Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.9 Å / Relative weight: 1
Reflection
Resolution: 2.6→50 Å / Num. obs: 51643 / % possible obs: 92.2 % / Redundancy: 4 % / Net I/σ(I): 10.3
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Processing
Software
Name
Version
Classification
REFMAC
5.8.0103
refinement
DENZO
datareduction
SCALEPACK
datascaling
PHENIX
phasing
Refinement
Resolution: 2.6→30 Å / Cor.coef. Fo:Fc: 0.915 / Cor.coef. Fo:Fc free: 0.849 / SU B: 18.839 / SU ML: 0.37 / Cross valid method: THROUGHOUT / ESU R Free: 0.403 / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.28778
2568
5 %
RANDOM
Rwork
0.21721
-
-
-
obs
0.22076
49025
92.1 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å