Software Name Version Classification SBC-Collectdata collection SHELXDphasing MLPHAREphasing DMmodel building ARPmodel building WARPmodel building HKL-3000phasing PHENIX(phenix.refine: 1.8.2_1309)refinement HKL-3000data reduction HKL-3000data scaling DMphasing
Refinement Method to determine structure : MAD / Resolution : 2.1→34.148 Å / SU ML : 0.29 / σ(F) : 1.97 / Phase error : 26.8 / Stereochemistry target values : MLRfactor Num. reflection % reflection Selection details Rfree 0.2368 2985 5.05 % random Rwork 0.1913 - - - all 0.1936 59075 - - obs 0.1936 59075 99.62 % -
Solvent computation Shrinkage radii : 0.9 Å / VDW probe radii : 1.11 Å / Solvent model : FLAT BULK SOLVENT MODELRefinement step Cycle : LAST / Resolution : 2.1→34.148 ÅProtein Nucleic acid Ligand Solvent Total Num. atoms 6800 0 33 288 7121
Refine LS restraints Refine-ID Type Dev ideal Number X-RAY DIFFRACTION f_bond_d0.008 6929 X-RAY DIFFRACTION f_angle_d1.089 9374 X-RAY DIFFRACTION f_dihedral_angle_d13.359 2574 X-RAY DIFFRACTION f_chiral_restr0.075 1104 X-RAY DIFFRACTION f_plane_restr0.005 1223
LS refinement shell Show large table (7 x 21) Hide large table Resolution (Å)Rfactor Rfree Num. reflection Rfree Rfactor Rwork Num. reflection Rwork Refine-ID % reflection obs (%)2.0992-2.1336 0.3726 149 0.2801 2642 X-RAY DIFFRACTION 100 2.1336-2.1704 0.2962 134 0.2617 2718 X-RAY DIFFRACTION 100 2.1704-2.2098 0.3171 143 0.2452 2636 X-RAY DIFFRACTION 100 2.2098-2.2523 0.3097 154 0.238 2715 X-RAY DIFFRACTION 100 2.2523-2.2983 0.2623 131 0.219 2661 X-RAY DIFFRACTION 100 2.2983-2.3482 0.2901 141 0.2249 2668 X-RAY DIFFRACTION 100 2.3482-2.4028 0.2512 137 0.2246 2716 X-RAY DIFFRACTION 100 2.4028-2.4629 0.2514 127 0.2176 2686 X-RAY DIFFRACTION 100 2.4629-2.5295 0.294 145 0.226 2667 X-RAY DIFFRACTION 100 2.5295-2.6039 0.2869 144 0.2298 2714 X-RAY DIFFRACTION 100 2.6039-2.6879 0.2928 152 0.2351 2658 X-RAY DIFFRACTION 100 2.6879-2.7839 0.2866 138 0.2337 2656 X-RAY DIFFRACTION 100 2.7839-2.8953 0.2728 129 0.2229 2727 X-RAY DIFFRACTION 100 2.8953-3.027 0.2606 161 0.2203 2660 X-RAY DIFFRACTION 100 3.027-3.1865 0.2554 151 0.2168 2670 X-RAY DIFFRACTION 100 3.1865-3.386 0.2643 144 0.2083 2695 X-RAY DIFFRACTION 100 3.386-3.6472 0.2478 145 0.1907 2665 X-RAY DIFFRACTION 100 3.6472-4.0137 0.2203 130 0.1688 2689 X-RAY DIFFRACTION 100 4.0137-4.5933 0.1968 146 0.1499 2688 X-RAY DIFFRACTION 100 4.5933-5.7825 0.2036 156 0.1601 2652 X-RAY DIFFRACTION 100 5.7825-34.1529 0.194 128 0.1742 2507 X-RAY DIFFRACTION 93
Refinement TLS params. Method : refined / Refine-ID : X-RAY DIFFRACTION
Show large table (25 x 30) Hide large table ID L11 (°2 )L12 (°2 )L13 (°2 )L22 (°2 )L23 (°2 )L33 (°2 )S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T11 (Å2 )T12 (Å2 )T13 (Å2 )T22 (Å2 )T23 (Å2 )T33 (Å2 )Origin x (Å)Origin y (Å)Origin z (Å)1 3.1153 -1.6261 0.4041 7.0565 -2.3839 2.7573 0.1063 -0.0418 -0.0845 0.6279 0.366 0.3757 -0.0651 -0.3063 -0.4688 0.32 0.0353 0.0405 0.4046 0.0099 0.3129 61.3082 27.1037 14.9731 2 2.8446 0.6305 1.8023 3.7138 2.6863 6.5475 0.4193 1.2546 -0.2219 -0.2539 0.3408 -0.767 -0.1667 0.1965 -0.7397 0.4439 0.0319 -0.0943 0.833 0.0144 0.4371 58.9613 25.5606 -7.6561 3 3.5278 -1.2008 -1.6063 3.7691 -0.3531 2.2018 0.4244 0.55 -0.0844 -0.2626 -0.2961 0.5341 -0.0164 -0.8678 -0.1263 0.3087 0.0344 -0.0284 0.6864 0.0579 0.5245 51.3402 26.9856 4.0841 4 3.7574 -0.3628 -3.3813 1.5022 -1.1436 4.2145 -0.0389 -0.5822 -0.2928 0.3119 0.3565 0.8668 -0.3227 -0.0612 -0.3179 0.6656 0.1715 0.2454 0.5123 0.132 0.5128 69.4658 53.209 -2.6405 5 2.5788 2.3672 -1.3264 3.3094 -2.7998 2.865 0.4632 0.4186 0.2899 0.4498 0.3861 0.7826 -0.5841 -0.7628 -0.5664 0.4726 0.2497 0.1606 0.7456 0.2865 1.0935 46.5281 42.878 4.1152 6 4.4821 1.1057 1.5545 7.5202 0.8526 3.4149 0.1317 -0.3834 0.6908 0.4964 0.148 1.6923 -0.1817 -0.9094 -0.4533 0.5193 0.1092 0.1896 0.6975 0.0718 0.7414 47.342 34.0737 15.3568 7 6.2207 1.5624 -0.2309 2.078 -0.1069 6.9628 0.5368 -0.8833 0.4897 1.2307 0.2363 -0.3445 -0.715 0.156 -0.5595 0.5725 0.18 0.0455 0.4191 -0.1173 0.4918 59.8859 37.4257 22.0465 8 3.6386 0.5996 -1.5614 1.5796 -1.129 4.932 0.1133 -0.1784 -0.2344 0.081 -0.2313 0.1206 0.4649 -0.5124 0.1202 0.3799 -0.0653 -0.0141 0.2105 -0.0732 0.2951 72.4163 17.3173 6.3305 9 3.4916 1.1802 1.7018 3.0169 0.0888 2.9301 -0.0366 -0.1992 0.7674 0.3683 -0.1801 0.0962 -0.597 0.2118 0.2423 0.4516 -0.0552 -0.0469 0.249 -0.0589 0.3974 80.0639 37.4309 11.4439 10 9.1035 -2.0727 -4.1361 2.6859 -0.5136 6.7779 0.1486 -0.2208 0.3634 -0.0839 0.1807 -0.1689 -0.2459 0.4364 -0.3946 0.3376 -0.0436 -0.013 0.2154 -0.0593 0.3078 77.8689 24.9865 9.4856 11 4.1342 -2.0647 -1.4224 4.433 -2.6152 4.6059 0.141 -0.5669 0.1721 0.318 -0.1677 -0.5687 0.2465 0.3529 0.0822 0.2716 0.0043 -0.0264 0.169 -0.0197 0.3732 86.9337 21.7736 6.0977 12 6.9525 -4.7576 -2.4595 3.3338 1.4969 1.8795 0.6902 0.3872 -0.3982 -1.4471 -0.5951 0.5544 -0.0347 -0.3278 -0.0137 0.5935 0.1567 0.0102 0.5643 -0.039 0.5039 73.5748 35.2836 -16.6793 13 1.697 -1.3713 -1.1141 6.2503 1.4779 5.7389 1.1121 0.5059 -0.2797 -1.526 -0.9145 0.6292 -0.2617 -0.6154 -0.1831 0.8405 0.2314 -0.1583 0.6426 -0.0539 0.553 69.7968 40.1841 -20.3943 14 5.1529 -3.4129 3.813 6.0945 -5.214 4.6627 0.0296 0.5139 0.5466 -0.5113 -0.5556 -1.0761 0.1384 1.0957 0.5722 0.3664 0.0294 0.0924 0.4049 -0.0051 0.4816 90.2385 27.6113 -6.2337 15 5.8418 -1.3966 0.6743 6.1844 -2.4374 5.8374 0.0233 -0.1557 -0.2227 -0.2867 -0.1791 -0.1914 0.978 0.1066 0.0813 0.4024 0.0915 0.024 0.2218 -0.0705 0.3172 81.0289 12.8754 -0.3312 16 4.6746 -0.4335 0.5414 5.4985 -1.2349 1.5806 0.0282 0.2599 -0.4118 0.0191 0.1984 0.3058 0.2688 -0.5884 -0.2304 0.2731 -0.0483 -0.079 0.5 0.0196 0.2283 64.4376 1.3363 48.4396 17 1.0081 -0.4403 -1.5912 3.0499 -3.7505 9.3377 -0.054 0.3988 0.2563 -0.2125 0.2032 0.1096 -0.3817 -0.1686 -0.1828 0.3767 -0.084 -0.0891 0.5191 0.0545 0.3852 66.1161 14.7854 32.1081 18 1.6302 -1.0012 -0.7543 3.1869 -1.8146 2.3779 -0.1329 0.2574 0.2646 -0.4764 0.2018 -0.0455 -0.4682 0.1949 -0.096 0.3759 -0.1325 -0.0564 0.5219 -0.0375 0.3602 72.2885 16.5298 37.0561 19 1.3449 0.1132 0.6853 3.8286 1.1482 3.9555 0.1085 -0.2396 -0.0725 0.032 -0.0383 -0.1639 -0.1502 0.0826 -0.0888 0.2064 -0.01 -0.0596 0.3496 -0.0127 0.2215 72.1254 9.1627 47.5389 20 8.9574 -2.353 6.6393 1.5956 -1.8463 4.8578 -0.3469 -0.8687 0.4558 0.2338 0.3019 -0.5473 0.2465 -0.8559 0.0449 0.5923 -0.1018 -0.1162 0.5744 -0.1544 0.4526 68.2082 -12.882 30.2108 21 4.8011 -0.9159 3.0593 2.7652 0.6965 5.1514 0.6574 -0.904 -0.118 0.7236 -0.2103 -0.2711 0.3441 0.2645 -0.3323 0.6616 -0.2449 -0.1646 0.6893 -0.0819 0.4727 63.9757 -16.377 25.1335 22 0.8942 0.1554 -0.6578 5.3274 4.5295 5.7414 0.0617 0.4852 -0.8823 -0.2005 0.4976 -0.1884 0.3888 0.4418 -0.4456 0.3777 0.0019 -0.1065 0.6658 -0.2063 0.6199 81.9347 -1.8726 41.7668 23 2.4087 2.6352 1.2853 6.1371 3.141 4.1701 0.1355 -0.2429 -0.3946 0.6992 0.2822 -0.1137 0.6278 0.0409 -0.3954 0.3876 -0.0114 -0.137 0.4609 0.0559 0.3418 71.5092 -0.4996 55.3028 24 4.8905 0.771 2.2556 4.6809 0.2743 4.1273 -0.1528 -0.363 -0.2778 -0.1382 0.4459 0.4922 -0.2373 -0.9825 -0.0596 0.2911 -0.0203 -0.1153 0.6698 0.1456 0.406 49.2001 11.7436 37.0566 25 6.6698 0.7816 1.7665 3.1759 -0.7651 2.9212 0.2959 -0.4553 -1.5063 -0.2549 0.2672 0.2748 0.8909 -0.6224 -0.5179 0.5168 -0.1983 -0.1887 0.7543 0.2141 0.8335 47.5733 -4.7405 41.3688 26 1.032 0.1776 -0.472 1.8679 0.3487 1.1259 -0.008 -0.859 -0.2938 -0.1619 -0.1576 1.0833 0.1295 -1.0433 -0.4813 0.2167 -0.1873 -0.3272 1.386 0.459 0.964 37.4764 5.928 37.4335 27 2.5167 0.5546 0.3934 2.6956 0.1896 2.057 -0.2339 0.3577 0.134 -0.9658 0.4157 0.0728 -0.2079 0.1035 -0.2001 0.7075 -0.2691 -0.0748 0.5335 -0.042 0.4815 61.9179 2.8492 13.9244 28 1.0052 -0.3794 -0.1572 1.1554 -0.6902 0.6267 0.095 -0.6768 -0.4963 -0.2772 0.2524 0.6076 0.518 -1.1322 0.1771 0.4631 -0.2997 -0.4595 1.0152 0.2311 0.8757 38.4863 3.4209 23.7884 29 0.4538 1.2132 0.2684 3.0905 0.5579 2.0902 -0.3755 0.2793 0.4328 0.0954 0.5448 1.1717 -0.4739 -1.4735 0.0105 0.511 0.0658 -0.138 1.202 0.2628 0.8269 36.5404 13.6154 35.0003 30 2.3356 -2.1047 -3.3903 8.412 1.7491 8.6191 -0.023 -0.5539 1.0955 -0.3194 0.8015 0.8303 -1.2826 -0.9957 -0.5769 0.5443 0.1115 -0.2283 0.739 0.0799 0.7715 47.4888 22.1587 34.7764
Refinement TLS group Show large table (4 x 30) Hide large table ID Refine-ID Refine TLS-ID Selection details 1 X-RAY DIFFRACTION 1 chain 'A' and (resid -9 through 26 ) 2 X-RAY DIFFRACTION 2 chain 'A' and (resid 27 through 55 )3 X-RAY DIFFRACTION 3 chain 'A' and (resid 56 through 112 )4 X-RAY DIFFRACTION 4 chain 'A' and (resid 113 through 160 )5 X-RAY DIFFRACTION 5 chain 'A' and (resid 161 through 183 )6 X-RAY DIFFRACTION 6 chain 'A' and (resid 184 through 203 )7 X-RAY DIFFRACTION 7 chain 'A' and (resid 204 through 217 )8 X-RAY DIFFRACTION 8 chain 'B' and (resid -9 through 26 ) 9 X-RAY DIFFRACTION 9 chain 'B' and (resid 27 through 73 )10 X-RAY DIFFRACTION 10 chain 'B' and (resid 74 through 89 )11 X-RAY DIFFRACTION 11 chain 'B' and (resid 90 through 112 )12 X-RAY DIFFRACTION 12 chain 'B' and (resid 113 through 134 )13 X-RAY DIFFRACTION 13 chain 'B' and (resid 135 through 160 )14 X-RAY DIFFRACTION 14 chain 'B' and (resid 161 through 183 )15 X-RAY DIFFRACTION 15 chain 'B' and (resid 184 through 218 )16 X-RAY DIFFRACTION 16 chain 'C' and (resid -1 through 26 ) 17 X-RAY DIFFRACTION 17 chain 'C' and (resid 27 through 54 )18 X-RAY DIFFRACTION 18 chain 'C' and (resid 55 through 73 )19 X-RAY DIFFRACTION 19 chain 'C'