温度: 293 K / 手法: 蒸気拡散法, ハンギングドロップ法 / pH: 4.75 詳細: Crystals were grown using the vapor diffusion hanging drop method with a protein concentration of 10 mg/ml. The reservoir solution consisted of 1.6 M ammonium sulfate and 0.1 M sodium acetate (pH 4.75).
解像度: 1.15→38.95 Å / Cor.coef. Fo:Fc: 0.985 / Cor.coef. Fo:Fc free: 0.972 / 交差検証法: THROUGHOUT / σ(F): 0 / ESU R: 0.031 / ESU R Free: 0.035 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS U VALUES : REFINED INDIVIDUALLY
Rfactor
反射数
%反射
Selection details
Rfree
0.1591
5067
5 %
RANDOM
Rwork
0.1182
-
-
-
obs
0.1202
96370
99.31 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK