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- PDB-5lox: Helical Assembly of the Anbu Complex from Pseudomonas aeruginosa -

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Open data

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Basic information

Entry

Database: PDB / ID: 5lox

Title

Helical Assembly of the Anbu Complex from Pseudomonas aeruginosa

Components

Peptidase

Keywords

HYDROLASE / Protein Degradation / Ancestral Beta Subunit / Proteasome Precursor

Function / homology

Uncharacterised conserved protein UCP009120, proteasome-type protease, Sll0069 / proteasome core complex / Proteasome subunit / Proteasome, subunit alpha/beta / Nucleophile aminohydrolases, N-terminal / proteolysis involved in protein catabolic process / Peptidase

Function and homology information

Biological species

Pseudomonas aeruginosa (bacteria)

Method

X-RAY DIFFRACTION /

SYNCHROTRON /

SAD / Resolution: 2.9 Å

Authors

Fuchs, A.C.D. / Albrecht, R. / Martin, J. / Hartmann, M.D.

Citation

Journal: Structure / Year: 2017
Title: The Architecture of the Anbu Complex Reflects an Evolutionary Intermediate at the Origin of the Proteasome System.
Authors: Fuchs, A.C.D. / Alva, V. / Maldoner, L. / Albrecht, R. / Hartmann, M.D. / Martin, J.

History

Deposition	Aug 10, 2016	Deposition site: PDBE / Processing site: PDBE
Revision 1.0	Jun 7, 2017	Provider: repository / Type: Initial release
Revision 1.1	Jun 14, 2017	Group: Database references / Category: citation Item: _citation.country / _citation.journal_id_ASTM ..._citation.country / _citation.journal_id_ASTM / _citation.journal_id_CSD / _citation.journal_volume / _citation.page_first / _citation.page_last

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Structure visualization

Structure viewer	Molecule: MolmilJmol/JSmol

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Downloads & links

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Download

PDBx/mmCIF format	5lox.cif.gz	3 MB	Display	PDBx/mmCIF format
PDB format	pdb5lox.ent.gz	2.6 MB	Display	PDB format
PDBx/mmJSON format	5lox.json.gz		Tree view	PDBx/mmJSON format
Others	Other downloads

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Validation report

Summary document	5lox_validation.pdf.gz	679.1 KB	Display	wwPDB validaton report
Full document	5lox_full_validation.pdf.gz	775.7 KB	Display
Data in XML	5lox_validation.xml.gz	256.2 KB	Display
Data in CIF	5lox_validation.cif.gz	342.7 KB	Display
Arichive directory	https://data.pdbj.org/pub/pdb/validation_reports/lo/5lox ftp://data.pdbj.org/pub/pdb/validation_reports/lo/5lox	HTTPS FTP

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Related structure data

Related structure data	5loyC C: citing same article (ref.)
Similar structure data	4pj1-d 5opx-d 8298 4pkn-d 10621 1546 Search similar-shape structures by Omokage search (details) Similarity search - Function & homologyF&H Search Similarity search - FunctionF&H Search Similarity search - HomologyF&H Search

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Links

PDB pages	PDBj / wwPDB / NCBI
Related items in Molecule of the Month	#166 - Oct 2013 Proteasome similarity (3) #80 - Aug 2006 AAA+ Proteases similarity (3) #176 - Aug 2014 Dynein similarity (3) #60 - Dec 2004 Ubiquitin similarity (3)

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Assembly

Deposited unit

A: Peptidase

B: Peptidase

C: Peptidase

D: Peptidase

E: Peptidase

F: Peptidase

G: Peptidase

H: Peptidase

I: Peptidase

J: Peptidase

K: Peptidase

L: Peptidase

M: Peptidase

N: Peptidase

O: Peptidase

P: Peptidase

Q: Peptidase

R: Peptidase

S: Peptidase

T: Peptidase

U: Peptidase

V: Peptidase

W: Peptidase

X: Peptidase

Y: Peptidase

Z: Peptidase

1: Peptidase

2: Peptidase

3: Peptidase

4: Peptidase

5: Peptidase

6: Peptidase

7: Peptidase

8: Peptidase

906 kDa, 34 polymers
Search similar-shape structures of this assembly by Omokage search (details)

Idetical with deposited unit
defined by author&software

Unit cell

Length a, b, c (Å)	150.070, 230.080, 171.720
Angle α, β, γ (deg.)	90.00, 108.39, 90.00
Int Tables number	4
Space group name H-M	P12₁1

Noncrystallographic symmetry (NCS)

NCS domain:

ID	Ens-ID	Details
1	1	A
2	1	B
1	2	A
2	2	C
1	3	A
2	3	D
1	4	A
2	4	E
1	5	A
2	5	F
1	6	A
2	6	G
1	7	A
2	7	H
1	8	A
2	8	I
1	9	A
2	9	J
1	10	A
2	10	K
1	11	A
2	11	L
1	12	A
2	12	M
1	13	A
2	13	N
1	14	A
2	14	O
1	15	A
2	15	P
1	16	A
2	16	Q
1	17	A
2	17	R
1	18	A
2	18	S
1	19	A
2	19	T
1	20	A
2	20	U
1	21	A
2	21	V
1	22	A
2	22	W
1	23	A
2	23	X
1	24	A
2	24	Y
1	25	A
2	25	Z
1	26	A
2	26	1
1	27	A
2	27	2
1	28	A
2	28	3
1	29	A
2	29	4
1	30	A
2	30	5
1	31	A
2	31	6
1	32	A
2	32	7
1	33	A
2	33	8
1	34	B
2	34	C
1	35	B
2	35	D
1	36	B
2	36	E
1	37	B
2	37	F
1	38	B
2	38	G
1	39	B
2	39	H
1	40	B
2	40	I
1	41	B
2	41	J
1	42	B
2	42	K
1	43	B
2	43	L
1	44	B
2	44	M
1	45	B
2	45	N
1	46	B
2	46	O
1	47	B
2	47	P
1	48	B
2	48	Q
1	49	B
2	49	R
1	50	B
2	50	S
1	51	B
2	51	T
1	52	B
2	52	U
1	53	B
2	53	V
1	54	B
2	54	W
1	55	B
2	55	X
1	56	B
2	56	Y
1	57	B
2	57	Z
1	58	B
2	58	1
1	59	B
2	59	2
1	60	B
2	60	3
1	61	B
2	61	4
1	62	B
2	62	5
1	63	B
2	63	6
1	64	B
2	64	7
1	65	B
2	65	8
1	66	C
2	66	D
1	67	C
2	67	E
1	68	C
2	68	F
1	69	C
2	69	G
1	70	C
2	70	H
1	71	C
2	71	I
1	72	C
2	72	J
1	73	C
2	73	K
1	74	C
2	74	L
1	75	C
2	75	M
1	76	C
2	76	N
1	77	C
2	77	O
1	78	C
2	78	P
1	79	C
2	79	Q
1	80	C
2	80	R
1	81	C
2	81	S
1	82	C
2	82	T
1	83	C
2	83	U
1	84	C
2	84	V
1	85	C
2	85	W
1	86	C
2	86	X
1	87	C
2	87	Y
1	88	C
2	88	Z
1	89	C
2	89	1
1	90	C
2	90	2
1	91	C
2	91	3
1	92	C
2	92	4
1	93	C
2	93	5
1	94	C
2	94	6
1	95	C
2	95	7
1	96	C
2	96	8
1	97	D
2	97	E
1	98	D
2	98	F
1	99	D
2	99	G
1	100	D
2	100	H
1	101	D
2	101	I
1	102	D
2	102	J
1	103	D
2	103	K
1	104	D
2	104	L
1	105	D
2	105	M
1	106	D
2	106	N
1	107	D
2	107	O
1	108	D
2	108	P
1	109	D
2	109	Q
1	110	D
2	110	R
1	111	D
2	111	S
1	112	D
2	112	T
1	113	D
2	113	U
1	114	D
2	114	V
1	115	D
2	115	W
1	116	D
2	116	X
1	117	D
2	117	Y
1	118	D
2	118	Z
1	119	D
2	119	1
1	120	D
2	120	2
1	121	D
2	121	3
1	122	D
2	122	4
1	123	D
2	123	5
1	124	D
2	124	6
1	125	D
2	125	7
1	126	D
2	126	8
1	127	E
2	127	F
1	128	E
2	128	G
1	129	E
2	129	H
1	130	E
2	130	I
1	131	E
2	131	J
1	132	E
2	132	K
1	133	E
2	133	L
1	134	E
2	134	M
1	135	E
2	135	N
1	136	E
2	136	O
1	137	E
2	137	P
1	138	E
2	138	Q
1	139	E
2	139	R
1	140	E
2	140	S
1	141	E
2	141	T
1	142	E
2	142	U
1	143	E
2	143	V
1	144	E
2	144	W
1	145	E
2	145	X
1	146	E
2	146	Y
1	147	E
2	147	Z
1	148	E
2	148	1
1	149	E
2	149	2
1	150	E
2	150	3
1	151	E
2	151	4
1	152	E
2	152	5
1	153	E
2	153	6
1	154	E
2	154	7
1	155	E
2	155	8
1	156	F
2	156	G
1	157	F
2	157	H
1	158	F
2	158	I
1	159	F
2	159	J
1	160	F
2	160	K
1	161	F
2	161	L
1	162	F
2	162	M
1	163	F
2	163	N
1	164	F
2	164	O
1	165	F
2	165	P
1	166	F
2	166	Q
1	167	F
2	167	R
1	168	F
2	168	S
1	169	F
2	169	T
1	170	F
2	170	U
1	171	F
2	171	V
1	172	F
2	172	W
1	173	F
2	173	X
1	174	F
2	174	Y
1	175	F
2	175	Z
1	176	F
2	176	1
1	177	F
2	177	2
1	178	F
2	178	3
1	179	F
2	179	4
1	180	F
2	180	5
1	181	F
2	181	6
1	182	F
2	182	7
1	183	F
2	183	8
1	184	G
2	184	H
1	185	G
2	185	I
1	186	G
2	186	J
1	187	G
2	187	K
1	188	G
2	188	L
1	189	G
2	189	M
1	190	G
2	190	N
1	191	G
2	191	O
1	192	G
2	192	P
1	193	G
2	193	Q
1	194	G
2	194	R
1	195	G
2	195	S
1	196	G
2	196	T
1	197	G
2	197	U
1	198	G
2	198	V
1	199	G
2	199	W
1	200	G
2	200	X
1	201	G
2	201	Y
1	202	G
2	202	Z
1	203	G
2	203	1
1	204	G
2	204	2
1	205	G
2	205	3
1	206	G
2	206	4
1	207	G
2	207	5
1	208	G
2	208	6
1	209	G
2	209	7
1	210	G
2	210	8
1	211	H
2	211	I
1	212	H
2	212	J
1	213	H
2	213	K
1	214	H
2	214	L
1	215	H
2	215	M
1	216	H
2	216	N
1	217	H
2	217	O
1	218	H
2	218	P
1	219	H
2	219	Q
1	220	H
2	220	R
1	221	H
2	221	S
1	222	H
2	222	T
1	223	H
2	223	U
1	224	H
2	224	V
1	225	H
2	225	W
1	226	H
2	226	X
1	227	H
2	227	Y
1	228	H
2	228	Z
1	229	H
2	229	1
1	230	H
2	230	2
1	231	H
2	231	3
1	232	H
2	232	4
1	233	H
2	233	5
1	234	H
2	234	6
1	235	H
2	235	7
1	236	H
2	236	8
1	237	I
2	237	J
1	238	I
2	238	K
1	239	I
2	239	L
1	240	I
2	240	M
1	241	I
2	241	N
1	242	I
2	242	O
1	243	I
2	243	P
1	244	I
2	244	Q
1	245	I
2	245	R
1	246	I
2	246	S
1	247	I
2	247	T
1	248	I
2	248	U
1	249	I
2	249	V
1	250	I
2	250	W
1	251	I
2	251	X
1	252	I
2	252	Y
1	253	I
2	253	Z
1	254	I
2	254	1
1	255	I
2	255	2
1	256	I
2	256	3
1	257	I
2	257	4
1	258	I
2	258	5
1	259	I
2	259	6
1	260	I
2	260	7
1	261	I
2	261	8
1	262	J
2	262	K
1	263	J
2	263	L
1	264	J
2	264	M
1	265	J
2	265	N
1	266	J
2	266	O
1	267	J
2	267	P
1	268	J
2	268	Q
1	269	J
2	269	R
1	270	J
2	270	S
1	271	J
2	271	T
1	272	J
2	272	U
1	273	J
2	273	V
1	274	J
2	274	W
1	275	J
2	275	X
1	276	J
2	276	Y
1	277	J
2	277	Z
1	278	J
2	278	1
1	279	J
2	279	2
1	280	J
2	280	3
1	281	J
2	281	4
1	282	J
2	282	5
1	283	J
2	283	6
1	284	J
2	284	7
1	285	J
2	285	8
1	286	K
2	286	L
1	287	K
2	287	M
1	288	K
2	288	N
1	289	K
2	289	O
1	290	K
2	290	P
1	291	K
2	291	Q
1	292	K
2	292	R
1	293	K
2	293	S
1	294	K
2	294	T
1	295	K
2	295	U
1	296	K
2	296	V
1	297	K
2	297	W
1	298	K
2	298	X
1	299	K
2	299	Y
1	300	K
2	300	Z
1	301	K
2	301	1
1	302	K
2	302	2
1	303	K
2	303	3
1	304	K
2	304	4
1	305	K
2	305	5
1	306	K
2	306	6
1	307	K
2	307	7
1	308	K
2	308	8
1	309	L
2	309	M
1	310	L
2	310	N
1	311	L
2	311	O
1	312	L
2	312	P
1	313	L
2	313	Q
1	314	L
2	314	R
1	315	L
2	315	S
1	316	L
2	316	T
1	317	L
2	317	U
1	318	L
2	318	V
1	319	L
2	319	W
1	320	L
2	320	X
1	321	L
2	321	Y
1	322	L
2	322	Z
1	323	L
2	323	1
1	324	L
2	324	2
1	325	L
2	325	3
1	326	L
2	326	4
1	327	L
2	327	5
1	328	L
2	328	6
1	329	L
2	329	7
1	330	L
2	330	8
1	331	M
2	331	N
1	332	M
2	332	O
1	333	M
2	333	P
1	334	M
2	334	Q
1	335	M
2	335	R
1	336	M
2	336	S
1	337	M
2	337	T
1	338	M
2	338	U
1	339	M
2	339	V
1	340	M
2	340	W
1	341	M
2	341	X
1	342	M
2	342	Y
1	343	M
2	343	Z
1	344	M
2	344	1
1	345	M
2	345	2
1	346	M
2	346	3
1	347	M
2	347	4
1	348	M
2	348	5
1	349	M
2	349	6
1	350	M
2	350	7
1	351	M
2	351	8
1	352	N
2	352	O
1	353	N
2	353	P
1	354	N
2	354	Q
1	355	N
2	355	R
1	356	N
2	356	S
1	357	N
2	357	T
1	358	N
2	358	U
1	359	N
2	359	V
1	360	N
2	360	W
1	361	N
2	361	X
1	362	N
2	362	Y
1	363	N
2	363	Z
1	364	N
2	364	1
1	365	N
2	365	2
1	366	N
2	366	3
1	367	N
2	367	4
1	368	N
2	368	5
1	369	N
2	369	6
1	370	N
2	370	7
1	371	N
2	371	8
1	372	O
2	372	P
1	373	O
2	373	Q
1	374	O
2	374	R
1	375	O
2	375	S
1	376	O
2	376	T
1	377	O
2	377	U
1	378	O
2	378	V
1	379	O
2	379	W
1	380	O
2	380	X
1	381	O
2	381	Y
1	382	O
2	382	Z
1	383	O
2	383	1
1	384	O
2	384	2
1	385	O
2	385	3
1	386	O
2	386	4
1	387	O
2	387	5
1	388	O
2	388	6
1	389	O
2	389	7
1	390	O
2	390	8
1	391	P
2	391	Q
1	392	P
2	392	R
1	393	P
2	393	S
1	394	P
2	394	T
1	395	P
2	395	U
1	396	P
2	396	V
1	397	P
2	397	W
1	398	P
2	398	X
1	399	P
2	399	Y
1	400	P
2	400	Z
1	401	P
2	401	1
1	402	P
2	402	2
1	403	P
2	403	3
1	404	P
2	404	4
1	405	P
2	405	5
1	406	P
2	406	6
1	407	P
2	407	7
1	408	P
2	408	8
1	409	Q
2	409	R
1	410	Q
2	410	S
1	411	Q
2	411	T
1	412	Q
2	412	U
1	413	Q
2	413	V
1	414	Q
2	414	W
1	415	Q
2	415	X
1	416	Q
2	416	Y
1	417	Q
2	417	Z
1	418	Q
2	418	1
1	419	Q
2	419	2
1	420	Q
2	420	3
1	421	Q
2	421	4
1	422	Q
2	422	5
1	423	Q
2	423	6
1	424	Q
2	424	7
1	425	Q
2	425	8
1	426	R
2	426	S
1	427	R
2	427	T
1	428	R
2	428	U
1	429	R
2	429	V
1	430	R
2	430	W
1	431	R
2	431	X
1	432	R
2	432	Y
1	433	R
2	433	Z
1	434	R
2	434	1
1	435	R
2	435	2
1	436	R
2	436	3
1	437	R
2	437	4
1	438	R
2	438	5
1	439	R
2	439	6
1	440	R
2	440	7
1	441	R
2	441	8
1	442	S
2	442	T
1	443	S
2	443	U
1	444	S
2	444	V
1	445	S
2	445	W
1	446	S
2	446	X
1	447	S
2	447	Y
1	448	S
2	448	Z
1	449	S
2	449	1
1	450	S
2	450	2
1	451	S
2	451	3
1	452	S
2	452	4
1	453	S
2	453	5
1	454	S
2	454	6
1	455	S
2	455	7
1	456	S
2	456	8
1	457	T
2	457	U
1	458	T
2	458	V
1	459	T
2	459	W
1	460	T
2	460	X
1	461	T
2	461	Y
1	462	T
2	462	Z
1	463	T
2	463	1
1	464	T
2	464	2
1	465	T
2	465	3
1	466	T
2	466	4
1	467	T
2	467	5
1	468	T
2	468	6
1	469	T
2	469	7
1	470	T
2	470	8
1	471	U
2	471	V
1	472	U
2	472	W
1	473	U
2	473	X
1	474	U
2	474	Y
1	475	U
2	475	Z
1	476	U
2	476	1
1	477	U
2	477	2
1	478	U
2	478	3
1	479	U
2	479	4
1	480	U
2	480	5
1	481	U
2	481	6
1	482	U
2	482	7
1	483	U
2	483	8
1	484	V
2	484	W
1	485	V
2	485	X
1	486	V
2	486	Y
1	487	V
2	487	Z
1	488	V
2	488	1
1	489	V
2	489	2
1	490	V
2	490	3
1	491	V
2	491	4
1	492	V
2	492	5
1	493	V
2	493	6
1	494	V
2	494	7
1	495	V
2	495	8
1	496	W
2	496	X
1	497	W
2	497	Y
1	498	W
2	498	Z
1	499	W
2	499	1
1	500	W
2	500	2
1	501	W
2	501	3
1	502	W
2	502	4
1	503	W
2	503	5
1	504	W
2	504	6
1	505	W
2	505	7
1	506	W
2	506	8
1	507	X
2	507	Y
1	508	X
2	508	Z
1	509	X
2	509	1
1	510	X
2	510	2
1	511	X
2	511	3
1	512	X
2	512	4
1	513	X
2	513	5
1	514	X
2	514	6
1	515	X
2	515	7
1	516	X
2	516	8
1	517	Y
2	517	Z
1	518	Y
2	518	1
1	519	Y
2	519	2
1	520	Y
2	520	3
1	521	Y
2	521	4
1	522	Y
2	522	5
1	523	Y
2	523	6
1	524	Y
2	524	7
1	525	Y
2	525	8
1	526	Z
2	526	1
1	527	Z
2	527	2
1	528	Z
2	528	3
1	529	Z
2	529	4
1	530	Z
2	530	5
1	531	Z
2	531	6
1	532	Z
2	532	7
1	533	Z
2	533	8
1	534	1
2	534	2
1	535	1
2	535	3
1	536	1
2	536	4
1	537	1
2	537	5
1	538	1
2	538	6
1	539	1
2	539	7
1	540	1
2	540	8
1	541	2
2	541	3
1	542	2
2	542	4
1	543	2
2	543	5
1	544	2
2	544	6
1	545	2
2	545	7
1	546	2
2	546	8
1	547	3
2	547	4
1	548	3
2	548	5
1	549	3
2	549	6
1	550	3
2	550	7
1	551	3
2	551	8
1	552	4
2	552	5
1	553	4
2	553	6
1	554	4
2	554	7
1	555	4
2	555	8
1	556	5
2	556	6
1	557	5
2	557	7
1	558	5
2	558	8
1	559	6
2	559	7
1	560	6
2	560	8
1	561	7
2	561	8

NCS domain segments:

Dom-ID	Ens-ID	Auth asym-ID	Auth seq-ID
1	1	A	1 - 241
2	1	B	1 - 241
1	2	A	1 - 241
2	2	C	1 - 241
1	3	A	1 - 241
2	3	D	1 - 241
1	4	A	1 - 241
2	4	E	1 - 241
1	5	A	1 - 241
2	5	F	1 - 241
1	6	A	1 - 241
2	6	G	1 - 241
1	7	A	1 - 241
2	7	H	1 - 241
1	8	A	1 - 241
2	8	I	1 - 241
1	9	A	1 - 241
2	9	J	1 - 241
1	10	A	1 - 241
2	10	K	1 - 241
1	11	A	1 - 241
2	11	L	1 - 241
1	12	A	1 - 241
2	12	M	1 - 241
1	13	A	1 - 241
2	13	N	1 - 241
1	14	A	1 - 241
2	14	O	1 - 241
1	15	A	1 - 241
2	15	P	1 - 241
1	16	A	1 - 241
2	16	Q	1 - 241
1	17	A	1 - 241
2	17	R	1 - 241
1	18	A	1 - 241
2	18	S	1 - 241
1	19	A	1 - 241
2	19	T	1 - 241
1	20	A	1 - 241
2	20	U	1 - 241
1	21	A	1 - 241
2	21	V	1 - 241
1	22	A	1 - 241
2	22	W	1 - 241
1	23	A	1 - 241
2	23	X	1 - 241
1	24	A	1 - 241
2	24	Y	1 - 241
1	25	A	1 - 241
2	25	Z	1 - 241
1	26	A	1 - 241
2	26	1	1 - 241
1	27	A	1 - 241
2	27	2	1 - 241
1	28	A	1 - 241
2	28	3	1 - 241
1	29	A	1 - 241
2	29	4	1 - 241
1	30	A	1 - 241
2	30	5	1 - 241
1	31	A	1 - 241
2	31	6	1 - 241
1	32	A	1 - 241
2	32	7	1 - 241
1	33	A	1 - 241
2	33	8	1 - 241
1	34	B	1 - 241
2	34	C	1 - 241
1	35	B	1 - 241
2	35	D	1 - 241
1	36	B	1 - 241
2	36	E	1 - 241
1	37	B	1 - 241
2	37	F	1 - 241
1	38	B	1 - 241
2	38	G	1 - 241
1	39	B	1 - 241
2	39	H	1 - 241
1	40	B	1 - 241
2	40	I	1 - 241
1	41	B	1 - 241
2	41	J	1 - 241
1	42	B	1 - 241
2	42	K	1 - 241
1	43	B	1 - 241
2	43	L	1 - 241
1	44	B	1 - 241
2	44	M	1 - 241
1	45	B	1 - 241
2	45	N	1 - 241
1	46	B	1 - 241
2	46	O	1 - 241
1	47	B	1 - 241
2	47	P	1 - 241
1	48	B	1 - 241
2	48	Q	1 - 241
1	49	B	1 - 241
2	49	R	1 - 241
1	50	B	1 - 241
2	50	S	1 - 241
1	51	B	1 - 241
2	51	T	1 - 241
1	52	B	1 - 241
2	52	U	1 - 241
1	53	B	1 - 241
2	53	V	1 - 241
1	54	B	1 - 241
2	54	W	1 - 241
1	55	B	1 - 241
2	55	X	1 - 241
1	56	B	1 - 241
2	56	Y	1 - 241
1	57	B	1 - 241
2	57	Z	1 - 241
1	58	B	1 - 241
2	58	1	1 - 241
1	59	B	1 - 241
2	59	2	1 - 241
1	60	B	1 - 241
2	60	3	1 - 241
1	61	B	1 - 241
2	61	4	1 - 241
1	62	B	1 - 241
2	62	5	1 - 241
1	63	B	1 - 241
2	63	6	1 - 241
1	64	B	1 - 241
2	64	7	1 - 241
1	65	B	1 - 241
2	65	8	1 - 241
1	66	C	1 - 241
2	66	D	1 - 241
1	67	C	1 - 241
2	67	E	1 - 241
1	68	C	1 - 241
2	68	F	1 - 241
1	69	C	1 - 241
2	69	G	1 - 241
1	70	C	1 - 241
2	70	H	1 - 241
1	71	C	1 - 241
2	71	I	1 - 241
1	72	C	1 - 241
2	72	J	1 - 241
1	73	C	1 - 241
2	73	K	1 - 241
1	74	C	1 - 241
2	74	L	1 - 241
1	75	C	1 - 241
2	75	M	1 - 241
1	76	C	1 - 241
2	76	N	1 - 241
1	77	C	1 - 241
2	77	O	1 - 241
1	78	C	1 - 241
2	78	P	1 - 241
1	79	C	1 - 241
2	79	Q	1 - 241
1	80	C	1 - 241
2	80	R	1 - 241
1	81	C	1 - 241
2	81	S	1 - 241
1	82	C	1 - 241
2	82	T	1 - 241
1	83	C	1 - 241
2	83	U	1 - 241
1	84	C	1 - 241
2	84	V	1 - 241
1	85	C	1 - 241
2	85	W	1 - 241
1	86	C	1 - 241
2	86	X	1 - 241
1	87	C	1 - 241
2	87	Y	1 - 241
1	88	C	1 - 241
2	88	Z	1 - 241
1	89	C	1 - 241
2	89	1	1 - 241
1	90	C	1 - 241
2	90	2	1 - 241
1	91	C	1 - 241
2	91	3	1 - 241
1	92	C	1 - 241
2	92	4	1 - 241
1	93	C	1 - 241
2	93	5	1 - 241
1	94	C	1 - 241
2	94	6	1 - 241
1	95	C	1 - 241
2	95	7	1 - 241
1	96	C	1 - 241
2	96	8	1 - 241
1	97	D	1 - 241
2	97	E	1 - 241
1	98	D	1 - 241
2	98	F	1 - 241
1	99	D	1 - 241
2	99	G	1 - 241
1	100	D	1 - 241
2	100	H	1 - 241
1	101	D	1 - 241
2	101	I	1 - 241
1	102	D	1 - 241
2	102	J	1 - 241
1	103	D	1 - 241
2	103	K	1 - 241
1	104	D	1 - 241
2	104	L	1 - 241
1	105	D	1 - 241
2	105	M	1 - 241
1	106	D	1 - 241
2	106	N	1 - 241
1	107	D	1 - 241
2	107	O	1 - 241
1	108	D	1 - 241
2	108	P	1 - 241
1	109	D	1 - 241
2	109	Q	1 - 241
1	110	D	1 - 241
2	110	R	1 - 241
1	111	D	1 - 241
2	111	S	1 - 241
1	112	D	1 - 241
2	112	T	1 - 241
1	113	D	1 - 241
2	113	U	1 - 241
1	114	D	1 - 241
2	114	V	1 - 241
1	115	D	1 - 241
2	115	W	1 - 241
1	116	D	1 - 241
2	116	X	1 - 241
1	117	D	1 - 241
2	117	Y	1 - 241
1	118	D	1 - 241
2	118	Z	1 - 241
1	119	D	1 - 241
2	119	1	1 - 241
1	120	D	1 - 241
2	120	2	1 - 241
1	121	D	1 - 241
2	121	3	1 - 241
1	122	D	1 - 241
2	122	4	1 - 241
1	123	D	1 - 241
2	123	5	1 - 241
1	124	D	1 - 241
2	124	6	1 - 241
1	125	D	1 - 241
2	125	7	1 - 241
1	126	D	1 - 241
2	126	8	1 - 241
1	127	E	1 - 241
2	127	F	1 - 241
1	128	E	1 - 241
2	128	G	1 - 241
1	129	E	1 - 241
2	129	H	1 - 241
1	130	E	1 - 241
2	130	I	1 - 241
1	131	E	1 - 241
2	131	J	1 - 241
1	132	E	1 - 241
2	132	K	1 - 241
1	133	E	1 - 241
2	133	L	1 - 241
1	134	E	1 - 241
2	134	M	1 - 241
1	135	E	1 - 241
2	135	N	1 - 241
1	136	E	1 - 241
2	136	O	1 - 241
1	137	E	1 - 241
2	137	P	1 - 241
1	138	E	1 - 241
2	138	Q	1 - 241
1	139	E	1 - 241
2	139	R	1 - 241
1	140	E	1 - 241
2	140	S	1 - 241
1	141	E	1 - 241
2	141	T	1 - 241
1	142	E	1 - 241
2	142	U	1 - 241
1	143	E	1 - 241
2	143	V	1 - 241
1	144	E	1 - 241
2	144	W	1 - 241
1	145	E	1 - 241
2	145	X	1 - 241
1	146	E	1 - 241
2	146	Y	1 - 241
1	147	E	1 - 241
2	147	Z	1 - 241
1	148	E	1 - 241
2	148	1	1 - 241
1	149	E	1 - 241
2	149	2	1 - 241
1	150	E	1 - 241
2	150	3	1 - 241
1	151	E	1 - 241
2	151	4	1 - 241
1	152	E	1 - 241
2	152	5	1 - 241
1	153	E	1 - 241
2	153	6	1 - 241
1	154	E	1 - 241
2	154	7	1 - 241
1	155	E	1 - 241
2	155	8	1 - 241
1	156	F	1 - 241
2	156	G	1 - 241
1	157	F	1 - 241
2	157	H	1 - 241
1	158	F	1 - 241
2	158	I	1 - 241
1	159	F	1 - 241
2	159	J	1 - 241
1	160	F	1 - 241
2	160	K	1 - 241
1	161	F	1 - 241
2	161	L	1 - 241
1	162	F	1 - 241
2	162	M	1 - 241
1	163	F	1 - 241
2	163	N	1 - 241
1	164	F	1 - 241
2	164	O	1 - 241
1	165	F	1 - 241
2	165	P	1 - 241
1	166	F	1 - 241
2	166	Q	1 - 241
1	167	F	1 - 241
2	167	R	1 - 241
1	168	F	1 - 241
2	168	S	1 - 241
1	169	F	1 - 241
2	169	T	1 - 241
1	170	F	1 - 241
2	170	U	1 - 241
1	171	F	1 - 241
2	171	V	1 - 241
1	172	F	1 - 241
2	172	W	1 - 241
1	173	F	1 - 241
2	173	X	1 - 241
1	174	F	1 - 241
2	174	Y	1 - 241
1	175	F	1 - 241
2	175	Z	1 - 241
1	176	F	1 - 241
2	176	1	1 - 241
1	177	F	1 - 241
2	177	2	1 - 241
1	178	F	1 - 241
2	178	3	1 - 241
1	179	F	1 - 241
2	179	4	1 - 241
1	180	F	1 - 241
2	180	5	1 - 241
1	181	F	1 - 241
2	181	6	1 - 241
1	182	F	1 - 241
2	182	7	1 - 241
1	183	F	1 - 241
2	183	8	1 - 241
1	184	G	1 - 241
2	184	H	1 - 241
1	185	G	1 - 241
2	185	I	1 - 241
1	186	G	1 - 241
2	186	J	1 - 241
1	187	G	1 - 241
2	187	K	1 - 241
1	188	G	1 - 241
2	188	L	1 - 241
1	189	G	1 - 241
2	189	M	1 - 241
1	190	G	1 - 241
2	190	N	1 - 241
1	191	G	1 - 241
2	191	O	1 - 241
1	192	G	1 - 241
2	192	P	1 - 241
1	193	G	1 - 241
2	193	Q	1 - 241
1	194	G	1 - 241
2	194	R	1 - 241
1	195	G	1 - 241
2	195	S	1 - 241
1	196	G	1 - 241
2	196	T	1 - 241
1	197	G	1 - 241
2	197	U	1 - 241
1	198	G	1 - 241
2	198	V	1 - 241
1	199	G	1 - 241
2	199	W	1 - 241
1	200	G	1 - 241
2	200	X	1 - 241
1	201	G	1 - 241
2	201	Y	1 - 241
1	202	G	1 - 241
2	202	Z	1 - 241
1	203	G	1 - 241
2	203	1	1 - 241
1	204	G	1 - 241
2	204	2	1 - 241
1	205	G	1 - 241
2	205	3	1 - 241
1	206	G	1 - 241
2	206	4	1 - 241
1	207	G	1 - 241
2	207	5	1 - 241
1	208	G	1 - 241
2	208	6	1 - 241
1	209	G	1 - 241
2	209	7	1 - 241
1	210	G	1 - 241
2	210	8	1 - 241
1	211	H	1 - 241
2	211	I	1 - 241
1	212	H	1 - 241
2	212	J	1 - 241
1	213	H	1 - 241
2	213	K	1 - 241
1	214	H	1 - 241
2	214	L	1 - 241
1	215	H	1 - 241
2	215	M	1 - 241
1	216	H	1 - 241
2	216	N	1 - 241
1	217	H	1 - 241
2	217	O	1 - 241
1	218	H	1 - 241
2	218	P	1 - 241
1	219	H	1 - 241
2	219	Q	1 - 241
1	220	H	1 - 241
2	220	R	1 - 241
1	221	H	1 - 241
2	221	S	1 - 241
1	222	H	1 - 241
2	222	T	1 - 241
1	223	H	1 - 241
2	223	U	1 - 241
1	224	H	1 - 241
2	224	V	1 - 241
1	225	H	1 - 241
2	225	W	1 - 241
1	226	H	1 - 241
2	226	X	1 - 241
1	227	H	1 - 241
2	227	Y	1 - 241
1	228	H	1 - 241
2	228	Z	1 - 241
1	229	H	1 - 241
2	229	1	1 - 241
1	230	H	1 - 241
2	230	2	1 - 241
1	231	H	1 - 241
2	231	3	1 - 241
1	232	H	1 - 241
2	232	4	1 - 241
1	233	H	1 - 241
2	233	5	1 - 241
1	234	H	1 - 241
2	234	6	1 - 241
1	235	H	1 - 241
2	235	7	1 - 241
1	236	H	1 - 241
2	236	8	1 - 241
1	237	I	1 - 241
2	237	J	1 - 241
1	238	I	1 - 241
2	238	K	1 - 241
1	239	I	1 - 241
2	239	L	1 - 241
1	240	I	1 - 241
2	240	M	1 - 241
1	241	I	1 - 241
2	241	N	1 - 241
1	242	I	1 - 241
2	242	O	1 - 241
1	243	I	1 - 241
2	243	P	1 - 241
1	244	I	1 - 241
2	244	Q	1 - 241
1	245	I	1 - 241
2	245	R	1 - 241
1	246	I	1 - 241
2	246	S	1 - 241
1	247	I	1 - 241
2	247	T	1 - 241
1	248	I	1 - 241
2	248	U	1 - 241
1	249	I	1 - 241
2	249	V	1 - 241
1	250	I	1 - 241
2	250	W	1 - 241
1	251	I	1 - 241
2	251	X	1 - 241
1	252	I	1 - 241
2	252	Y	1 - 241
1	253	I	1 - 241
2	253	Z	1 - 241
1	254	I	1 - 241
2	254	1	1 - 241
1	255	I	1 - 241
2	255	2	1 - 241
1	256	I	1 - 241
2	256	3	1 - 241
1	257	I	1 - 241
2	257	4	1 - 241
1	258	I	1 - 241
2	258	5	1 - 241
1	259	I	1 - 241
2	259	6	1 - 241
1	260	I	1 - 241
2	260	7	1 - 241
1	261	I	1 - 241
2	261	8	1 - 241
1	262	J	1 - 241
2	262	K	1 - 241
1	263	J	1 - 241
2	263	L	1 - 241
1	264	J	1 - 241
2	264	M	1 - 241
1	265	J	1 - 241
2	265	N	1 - 241
1	266	J	1 - 241
2	266	O	1 - 241
1	267	J	1 - 241
2	267	P	1 - 241
1	268	J	1 - 241
2	268	Q	1 - 241
1	269	J	1 - 241
2	269	R	1 - 241
1	270	J	1 - 241
2	270	S	1 - 241
1	271	J	1 - 241
2	271	T	1 - 241
1	272	J	1 - 241
2	272	U	1 - 241
1	273	J	1 - 241
2	273	V	1 - 241
1	274	J	1 - 241
2	274	W	1 - 241
1	275	J	1 - 241
2	275	X	1 - 241
1	276	J	1 - 241
2	276	Y	1 - 241
1	277	J	1 - 241
2	277	Z	1 - 241
1	278	J	1 - 241
2	278	1	1 - 241
1	279	J	1 - 241
2	279	2	1 - 241
1	280	J	1 - 241
2	280	3	1 - 241
1	281	J	1 - 241
2	281	4	1 - 241
1	282	J	1 - 241
2	282	5	1 - 241
1	283	J	1 - 241
2	283	6	1 - 241
1	284	J	1 - 241
2	284	7	1 - 241
1	285	J	1 - 241
2	285	8	1 - 241
1	286	K	1 - 241
2	286	L	1 - 241
1	287	K	1 - 241
2	287	M	1 - 241
1	288	K	1 - 241
2	288	N	1 - 241
1	289	K	1 - 241
2	289	O	1 - 241
1	290	K	1 - 241
2	290	P	1 - 241
1	291	K	1 - 241
2	291	Q	1 - 241
1	292	K	1 - 241
2	292	R	1 - 241
1	293	K	1 - 241
2	293	S	1 - 241
1	294	K	1 - 241
2	294	T	1 - 241
1	295	K	1 - 241
2	295	U	1 - 241
1	296	K	1 - 241
2	296	V	1 - 241
1	297	K	1 - 241
2	297	W	1 - 241
1	298	K	1 - 241
2	298	X	1 - 241
1	299	K	1 - 241
2	299	Y	1 - 241
1	300	K	1 - 241
2	300	Z	1 - 241
1	301	K	1 - 241
2	301	1	1 - 241
1	302	K	1 - 241
2	302	2	1 - 241
1	303	K	1 - 241
2	303	3	1 - 241
1	304	K	1 - 241
2	304	4	1 - 241
1	305	K	1 - 241
2	305	5	1 - 241
1	306	K	1 - 241
2	306	6	1 - 241
1	307	K	1 - 241
2	307	7	1 - 241
1	308	K	1 - 241
2	308	8	1 - 241
1	309	L	1 - 241
2	309	M	1 - 241
1	310	L	1 - 241
2	310	N	1 - 241
1	311	L	1 - 241
2	311	O	1 - 241
1	312	L	1 - 241
2	312	P	1 - 241
1	313	L	1 - 241
2	313	Q	1 - 241
1	314	L	1 - 241
2	314	R	1 - 241
1	315	L	1 - 241
2	315	S	1 - 241
1	316	L	1 - 241
2	316	T	1 - 241
1	317	L	1 - 241
2	317	U	1 - 241
1	318	L	1 - 241
2	318	V	1 - 241
1	319	L	1 - 241
2	319	W	1 - 241
1	320	L	1 - 241
2	320	X	1 - 241
1	321	L	1 - 241
2	321	Y	1 - 241
1	322	L	1 - 241
2	322	Z	1 - 241
1	323	L	1 - 241
2	323	1	1 - 241
1	324	L	1 - 241
2	324	2	1 - 241
1	325	L	1 - 241
2	325	3	1 - 241
1	326	L	1 - 241
2	326	4	1 - 241
1	327	L	1 - 241
2	327	5	1 - 241
1	328	L	1 - 241
2	328	6	1 - 241
1	329	L	1 - 241
2	329	7	1 - 241
1	330	L	1 - 241
2	330	8	1 - 241
1	331	M	1 - 241
2	331	N	1 - 241
1	332	M	1 - 241
2	332	O	1 - 241
1	333	M	1 - 241
2	333	P	1 - 241
1	334	M	1 - 241
2	334	Q	1 - 241
1	335	M	1 - 241
2	335	R	1 - 241
1	336	M	1 - 241
2	336	S	1 - 241
1	337	M	1 - 241
2	337	T	1 - 241
1	338	M	1 - 241
2	338	U	1 - 241
1	339	M	1 - 241
2	339	V	1 - 241
1	340	M	1 - 241
2	340	W	1 - 241
1	341	M	1 - 241
2	341	X	1 - 241
1	342	M	1 - 241
2	342	Y	1 - 241
1	343	M	1 - 241
2	343	Z	1 - 241
1	344	M	1 - 241
2	344	1	1 - 241
1	345	M	1 - 241
2	345	2	1 - 241
1	346	M	1 - 241
2	346	3	1 - 241
1	347	M	1 - 241
2	347	4	1 - 241
1	348	M	1 - 241
2	348	5	1 - 241
1	349	M	1 - 241
2	349	6	1 - 241
1	350	M	1 - 241
2	350	7	1 - 241
1	351	M	1 - 241
2	351	8	1 - 241
1	352	N	1 - 241
2	352	O	1 - 241
1	353	N	1 - 241
2	353	P	1 - 241
1	354	N	1 - 241
2	354	Q	1 - 241
1	355	N	1 - 241
2	355	R	1 - 241
1	356	N	1 - 241
2	356	S	1 - 241
1	357	N	1 - 241
2	357	T	1 - 241
1	358	N	1 - 241
2	358	U	1 - 241
1	359	N	1 - 241
2	359	V	1 - 241
1	360	N	1 - 241
2	360	W	1 - 241
1	361	N	1 - 241
2	361	X	1 - 241
1	362	N	1 - 241
2	362	Y	1 - 241
1	363	N	1 - 241
2	363	Z	1 - 241
1	364	N	1 - 241
2	364	1	1 - 241
1	365	N	1 - 241
2	365	2	1 - 241
1	366	N	1 - 241
2	366	3	1 - 241
1	367	N	1 - 241
2	367	4	1 - 241
1	368	N	1 - 241
2	368	5	1 - 241
1	369	N	1 - 241
2	369	6	1 - 241
1	370	N	1 - 241
2	370	7	1 - 241
1	371	N	1 - 241
2	371	8	1 - 241
1	372	O	1 - 241
2	372	P	1 - 241
1	373	O	1 - 241
2	373	Q	1 - 241
1	374	O	1 - 241
2	374	R	1 - 241
1	375	O	1 - 241
2	375	S	1 - 241
1	376	O	1 - 241
2	376	T	1 - 241
1	377	O	1 - 241
2	377	U	1 - 241
1	378	O	1 - 241
2	378	V	1 - 241
1	379	O	1 - 241
2	379	W	1 - 241
1	380	O	1 - 241
2	380	X	1 - 241
1	381	O	1 - 241
2	381	Y	1 - 241
1	382	O	1 - 241
2	382	Z	1 - 241
1	383	O	1 - 241
2	383	1	1 - 241
1	384	O	1 - 241
2	384	2	1 - 241
1	385	O	1 - 241
2	385	3	1 - 241
1	386	O	1 - 241
2	386	4	1 - 241
1	387	O	1 - 241
2	387	5	1 - 241
1	388	O	1 - 241
2	388	6	1 - 241
1	389	O	1 - 241
2	389	7	1 - 241
1	390	O	1 - 241
2	390	8	1 - 241
1	391	P	1 - 241
2	391	Q	1 - 241
1	392	P	1 - 241
2	392	R	1 - 241
1	393	P	1 - 241
2	393	S	1 - 241
1	394	P	1 - 241
2	394	T	1 - 241
1	395	P	1 - 241
2	395	U	1 - 241
1	396	P	1 - 241
2	396	V	1 - 241
1	397	P	1 - 241
2	397	W	1 - 241
1	398	P	1 - 241
2	398	X	1 - 241
1	399	P	1 - 241
2	399	Y	1 - 241
1	400	P	1 - 241
2	400	Z	1 - 241
1	401	P	1 - 241
2	401	1	1 - 241
1	402	P	1 - 241
2	402	2	1 - 241
1	403	P	1 - 241
2	403	3	1 - 241
1	404	P	1 - 241
2	404	4	1 - 241
1	405	P	1 - 241
2	405	5	1 - 241
1	406	P	1 - 241
2	406	6	1 - 241
1	407	P	1 - 241
2	407	7	1 - 241
1	408	P	1 - 241
2	408	8	1 - 241
1	409	Q	1 - 241
2	409	R	1 - 241
1	410	Q	1 - 241
2	410	S	1 - 241
1	411	Q	1 - 241
2	411	T	1 - 241
1	412	Q	1 - 241
2	412	U	1 - 241
1	413	Q	1 - 241
2	413	V	1 - 241
1	414	Q	1 - 241
2	414	W	1 - 241
1	415	Q	1 - 241
2	415	X	1 - 241
1	416	Q	1 - 241
2	416	Y	1 - 241
1	417	Q	1 - 241
2	417	Z	1 - 241
1	418	Q	1 - 241
2	418	1	1 - 241
1	419	Q	1 - 241
2	419	2	1 - 241
1	420	Q	1 - 241
2	420	3	1 - 241
1	421	Q	1 - 241
2	421	4	1 - 241
1	422	Q	1 - 241
2	422	5	1 - 241
1	423	Q	1 - 241
2	423	6	1 - 241
1	424	Q	1 - 241
2	424	7	1 - 241
1	425	Q	1 - 241
2	425	8	1 - 241
1	426	R	1 - 241
2	426	S	1 - 241
1	427	R	1 - 241
2	427	T	1 - 241
1	428	R	1 - 241
2	428	U	1 - 241
1	429	R	1 - 241
2	429	V	1 - 241
1	430	R	1 - 241
2	430	W	1 - 241
1	431	R	1 - 241
2	431	X	1 - 241
1	432	R	1 - 241
2	432	Y	1 - 241
1	433	R	1 - 241
2	433	Z	1 - 241
1	434	R	1 - 241
2	434	1	1 - 241
1	435	R	1 - 241
2	435	2	1 - 241
1	436	R	1 - 241
2	436	3	1 - 241
1	437	R	1 - 241
2	437	4	1 - 241
1	438	R	1 - 241
2	438	5	1 - 241
1	439	R	1 - 241
2	439	6	1 - 241
1	440	R	1 - 241
2	440	7	1 - 241
1	441	R	1 - 241
2	441	8	1 - 241
1	442	S	1 - 241
2	442	T	1 - 241
1	443	S	1 - 241
2	443	U	1 - 241
1	444	S	1 - 241
2	444	V	1 - 241
1	445	S	1 - 241
2	445	W	1 - 241
1	446	S	1 - 241
2	446	X	1 - 241
1	447	S	1 - 241
2	447	Y	1 - 241
1	448	S	1 - 241
2	448	Z	1 - 241
1	449	S	1 - 241
2	449	1	1 - 241
1	450	S	1 - 241
2	450	2	1 - 241
1	451	S	1 - 241
2	451	3	1 - 241
1	452	S	1 - 241
2	452	4	1 - 241
1	453	S	1 - 241
2	453	5	1 - 241
1	454	S	1 - 241
2	454	6	1 - 241
1	455	S	1 - 241
2	455	7	1 - 241
1	456	S	1 - 241
2	456	8	1 - 241
1	457	T	1 - 241
2	457	U	1 - 241
1	458	T	1 - 241
2	458	V	1 - 241
1	459	T	1 - 241
2	459	W	1 - 241
1	460	T	1 - 241
2	460	X	1 - 241
1	461	T	1 - 241
2	461	Y	1 - 241
1	462	T	1 - 241
2	462	Z	1 - 241
1	463	T	1 - 241
2	463	1	1 - 241
1	464	T	1 - 241
2	464	2	1 - 241
1	465	T	1 - 241
2	465	3	1 - 241
1	466	T	1 - 241
2	466	4	1 - 241
1	467	T	1 - 241
2	467	5	1 - 241
1	468	T	1 - 241
2	468	6	1 - 241
1	469	T	1 - 241
2	469	7	1 - 241
1	470	T	1 - 241
2	470	8	1 - 241
1	471	U	1 - 241
2	471	V	1 - 241
1	472	U	1 - 241
2	472	W	1 - 241
1	473	U	1 - 241
2	473	X	1 - 241
1	474	U	1 - 241
2	474	Y	1 - 241
1	475	U	1 - 241
2	475	Z	1 - 241
1	476	U	1 - 241
2	476	1	1 - 241
1	477	U	1 - 241
2	477	2	1 - 241
1	478	U	1 - 241
2	478	3	1 - 241
1	479	U	1 - 241
2	479	4	1 - 241
1	480	U	1 - 241
2	480	5	1 - 241
1	481	U	1 - 241
2	481	6	1 - 241
1	482	U	1 - 241
2	482	7	1 - 241
1	483	U	1 - 241
2	483	8	1 - 241
1	484	V	1 - 241
2	484	W	1 - 241
1	485	V	1 - 241
2	485	X	1 - 241
1	486	V	1 - 241
2	486	Y	1 - 241
1	487	V	1 - 241
2	487	Z	1 - 241
1	488	V	1 - 241
2	488	1	1 - 241
1	489	V	1 - 241
2	489	2	1 - 241
1	490	V	1 - 241
2	490	3	1 - 241
1	491	V	1 - 241
2	491	4	1 - 241
1	492	V	1 - 241
2	492	5	1 - 241
1	493	V	1 - 241
2	493	6	1 - 241
1	494	V	1 - 241
2	494	7	1 - 241
1	495	V	1 - 241
2	495	8	1 - 241
1	496	W	1 - 241
2	496	X	1 - 241
1	497	W	1 - 241
2	497	Y	1 - 241
1	498	W	1 - 241
2	498	Z	1 - 241
1	499	W	1 - 241
2	499	1	1 - 241
1	500	W	1 - 241
2	500	2	1 - 241
1	501	W	1 - 241
2	501	3	1 - 241
1	502	W	1 - 241
2	502	4	1 - 241
1	503	W	1 - 241
2	503	5	1 - 241
1	504	W	1 - 241
2	504	6	1 - 241
1	505	W	1 - 241
2	505	7	1 - 241
1	506	W	1 - 241
2	506	8	1 - 241
1	507	X	1 - 241
2	507	Y	1 - 241
1	508	X	1 - 241
2	508	Z	1 - 241
1	509	X	1 - 241
2	509	1	1 - 241
1	510	X	1 - 241
2	510	2	1 - 241
1	511	X	1 - 241
2	511	3	1 - 241
1	512	X	1 - 241
2	512	4	1 - 241
1	513	X	1 - 241
2	513	5	1 - 241
1	514	X	1 - 241
2	514	6	1 - 241
1	515	X	1 - 241
2	515	7	1 - 241
1	516	X	1 - 241
2	516	8	1 - 241
1	517	Y	1 - 241
2	517	Z	1 - 241
1	518	Y	1 - 241
2	518	1	1 - 241
1	519	Y	1 - 241
2	519	2	1 - 241
1	520	Y	1 - 241
2	520	3	1 - 241
1	521	Y	1 - 241
2	521	4	1 - 241
1	522	Y	1 - 241
2	522	5	1 - 241
1	523	Y	1 - 241
2	523	6	1 - 241
1	524	Y	1 - 241
2	524	7	1 - 241
1	525	Y	1 - 241
2	525	8	1 - 241
1	526	Z	1 - 241
2	526	1	1 - 241
1	527	Z	1 - 241
2	527	2	1 - 241
1	528	Z	1 - 241
2	528	3	1 - 241
1	529	Z	1 - 241
2	529	4	1 - 241
1	530	Z	1 - 241
2	530	5	1 - 241
1	531	Z	1 - 241
2	531	6	1 - 241
1	532	Z	1 - 241
2	532	7	1 - 241
1	533	Z	1 - 241
2	533	8	1 - 241
1	534	1	1 - 241
2	534	2	1 - 241
1	535	1	1 - 241
2	535	3	1 - 241
1	536	1	1 - 241
2	536	4	1 - 241
1	537	1	1 - 241
2	537	5	1 - 241
1	538	1	1 - 241
2	538	6	1 - 241
1	539	1	1 - 241
2	539	7	1 - 241
1	540	1	1 - 241
2	540	8	1 - 241
1	541	2	1 - 241
2	541	3	1 - 241
1	542	2	1 - 241
2	542	4	1 - 241
1	543	2	1 - 241
2	543	5	1 - 241
1	544	2	1 - 241
2	544	6	1 - 241
1	545	2	1 - 241
2	545	7	1 - 241
1	546	2	1 - 241
2	546	8	1 - 241
1	547	3	1 - 241
2	547	4	1 - 241
1	548	3	1 - 241
2	548	5	1 - 241
1	549	3	1 - 241
2	549	6	1 - 241
1	550	3	1 - 241
2	550	7	1 - 241
1	551	3	1 - 241
2	551	8	1 - 241
1	552	4	1 - 241
2	552	5	1 - 241
1	553	4	1 - 241
2	553	6	1 - 241
1	554	4	1 - 241
2	554	7	1 - 241
1	555	4	1 - 241
2	555	8	1 - 241
1	556	5	1 - 241
2	556	6	1 - 241
1	557	5	1 - 241
2	557	7	1 - 241
1	558	5	1 - 241
2	558	8	1 - 241
1	559	6	1 - 241
2	559	7	1 - 241
1	560	6	1 - 241
2	560	8	1 - 241
1	561	7	1 - 241
2	561	8	1 - 241

NCS ensembles :

-
Components

#1: Protein	... Peptidase / ANCESTRAL BETA SUBUNIT Mass: 26647.344 Da / Num. of mol.: 34 / Mutation: L94M, L112M,L228M Source method: isolated from a genetically manipulated source Source: (gene. exp.) Pseudomonas aeruginosa (bacteria) Gene: AO946_34255, PAERUG_E15_London_28_01_14_04292, PAERUG_P32_London_17_VIM_2_10_11_02206 Production host: Escherichia coli (E. coli) / References: UniProt: A0A0D6I0H1

#1: Protein

...
Peptidase / ANCESTRAL BETA SUBUNIT

Mass: 26647.344 Da / Num. of mol.: 34 / Mutation: L94M, L112M,L228M
Source method: isolated from a genetically manipulated source
Source: (gene. exp.)

Pseudomonas aeruginosa (bacteria)
Gene: AO946_34255, PAERUG_E15_London_28_01_14_04292, PAERUG_P32_London_17_VIM_2_10_11_02206
Production host:

Escherichia coli (E. coli) / References: UniProt: A0A0D6I0H1

-
Experimental details

-
Experiment

Experiment	Method: X-RAY DIFFRACTION / Number of used crystals: 1

-
Sample preparation

Crystal	Density Matthews: 3.11 Å³/Da / Density % sol: 60.39 %
Crystal grow	Temperature: 295 K / Method: vapor diffusion, hanging drop / Details: 0.1 M sodium acetate pH 4.8, 1.2 M sodium nitrate

-
Data collection

Diffraction	Mean temperature: 100 K
Diffraction source	Source: SYNCHROTRON / Site: SLS / Beamline: X10SA / Wavelength: 0.979 Å
Detector	Type: DECTRIS PILATUS 6M / Detector: PIXEL / Date: Dec 13, 2013
Radiation	Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength	Wavelength: 0.979 Å / Relative weight: 1
Reflection	Resolution: 2.9→39.6 Å / Num. obs: 244138 / % possible obs: 99.6 % / Redundancy: 14.2 % / CC_1/2: 0.998 / R_merge(I) obs: 0.172 / Net I/σ(I): 14.33
Reflection shell	Resolution: 2.9→3.07 Å / Redundancy: 14.1 % / R_merge(I) obs: 1.193 / Mean I/σ(I) obs: 2.31 / CC_1/2: 0.822 / % possible all: 98.2

-
Processing

Software

Name	Version	Classification
REFMAC	5.8.0049	refinement
XDS		data reduction
XDS		data scaling
SHELXDE		phasing

Refinement

Method to determine structure:

SAD / Resolution: 2.9→39.6 Å / Cor.coef. F_o:F_c: 0.943 / Cor.coef. F_o:F_c free: 0.93 / SU B: 33.691 / SU ML: 0.271 / Cross valid method: THROUGHOUT / ESU R Free: 0.334 / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS

	R_factor	Num. reflection	% reflection	Selection details
R_free	0.2184	12254	5 %	RANDOM
R_work	0.19783	-	-	-
obs	0.19886	231884	99.69 %	-

Solvent computation

Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å

Displacement parameters

B_iso mean: 79.563 Å²

	B_aniso -1	B_aniso -2	B_aniso -3
1-	-0.92 Å²	-0 Å²	5.34 Å²
2-	-	-6.22 Å²	0 Å²
3-	-	-	2.94 Å²

Refinement step

Cycle: 1 / Resolution: 2.9→39.6 Å

	Protein	Nucleic acid	Ligand	Solvent	Total
Num. atoms	62186	0	0	0	62186

Refine LS restraints

Refine-ID	Type	Dev ideal	Dev ideal target	Number
X-RAY DIFFRACTION	r_bond_refined_d	0.012	0.019	63478
X-RAY DIFFRACTION	r_bond_other_d	0.008	0.02	59806
X-RAY DIFFRACTION	r_angle_refined_deg	1.446	1.981	86530
X-RAY DIFFRACTION	r_angle_other_deg	1.123	3	137088
X-RAY DIFFRACTION	r_dihedral_angle_1_deg	5.663	5	8160
X-RAY DIFFRACTION	r_dihedral_angle_2_deg	37.399	23.5	2720
X-RAY DIFFRACTION	r_dihedral_angle_3_deg	18.008	15	9282
X-RAY DIFFRACTION	r_dihedral_angle_4_deg	17.314	15	476
X-RAY DIFFRACTION	r_chiral_restr	0.072	0.2	10030
X-RAY DIFFRACTION	r_gen_planes_refined	0.009	0.021	73032
X-RAY DIFFRACTION	r_gen_planes_other	0.007	0.02	14620
X-RAY DIFFRACTION	r_nbd_refined
X-RAY DIFFRACTION	r_nbd_other
X-RAY DIFFRACTION	r_nbtor_refined
X-RAY DIFFRACTION	r_nbtor_other
X-RAY DIFFRACTION	r_xyhbond_nbd_refined
X-RAY DIFFRACTION	r_xyhbond_nbd_other
X-RAY DIFFRACTION	r_metal_ion_refined
X-RAY DIFFRACTION	r_metal_ion_other
X-RAY DIFFRACTION	r_symmetry_vdw_refined
X-RAY DIFFRACTION	r_symmetry_vdw_other
X-RAY DIFFRACTION	r_symmetry_hbond_refined
X-RAY DIFFRACTION	r_symmetry_hbond_other
X-RAY DIFFRACTION	r_symmetry_metal_ion_refined
X-RAY DIFFRACTION	r_symmetry_metal_ion_other
X-RAY DIFFRACTION	r_mcbond_it	3.455	4.772	32742
X-RAY DIFFRACTION	r_mcbond_other	3.455	4.772	32741
X-RAY DIFFRACTION	r_mcangle_it	5.43	7.165	40868
X-RAY DIFFRACTION	r_mcangle_other	5.43	7.165	40869
X-RAY DIFFRACTION	r_scbond_it	4.182	5.039	30736
X-RAY DIFFRACTION	r_scbond_other	4.182	5.039	30737
X-RAY DIFFRACTION	r_scangle_it
X-RAY DIFFRACTION	r_scangle_other	6.409	7.432	45663
X-RAY DIFFRACTION	r_long_range_B_refined	9.136	38.114	67126
X-RAY DIFFRACTION	r_long_range_B_other	9.136	38.114	67127
X-RAY DIFFRACTION	r_rigid_bond_restr
X-RAY DIFFRACTION	r_sphericity_free
X-RAY DIFFRACTION	r_sphericity_bonded

Refine LS restraints NCS

Refine-ID: X-RAY DIFFRACTION / Type: interatomic distance / Weight position: 0.05

Ens-ID	Dom-ID	Auth asym-ID	Number	Rms dev position (Å)
1	1	A	13999	0.03
1	2	B	13999	0.03
2	1	A	14061	0.02
2	2	C	14061	0.02
3	1	A	14013	0.03
3	2	D	14013	0.03
4	1	A	13939	0.04
4	2	E	13939	0.04
5	1	A	13991	0.04
5	2	F	13991	0.04
6	1	A	14038	0.03
6	2	G	14038	0.03
7	1	A	13993	0.03
7	2	H	13993	0.03
8	1	A	14054	0.02
8	2	I	14054	0.02
9	1	A	13977	0.03
9	2	J	13977	0.03
10	1	A	13988	0.03
10	2	K	13988	0.03
11	1	A	14038	0.03
11	2	L	14038	0.03
12	1	A	14008	0.03
12	2	M	14008	0.03
13	1	A	13987	0.03
13	2	N	13987	0.03
14	1	A	14033	0.02
14	2	O	14033	0.02
15	1	A	14045	0.02
15	2	P	14045	0.02
16	1	A	14030	0.03
16	2	Q	14030	0.03
17	1	A	13991	0.03
17	2	R	13991	0.03
18	1	A	14011	0.03
18	2	S	14011	0.03
19	1	A	14003	0.03
19	2	T	14003	0.03
20	1	A	14004	0.03
20	2	U	14004	0.03
21	1	A	14058	0.02
21	2	V	14058	0.02
22	1	A	13974	0.04
22	2	W	13974	0.04
23	1	A	14041	0.02
23	2	X	14041	0.02
24	1	A	14012	0.03
24	2	Y	14012	0.03
25	1	A	14034	0.03
25	2	Z	14034	0.03
26	1	A	13962	0.03
26	2	1	13962	0.03
27	1	A	14006	0.03
27	2	2	14006	0.03
28	1	A	14057	0.02
28	2	3	14057	0.02
29	1	A	13948	0.04
29	2	4	13948	0.04
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320	2	X	14011	0.03
321	1	L	14028	0.03
321	2	Y	14028	0.03
322	1	L	14053	0.03
322	2	Z	14053	0.03
323	1	L	14010	0.03
323	2	1	14010	0.03
324	1	L	14006	0.03
324	2	2	14006	0.03
325	1	L	14025	0.03
325	2	3	14025	0.03
326	1	L	14016	0.03
326	2	4	14016	0.03
327	1	L	13990	0.03
327	2	5	13990	0.03
328	1	L	14031	0.03
328	2	6	14031	0.03
329	1	L	14028	0.03
329	2	7	14028	0.03
330	1	L	14022	0.03
330	2	8	14022	0.03
331	1	M	14007	0.03
331	2	N	14007	0.03
332	1	M	14002	0.03
332	2	O	14002	0.03
333	1	M	13972	0.03
333	2	P	13972	0.03
334	1	M	14004	0.02
334	2	Q	14004	0.02
335	1	M	14037	0.02
335	2	R	14037	0.02
336	1	M	13977	0.03
336	2	S	13977	0.03
337	1	M	14026	0.03
337	2	T	14026	0.03
338	1	M	14006	0.03
338	2	U	14006	0.03
339	1	M	13999	0.03
339	2	V	13999	0.03
340	1	M	14002	0.03
340	2	W	14002	0.03
341	1	M	14046	0.02
341	2	X	14046	0.02
342	1	M	14055	0.01
342	2	Y	14055	0.01
343	1	M	14016	0.02
343	2	Z	14016	0.02
344	1	M	13941	0.03
344	2	1	13941	0.03
345	1	M	14033	0.02
345	2	2	14033	0.02
346	1	M	14007	0.03
346	2	3	14007	0.03
347	1	M	13995	0.03
347	2	4	13995	0.03
348	1	M	14032	0.02
348	2	5	14032	0.02
349	1	M	14060	0.01
349	2	6	14060	0.01
350	1	M	14028	0.03
350	2	7	14028	0.03
351	1	M	13984	0.03
351	2	8	13984	0.03
352	1	N	13996	0.03
352	2	O	13996	0.03
353	1	N	13951	0.03
353	2	P	13951	0.03
354	1	N	13970	0.03
354	2	Q	13970	0.03
355	1	N	14003	0.03
355	2	R	14003	0.03
356	1	N	14008	0.02
356	2	S	14008	0.02
357	1	N	14031	0.02
357	2	T	14031	0.02
358	1	N	14012	0.03
358	2	U	14012	0.03
359	1	N	13966	0.03
359	2	V	13966	0.03
360	1	N	14011	0.03
360	2	W	14011	0.03
361	1	N	14020	0.03
361	2	X	14020	0.03
362	1	N	14040	0.02
362	2	Y	14040	0.02
363	1	N	13988	0.03
363	2	Z	13988	0.03
364	1	N	13972	0.03
364	2	1	13972	0.03
365	1	N	14039	0.02
365	2	2	14039	0.02
366	1	N	13996	0.03
366	2	3	13996	0.03
367	1	N	14015	0.02
367	2	4	14015	0.02
368	1	N	14008	0.03
368	2	5	14008	0.03
369	1	N	14039	0.02
369	2	6	14039	0.02
370	1	N	14049	0.02
370	2	7	14049	0.02
371	1	N	13988	0.03
371	2	8	13988	0.03
372	1	O	14011	0.02
372	2	P	14011	0.02
373	1	O	14034	0.02
373	2	Q	14034	0.02
374	1	O	14007	0.03
374	2	R	14007	0.03
375	1	O	14007	0.03
375	2	S	14007	0.03
376	1	O	14008	0.03
376	2	T	14008	0.03
377	1	O	13993	0.03
377	2	U	13993	0.03
378	1	O	14014	0.02
378	2	V	14014	0.02
379	1	O	13982	0.03
379	2	W	13982	0.03
380	1	O	13997	0.03
380	2	X	13997	0.03
381	1	O	14029	0.03
381	2	Y	14029	0.03
382	1	O	14048	0.03
382	2	Z	14048	0.03
383	1	O	13981	0.03
383	2	1	13981	0.03
384	1	O	14021	0.02
384	2	2	14021	0.02
385	1	O	14054	0.02
385	2	3	14054	0.02
386	1	O	13962	0.04
386	2	4	13962	0.04
387	1	O	14015	0.02
387	2	5	14015	0.02
388	1	O	14020	0.03
388	2	6	14020	0.03
389	1	O	14018	0.03
389	2	7	14018	0.03
390	1	O	14042	0.02
390	2	8	14042	0.02
391	1	P	14005	0.02
391	2	Q	14005	0.02
392	1	P	13956	0.04
392	2	R	13956	0.04
393	1	P	13973	0.03
393	2	S	13973	0.03
394	1	P	13972	0.03
394	2	T	13972	0.03
395	1	P	13973	0.03
395	2	U	13973	0.03
396	1	P	14022	0.02
396	2	V	14022	0.02
397	1	P	13941	0.04
397	2	W	13941	0.04
398	1	P	13990	0.02
398	2	X	13990	0.02
399	1	P	13991	0.03
399	2	Y	13991	0.03
400	1	P	13993	0.03
400	2	Z	13993	0.03
401	1	P	13924	0.04
401	2	1	13924	0.04
402	1	P	13986	0.03
402	2	2	13986	0.03
403	1	P	14033	0.02
403	2	3	14033	0.02
404	1	P	13924	0.04
404	2	4	13924	0.04
405	1	P	13980	0.02
405	2	5	13980	0.02
406	1	P	13984	0.03
406	2	6	13984	0.03
407	1	P	13976	0.03
407	2	7	13976	0.03
408	1	P	14030	0.02
408	2	8	14030	0.02
409	1	Q	13985	0.03
409	2	R	13985	0.03
410	1	Q	13990	0.03
410	2	S	13990	0.03
411	1	Q	13967	0.03
411	2	T	13967	0.03
412	1	Q	13957	0.03
412	2	U	13957	0.03
413	1	Q	14005	0.03
413	2	V	14005	0.03
414	1	Q	13958	0.03
414	2	W	13958	0.03
415	1	Q	13997	0.03
415	2	X	13997	0.03
416	1	Q	14006	0.03
416	2	Y	14006	0.03
417	1	Q	14022	0.03
417	2	Z	14022	0.03
418	1	Q	13953	0.03
418	2	1	13953	0.03
419	1	Q	13999	0.03
419	2	2	13999	0.03
420	1	Q	14037	0.03
420	2	3	14037	0.03
421	1	Q	13939	0.04
421	2	4	13939	0.04
422	1	Q	13980	0.03
422	2	5	13980	0.03
423	1	Q	14000	0.03
423	2	6	14000	0.03
424	1	Q	13981	0.03
424	2	7	13981	0.03
425	1	Q	14012	0.03
425	2	8	14012	0.03
426	1	R	13972	0.03
426	2	S	13972	0.03
427	1	R	14019	0.03
427	2	T	14019	0.03
428	1	R	13996	0.03
428	2	U	13996	0.03
429	1	R	13963	0.04
429	2	V	13963	0.04
430	1	R	14000	0.03
430	2	W	14000	0.03
431	1	R	14029	0.02
431	2	X	14029	0.02
432	1	R	14059	0.02
432	2	Y	14059	0.02
433	1	R	14046	0.02
433	2	Z	14046	0.02
434	1	R	13971	0.03
434	2	1	13971	0.03
435	1	R	14035	0.03
435	2	2	14035	0.03
436	1	R	13985	0.04
436	2	3	13985	0.04
437	1	R	14009	0.03
437	2	4	14009	0.03
438	1	R	14027	0.03
438	2	5	14027	0.03
439	1	R	14054	0.02
439	2	6	14054	0.02
440	1	R	14028	0.03
440	2	7	14028	0.03
441	1	R	13987	0.03
441	2	8	13987	0.03
442	1	S	13978	0.03
442	2	T	13978	0.03
443	1	S	13962	0.03
443	2	U	13962	0.03
444	1	S	13990	0.03
444	2	V	13990	0.03
445	1	S	13969	0.04
445	2	W	13969	0.04
446	1	S	13975	0.03
446	2	X	13975	0.03
447	1	S	14004	0.03
447	2	Y	14004	0.03
448	1	S	14010	0.03
448	2	Z	14010	0.03
449	1	S	13974	0.03
449	2	1	13974	0.03
450	1	S	13985	0.03
450	2	2	13985	0.03
451	1	S	14001	0.03
451	2	3	14001	0.03
452	1	S	13979	0.03
452	2	4	13979	0.03
453	1	S	13964	0.03
453	2	5	13964	0.03
454	1	S	14006	0.03
454	2	6	14006	0.03
455	1	S	14002	0.03
455	2	7	14002	0.03
456	1	S	14007	0.03
456	2	8	14007	0.03
457	1	T	14026	0.03
457	2	U	14026	0.03
458	1	T	13987	0.03
458	2	V	13987	0.03
459	1	T	13998	0.04
459	2	W	13998	0.04
460	1	T	14028	0.03
460	2	X	14028	0.03
461	1	T	14054	0.02
461	2	Y	14054	0.02
462	1	T	13996	0.03
462	2	Z	13996	0.03
463	1	T	13961	0.04
463	2	1	13961	0.04
464	1	T	14044	0.03
464	2	2	14044	0.03
465	1	T	14006	0.03
465	2	3	14006	0.03
466	1	T	13992	0.04
466	2	4	13992	0.04
467	1	T	14033	0.02
467	2	5	14033	0.02
468	1	T	14058	0.02
468	2	6	14058	0.02
469	1	T	14030	0.03
469	2	7	14030	0.03
470	1	T	14006	0.03
470	2	8	14006	0.03
471	1	U	13986	0.03
471	2	V	13986	0.03
472	1	U	13995	0.04
472	2	W	13995	0.04
473	1	U	14021	0.02
473	2	X	14021	0.02
474	1	U	14036	0.02
474	2	Y	14036	0.02
475	1	U	13980	0.03
475	2	Z	13980	0.03
476	1	U	13930	0.04
476	2	1	13930	0.04
477	1	U	14031	0.02
477	2	2	14031	0.02
478	1	U	13992	0.03
478	2	3	13992	0.03
479	1	U	13994	0.03
479	2	4	13994	0.03
480	1	U	14031	0.02
480	2	5	14031	0.02
481	1	U	14038	0.02
481	2	6	14038	0.02
482	1	U	14023	0.03
482	2	7	14023	0.03
483	1	U	14011	0.03
483	2	8	14011	0.03
484	1	V	14003	0.03
484	2	W	14003	0.03
485	1	V	14000	0.03
485	2	X	14000	0.03
486	1	V	13997	0.03
486	2	Y	13997	0.03
487	1	V	14006	0.03
487	2	Z	14006	0.03
488	1	V	13938	0.04
488	2	1	13938	0.04
489	1	V	13987	0.03
489	2	2	13987	0.03
490	1	V	14038	0.02
490	2	3	14038	0.02
491	1	V	13973	0.03
491	2	4	13973	0.03
492	1	V	13998	0.03
492	2	5	13998	0.03
493	1	V	13998	0.03
493	2	6	13998	0.03
494	1	V	13995	0.03
494	2	7	13995	0.03
495	1	V	14069	0.01
495	2	8	14069	0.01
496	1	W	13988	0.03
496	2	X	13988	0.03
497	1	W	14008	0.03
497	2	Y	14008	0.03
498	1	W	13970	0.04
498	2	Z	13970	0.04
499	1	W	13934	0.04
499	2	1	13934	0.04
500	1	W	14003	0.03
500	2	2	14003	0.03
501	1	W	13963	0.04
501	2	3	13963	0.04
502	1	W	14031	0.03
502	2	4	14031	0.03
503	1	W	14023	0.03
503	2	5	14023	0.03
504	1	W	14014	0.03
504	2	6	14014	0.03
505	1	W	14062	0.03
505	2	7	14062	0.03
506	1	W	14011	0.03
506	2	8	14011	0.03
507	1	X	14051	0.02
507	2	Y	14051	0.02
508	1	X	14009	0.03
508	2	Z	14009	0.03
509	1	X	13935	0.03
509	2	1	13935	0.03
510	1	X	14043	0.02
510	2	2	14043	0.02
511	1	X	14027	0.03
511	2	3	14027	0.03
512	1	X	13992	0.03
512	2	4	13992	0.03
513	1	X	14027	0.02
513	2	5	14027	0.02
514	1	X	14054	0.02
514	2	6	14054	0.02
515	1	X	14024	0.03
515	2	7	14024	0.03
516	1	X	14003	0.03
516	2	8	14003	0.03
517	1	Y	14036	0.02
517	2	Z	14036	0.02
518	1	Y	13963	0.03
518	2	1	13963	0.03
519	1	Y	14077	0.01
519	2	2	14077	0.01
520	1	Y	14023	0.03
520	2	3	14023	0.03
521	1	Y	14033	0.03
521	2	4	14033	0.03
522	1	Y	14048	0.02
522	2	5	14048	0.02
523	1	Y	14091	0
523	2	6	14091	0
524	1	Y	14046	0.03
524	2	7	14046	0.03
525	1	Y	14027	0.03
525	2	8	14027	0.03
526	1	Z	14014	0.02
526	2	1	14014	0.02
527	1	Z	14014	0.03
527	2	2	14014	0.03
528	1	Z	14032	0.03
528	2	3	14032	0.03
529	1	Z	13977	0.04
529	2	4	13977	0.04
530	1	Z	14006	0.03
530	2	5	14006	0.03
531	1	Z	14033	0.02
531	2	6	14033	0.02
532	1	Z	14013	0.03
532	2	7	14013	0.03
533	1	Z	14027	0.03
533	2	8	14027	0.03
534	1	1	13946	0.04
534	2	2	13946	0.04
535	1	1	13962	0.04
535	2	3	13962	0.04
536	1	1	13967	0.03
536	2	4	13967	0.03
537	1	1	13965	0.03
537	2	5	13965	0.03
538	1	1	13959	0.03
538	2	6	13959	0.03
539	1	1	13973	0.03
539	2	7	13973	0.03
540	1	1	13958	0.04
540	2	8	13958	0.04
541	1	2	14024	0.03
541	2	3	14024	0.03
542	1	2	14010	0.03
542	2	4	14010	0.03
543	1	2	14041	0.02
543	2	5	14041	0.02
544	1	2	14072	0.01
544	2	6	14072	0.01
545	1	2	14040	0.03
545	2	7	14040	0.03
546	1	2	14019	0.03
546	2	8	14019	0.03
547	1	3	13958	0.04
547	2	4	13958	0.04
548	1	3	13997	0.03
548	2	5	13997	0.03
549	1	3	14019	0.03
549	2	6	14019	0.03
550	1	3	14002	0.03
550	2	7	14002	0.03
551	1	3	14041	0.02
551	2	8	14041	0.02
552	1	4	13985	0.03
552	2	5	13985	0.03
553	1	4	14028	0.03
553	2	6	14028	0.03
554	1	4	14026	0.03
554	2	7	14026	0.03
555	1	4	13994	0.03
555	2	8	13994	0.03
556	1	5	14049	0.02
556	2	6	14049	0.02
557	1	5	14055	0.03
557	2	7	14055	0.03
558	1	5	14018	0.02
558	2	8	14018	0.02
559	1	6	14046	0.03
559	2	7	14046	0.03
560	1	6	14019	0.03
560	2	8	14019	0.03
561	1	7	14009	0.03
561	2	8	14009	0.03

LS refinement shell

Resolution: 2.896→2.971 Å / Total num. of bins used: 20

	R_factor	Num. reflection	% reflection
R_free	0.399	862	-
R_work	0.356	16559	-
obs	-	-	96.43 %

Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°²)	L12 (°²)	L13 (°²)	L22 (°²)	L23 (°²)	L33 (°²)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å²)	T12 (Å²)	T13 (Å²)	T22 (Å²)	T23 (Å²)	T33 (Å²)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	2.9116	0.7361	-0.5108	1.5569	-0.7241	3.142	0.1603	-0.2546	-0.0298	0.1016	-0.1564	0.0324	0.2271	0.1498	-0.0039	0.2636	-0.0549	0.0273	0.1855	-0.1025	0.0692	209.759	49.4771	94.0046
2	2.5841	0.7619	-0.7675	1.2942	-0.6924	3.7325	-0.0371	0.486	0.1635	-0.1754	0.1445	-0.124	0.1309	0.0356	-0.1074	0.236	-0.0758	-0.0183	0.2414	0.0536	0.1582	213.0786	58.0486	62.9247
3	1.747	0.608	0.4925	3.5336	-1.5886	3.6188	0.1191	-0.0427	-0.1022	0.4043	-0.2051	0.0099	0.1095	0.219	0.086	0.3318	-0.102	0.0621	0.1598	-0.0578	0.045	188.8818	23.362	91.0917
4	1.3231	0.554	0.5568	3.2281	-1.4717	3.9233	-0.0048	0.1017	0.2181	-0.1194	0.1423	0.1752	0.1834	0.183	-0.1375	0.1682	0.0007	-0.055	0.0663	-0.0209	0.1899	184.4948	40.3875	63.9306
5	2.974	-1.4673	1.1621	3.5063	-0.2184	2.206	-0.2327	0.0149	-0.0263	0.5323	0.172	-0.2063	0.2646	0.2157	0.0607	0.441	0.0002	0.034	0.0913	-0.0276	0.0388	189.0601	-7.897	78.4563
6	1.8081	-0.8365	0.3085	2.6005	-0.5934	3.3546	-0.0284	0.1555	0.21	0.0535	-0.0948	-0.0592	-0.0477	0.2078	0.1232	0.0961	-0.0305	-0.0096	0.1455	-0.0175	0.1161	172.8766	9.4851	56.6846
7	3.8737	-1.0659	0.5559	1.9131	0.1513	2.1971	-0.2382	-0.1088	0.244	0.0512	0.0727	-0.2509	0.0852	0.2208	0.1655	0.3023	0.0687	0.0389	0.1188	0.0444	0.1294	206.6986	-27.8145	57.4961
8	3.318	-1.5916	0.0992	2.4186	-0.3076	3.0626	0.0664	0.3101	-0.0162	0.0098	-0.2008	0.1907	-0.0318	-0.2207	0.1344	0.0674	-0.0746	0.0409	0.2963	-0.1215	0.124	180.243	-19.5741	40.9441
9	3.2443	0.543	-0.1753	1.7779	-0.0051	2.0798	-0.0688	-0.4619	-0.0864	0.0184	-0.1325	-0.1635	0.0362	0.1204	0.2013	0.1432	0.0824	0.0369	0.2178	0.06	0.0958	229.4955	-27.3406	32.8112
10	3.5411	0.2936	0.5041	1.1108	-0.6186	2.3796	-0.2139	0.1062	0.0241	0.0938	0.0703	0.2148	0.0771	-0.2675	0.1435	0.1945	-0.106	0.0886	0.1383	-0.109	0.1659	201.0907	-32.1463	17.7947
11	2.0699	1.0992	0.2187	2.6883	0.2057	2.6985	0.0711	-0.0549	0.0049	0.1724	-0.1056	-0.2163	-0.1124	0.0462	0.0345	0.025	-0.0175	-0.0412	0.1169	0.0368	0.1033	243.5383	-5.327	11.6599
12	3.1426	0.9619	0.7466	2.5125	-0.4118	1.7569	-0.2699	0.1191	-0.182	-0.2378	0.166	0.142	0.2122	-0.1468	0.1039	0.1847	-0.0791	0.0245	0.1185	-0.0644	0.0934	221.1557	-20.2403	-6.3107
13	1.5368	0.2602	1.0748	3.7396	0.7953	3.0486	-0.0143	-0.1619	0.2794	0.1613	-0.029	0.0867	-0.0297	-0.1832	0.0433	0.0406	-0.0072	-0.0513	0.0616	-0.0305	0.1663	237.8172	26.6029	3.0684
14	1.8724	0.1203	0.4617	3.3673	0.8232	1.9592	-0.0639	0.023	-0.0822	-0.5251	-0.1027	0.3346	-0.0002	-0.1961	0.1666	0.2201	0.038	-0.1074	0.1225	-0.0557	0.0818	225.4308	9.5726	-21.4507
15	2.0132	-0.8694	-0.5678	2.1145	0.5447	4.2533	-0.0729	-0.361	0.2305	0.1529	0.278	-0.0852	0.2359	-0.0165	-0.205	0.0582	0.0445	-0.0991	0.1166	-0.1177	0.2388	213.4859	49.3118	7.526
16	2.3487	-0.8144	-0.5188	2.8394	1.882	4.2666	0.2013	0.2635	-0.0512	-0.2177	-0.1268	-0.1346	0.151	-0.426	-0.0745	0.1134	0.0197	-0.0349	0.2311	0.0634	0.0916	210.1912	39.6298	-23.1437
17	2.5079	-0.3121	-0.3683	1.4031	-0.477	3.689	0.0419	-0.1248	0.0201	0.0664	-0.0897	0.1034	0.3282	0.1073	0.0479	0.0761	-0.0245	-0.0339	0.1381	-0.0454	0.1286	180.89	51.625	16.1616
18	3.0075	-0.0995	-0.9329	1.3478	0.6697	4.3367	0.1208	0.7889	0.1928	-0.1508	-0.0173	-0.0681	0.1159	-0.2662	-0.1036	0.0694	0.0007	-0.0579	0.3914	0.1921	0.2042	181.2508	55.5476	-15.8438
19	1.9581	0.3897	0.796	2.2527	-2.0013	4.4513	0.1597	0.0592	-0.0795	0.2283	-0.1295	0.2826	0.1226	0.009	-0.0303	0.0949	-0.0739	0.0366	0.1718	-0.0857	0.1675	152.4198	33.5623	19.4905
20	1.9939	0.7688	0.5888	3.61	-2.3944	3.906	0.0017	0.2274	0.2868	-0.3964	0.1184	0.3154	0.2163	0.0412	-0.1201	0.1108	-0.007	-0.1495	0.1209	0.0213	0.3438	148.9834	49.0621	-8.626
21	1.8929	-0.1196	0.7124	3.9372	-0.1581	1.7438	0.1079	-0.0726	-0.0485	0.6473	-0.2417	-0.2568	0.1657	-0.0258	0.1338	0.2987	-0.2107	-0.1441	0.2376	0.0554	0.1937	139.7357	3.4455	11.8389
22	1.4468	-0.299	0.9862	3.225	-0.0184	2.9128	-0.0056	-0.0059	0.3441	-0.0407	-0.1734	-0.056	-0.0729	0.1238	0.1789	0.0467	-0.0071	-0.1109	0.1333	-0.0121	0.3658	127.009	23.5637	-10.1012
23	2.3006	-0.6984	1.3258	2.5537	0.0217	2.1286	-0.0135	0.0956	0.0625	0.0406	-0.1869	-0.5796	0.0267	0.2684	0.2004	0.062	-0.0235	-0.021	0.2098	0.1582	0.233	147.2957	-22.788	-7.7033
24	1.9887	-1.1805	0.2292	3.4472	-0.1121	2.1041	0.1606	0.2734	0.117	-0.3087	-0.3097	0.084	-0.1549	0.0482	0.1491	0.0446	0.0299	-0.0226	0.2558	-0.0289	0.1311	124.5412	-6.8935	-24.3041
25	5.9884	-0.3659	0.1871	1.0175	0.2755	2.7378	-0.2928	-0.4801	-0.3107	-0.0385	0.0489	-0.1381	0.0324	0.402	0.244	0.1495	0.1296	0.1031	0.3421	0.1523	0.3591	168.6193	-30.0187	-32.7396
26	5.5276	-1.0451	0.348	1.18	-0.1993	2.9773	-0.1515	0.6246	-0.3911	0.0139	-0.0845	0.0749	-0.0643	-0.2562	0.2359	0.0911	-0.0891	0.0754	0.3793	-0.1471	0.277	139.9593	-26.5393	-47.2091
27	3.6846	1.5341	0.5546	3.0062	0.2288	3.0033	0.1113	-0.451	-0.0702	0.1714	-0.3525	-0.3768	-0.2399	0.2177	0.2412	0.0849	-0.0181	0.069	0.4057	0.114	0.3117	188.0628	-14.5342	-55.4378
28	4.3812	1.5754	0.448	2.443	-0.2737	2.1493	-0.3921	0.2493	0.2204	-0.2672	0.1623	0.2881	0.0549	-0.3904	0.2298	0.2799	-0.0761	0.0558	0.3133	-0.1153	0.2743	162.4747	-24.6768	-72.323
29	1.8617	1.0407	0.7485	3.967	0.8311	2.7137	0.013	-0.2776	0.2766	0.2505	-0.2819	0.1391	-0.1678	-0.2651	0.2689	0.1662	-0.0186	0.002	0.2703	-0.0497	0.3049	192.6195	15.654	-69.8246
30	2.3515	1.2787	1.0108	3.7258	0.4692	2.1385	-0.1106	-0.0395	-0.0165	-0.6223	0.0045	0.4392	0.0928	-0.259	0.1061	0.414	0.0457	0.0064	0.2141	-0.0765	0.2235	177.686	-2.1485	-92.3377
31	1.7722	-1.5183	0.0132	4.5155	2.5897	4.0548	0.0038	-0.2161	0.4552	0.4058	0.3452	-0.7269	0.2167	0.0944	-0.3491	0.2872	0.0521	-0.1402	0.2084	-0.1307	0.5012	177.1243	45.1738	-74.6753
32	1.8276	-1.1457	0.2393	4.0401	2.1256	3.8744	0.3143	0.1658	-0.0383	-0.6686	-0.2836	-0.3386	-0.1439	-0.1877	-0.0307	0.4375	0.1705	0.1456	0.3179	0.0164	0.2522	174.1424	29.6835	-102.9385
33	2.9496	-0.3234	-0.9007	1.3861	-0.5836	3.6282	-0.0385	-0.4615	0.1358	0.0964	0.1173	-0.0249	0.2424	0.1101	-0.0787	0.2266	0.0247	-0.0235	0.2837	-0.1522	0.2133	146.372	58.6467	-72.1758
34	2.9925	-0.2259	-0.5036	1.0734	0.2089	3.3784	0.0125	0.3685	-0.0538	-0.1248	-0.1423	-0.1385	0.511	-0.0957	0.1298	0.3059	0.0127	0.1076	0.3011	0.0483	0.1707	150.4592	53.546	-103.8639

Refinement TLS group

ID	Refine-ID	Refine TLS-ID	Auth asym-ID	Auth seq-ID
1	X-RAY DIFFRACTION	1	A	1 - 241
2	X-RAY DIFFRACTION	2	B	1 - 241
3	X-RAY DIFFRACTION	3	C	1 - 241
4	X-RAY DIFFRACTION	4	D	1 - 241
5	X-RAY DIFFRACTION	5	E	1 - 241
6	X-RAY DIFFRACTION	6	F	1 - 241
7	X-RAY DIFFRACTION	7	G	1 - 241
8	X-RAY DIFFRACTION	8	H	1 - 241
9	X-RAY DIFFRACTION	9	I	1 - 241
10	X-RAY DIFFRACTION	10	J	1 - 241
11	X-RAY DIFFRACTION	11	K	1 - 241
12	X-RAY DIFFRACTION	12	L	1 - 241
13	X-RAY DIFFRACTION	13	M	1 - 241
14	X-RAY DIFFRACTION	14	N	1 - 241
15	X-RAY DIFFRACTION	15	O	1 - 241
16	X-RAY DIFFRACTION	16	P	1 - 241
17	X-RAY DIFFRACTION	17	Q	1 - 241
18	X-RAY DIFFRACTION	18	R	1 - 241
19	X-RAY DIFFRACTION	19	S	1 - 241
20	X-RAY DIFFRACTION	20	T	1 - 241
21	X-RAY DIFFRACTION	21	U	1 - 241
22	X-RAY DIFFRACTION	22	V	1 - 241
23	X-RAY DIFFRACTION	23	W	1 - 241
24	X-RAY DIFFRACTION	24	X	1 - 241
25	X-RAY DIFFRACTION	25	Y	1 - 241
26	X-RAY DIFFRACTION	26	Z	1 - 241
27	X-RAY DIFFRACTION	27	1	1 - 241
28	X-RAY DIFFRACTION	28	2	1 - 241
29	X-RAY DIFFRACTION	29	3	1 - 241
30	X-RAY DIFFRACTION	30	4	1 - 241
31	X-RAY DIFFRACTION	31	5	1 - 241
32	X-RAY DIFFRACTION	32	6	1 - 241
33	X-RAY DIFFRACTION	33	7	1 - 241
34	X-RAY DIFFRACTION	34	8	1 - 241

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