Resolution: 3.4→19.91 Å / Cor.coef. Fo:Fc: 0.939 / Cor.coef. Fo:Fc free: 0.875 / SU B: 23.476 / SU ML: 0.368 / Cross valid method: THROUGHOUT / ESU R Free: 0.511 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES REFINED INDIVIDUALLY THERE ARE BREAKS IN THE STRUCTURE FROM GLU702 TO GLY708, ASN729 TO GLU737 AND VAL755 TO LEU760
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.25289
834
5 %
RANDOM
Rwork
0.18624
-
-
-
obs
0.18954
15849
99.43 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK