pH: 6.5 詳細: 30 MM DI-ETHYLENE GLYCOL, 30 MM TRI-ETHYLENE GLYCOL, 30 MM TETRA-ETHYLENE GLYCOL, 30 MM PENTA-ETHYLENE GLYCOL, 45 MM IMIDAZOLE, 20% (W/V) PEGMME550, 10% (W/V) PEG 20000 AND 56 MM MES (PH 6.5)
解像度: 2.6→36.42 Å / Cor.coef. Fo:Fc: 0.926 / Cor.coef. Fo:Fc free: 0.898 / SU B: 11.193 / SU ML: 0.244 / 交差検証法: THROUGHOUT / ESU R: 0.503 / ESU R Free: 0.317 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. IDENTITY OF THE BOUND FE CONFIRMED FROM ANOMALOUS DIFFRACTION DATA COLLECTED AT 1.74A FROM THE SAME CRYSTAL.
Rfactor
反射数
%反射
Selection details
Rfree
0.27749
1506
5 %
RANDOM
Rwork
0.22654
-
-
-
obs
0.22918
28422
97.25 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK