure: SAD / Resolution: 2.424→28.986 Å / SU ML: 0.29 / Cross valid method: THROUGHOUT / σ(F): 1.34 / Phase error: 23.98 / Stereochemistry target values: ML
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Solvent computation | Shrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å / Solvent model: FLAT BULK SOLVENT MODEL | ||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | Biso max: 138.42 Å2 / Biso mean: 53.676 Å2 / Biso min: 24 Å2 | ||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refinement step | Cycle: final / Resolution: 2.424→28.986 Å
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LS refinement shell | Refine-ID: X-RAY DIFFRACTION / Rfactor Rfree error: 0
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